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Crystal structures of methanol and ethanol solvates of secalonic acid D

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Abstract

The methanol and ethanol solvates of secalonic acid D (SAD) share the same packing pattern exhibited by the acetic acid solvate of secalonic acid A, the enantiomer of SAD. Both solvates crystallize in space group C2, with a = 17.648(2), b = 7.0897(10), c = 13.060(2) Å and β = 93.482(2)° for the methanol form, and a = 18.010(4), b = 7.395(2), c = 13.053(3) Å andβ = 96.882(4)° for the ethanol form.

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Authors and Affiliations

  1. Department of Chemistry, University of Missouri-Columbia, Columbia, Missouri, 65211

    Charles L. Barnes

  2. Phytera, 377 Plantation St., Worcester, Massachusetts, 01605

    Rosa Ubillas

  3. Nat Prod Consulting Services, 846 San Carlos Ave., El Granada, California, 94018-2439

    Michael S. Tempesta

Authors
  1. Charles L. Barnes
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  2. Rosa Ubillas
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  3. Michael S. Tempesta
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Correspondence to Charles L. Barnes.

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Barnes, C.L., Ubillas, R. & Tempesta, M.S. Crystal structures of methanol and ethanol solvates of secalonic acid D. Journal of Chemical Crystallography 29, 1031–1035 (1999). https://doi.org/10.1023/A:1009576817952

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