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Chemical preparation and crystal structure of 6′-butoxy-2,6-diamino-3,3′azo-dipyridine monohydrate

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Abstract

Chemical preparation, X-ray single crystal, and calorimetric studies of C14H18N6O · H2O are described. The compound crystallizes in the triclinic space group, P \({\bar 1}\) with unit cell dimensions: a = 6.2640(3), b = 10.9840(4), c = 12.2220(3) Å, α = 105.03(2), β = 96.96(2), γ = 101.6(2)°, V = 712.10(5) Å3, and Z = 2. The 6′-butoxy-2,6-diamino-3,3′-azo-dipyridine monohydrate structure is built up from organic layers parallel to the (120) plane linked via O—H···N bond.

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References

  1. Masse, R.; Zyss, J. Mol. Eng. 1991, 1, 141.

    Google Scholar 

  2. Masse, R.; Bagieu-Beucher, M.; Pecoult, J.; Levy, J. P.; Zyss, J. Nonlinear Apt. 1993, 5, 413.

    Google Scholar 

  3. Zyss, J.; In Conjugated Polymeric Materials: Opportunities in Electronics, Optoelectronics and Molecular Electronic; Brédas, J. L.; Chance, R. R., Eds.; Kluver: Dordrecht, 1990, p 545.

    Google Scholar 

  4. Toumi, M.; Hlel, F.; Ben Chabaane, T.; Smiri, L.; Laligant, Y.; Emry, J. Eur. J. Solid State Inorg. Chem. 1998, 35, 689-697.

    Google Scholar 

  5. Sheldrick, G. M. SHELXS-86, in Crystallographic Computing 3; Sheldrick, G. M.; Krüger, C.; Goddard, R. Eds.; Oxford University Press: Oxford, 1986.

    Google Scholar 

  6. Sheldrick, G. M. SHELXL-93, A Program for the Refinement of Crystal Structures from Diffraction Data; University of Góttingen: Germany, 1993.

    Google Scholar 

  7. Brown I. D. Acta Crystallogr. 1976, A32, 24.

    Google Scholar 

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Authors and Affiliations

  1. Laboratoire de Chimie Inorganique et Structurale, Faculté des Sciences de Bizerte, 7021, Jarzouna, Tunisia

    Faouzi Hlel & Leila Smiri

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  1. Faouzi Hlel
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  2. Leila Smiri
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Hlel, F., Smiri, L. Chemical preparation and crystal structure of 6′-butoxy-2,6-diamino-3,3′azo-dipyridine monohydrate. Journal of Chemical Crystallography 29, 667–670 (1999). https://doi.org/10.1023/A:1009567619284

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  • DOI: https://doi.org/10.1023/A:1009567619284

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