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Crystal structure and thermal analysis of 1,5-diammonium-2-methyl pentane sulfate monohydrate

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Abstract

Chemical preparation, x-ray single crystal, and thermal analysis of C6H18N2SO4·H2O (denoted DMPS) are described. The compound crystallizes in the triclinic system with P\(\overline 1\) space group. Its unit cell dimensions are a = 5.826(1) Å, b = 10.014(1) Å, c = 11.221(1) Å, α = 66.716(1)°, β = 84.395(1)°, γ = 83.759(1)°, V = 596.7(1) Å3, and Z = 2. The DMPS structure is built up from inorganic chains parallel to the a axis and linked via O(W)-H···O hydrogen bonds. These chains are interconnected by organic groups. Thermal analysis reveals the presence of one water molecule in the structure and shows a reversible weak phase transition.

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Authors and Affiliations

  1. Laboratoire de Chimie du Solide, Département de Chimie, Faculté des Sciences de Monastir, Université du Centre, 5000, Monastir (, Tunisia

    Taha Guerfel & Amor Jouini

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  1. Taha Guerfel
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  2. Amor Jouini
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Guerfel, T., Jouini, A. Crystal structure and thermal analysis of 1,5-diammonium-2-methyl pentane sulfate monohydrate. Journal of Chemical Crystallography 30, 95–98 (2000). https://doi.org/10.1023/A:1009561411167

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