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The crystal structure of dimethyl 4-methoxy-2,3,5,6-tetrachlorophenyl phosphate

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Abstract

The crystal structure of dimethyl 4-methoxy-2,3,5,6-tetrachlorophenyl phosphate was determined by X-ray analysis. It crystallized in the space group P2 1/c (#14) with a = 9.446(2), b = 11.977(2), c = 12.306(2) Å, β = 96.55(1)°, V = 1383.1(4) Å3, D calc = 1,665 5/cm3, and Z = 4.

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References

  1. Reetz, T. U.S. Patent 2935518, 19609, CA 54, 19598, 1960; (b) Reetz, T.; Powers, J.F.; Grahan, G.R. Abstract of papers for the 134th meeting; Am. Chem. Soc.: Chicago, 1958; p 86; (c) Ramirez, F.; Chen, E.H.; Dershowitz, S. J. Am. Chem. Soc. 1959, 81, 4338.

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Authors and Affiliations

  1. Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, 354 Fenglin Lu, Shanghai, 200032, China

    Min Shi

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  1. Min Shi
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Shi, M. The crystal structure of dimethyl 4-methoxy-2,3,5,6-tetrachlorophenyl phosphate. Journal of Chemical Crystallography 29, 497–499 (1999). https://doi.org/10.1023/A:1009583531502

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  • DOI: https://doi.org/10.1023/A:1009583531502

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