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Crystal and molecular structure of the symmetrical bidentate ligand 3,3-di(1-pyrazolyl)pentane, CH3CH2C(C3H3N2)2CH2CH3

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Abstract

The title compound crystallizes in the centrosymmetric space group C2/c with a = 14.4005(23), b = 7.0494(12), c = 11.2462(20) Å, β = 101.572(13)° and Z = 4; the molecule lies on a crystallographic C 2 axis. Hydrogen atoms were both located and refined.

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References

  1. Bessel, C.A.; See, R.F.; Jameson, D.L.; Churchill, M.R.; Takeuchi, K.J. J. Chem. Soc. Dalton Trans. 1992, 3223.

  2. Churchill, M.R.; Churchill, D.G.; Huynh, M.H.V.; Takeuchi, K.J.; Castellano, R.K.; Jameson, D.L. J. Chem. Crystallogr. 1996, 26, 93.

    Google Scholar 

  3. Churchill, M.R.; Churchill, D.G.; Huynh, M.H.V.; Takeuchi, K.J.; Castellano, R.K.; Jameson, D.L. J. Chem. Crystallogr. 1996, 26, 179.

    Google Scholar 

  4. Trofimenko, S. J. Am. Chem. Soc. 1970, 92, 5118.

    Google Scholar 

  5. Churchill, M.R.; Lashewycz, R.A.; Rotella, F.J. Inorg. Chem. 1977, 16, 265.

    Google Scholar 

  6. International Tables for X-Ray Crystallography, Vol. 1 (2nd ed.) Kynoch Press: Birmingham, England, 1965; (a) p 89; (b) p 101.

  7. Karle, I.L.; Dragonette, K.S.; Brenner, S.A. Acta Crystallogr. 1965, 19, 713.

    Google Scholar 

  8. Bearden, J.A. Rev. Mod. Phys. 1967, 39, 78.

    Google Scholar 

  9. Sheldrick, G.M. SHELXTL PLUS; Siemens Analytical Instruments: Madison, WI, 1989.

    Google Scholar 

  10. Sheldrick, G.M. SHELXTL PLUS. An Integrated System for Solving, Refining and Displaying Crystal Structures from Diffraction Data. For Nicolet R3m/V; University of Göttingen: Germany 1987.

    Google Scholar 

  11. International Tables for X-Ray Crystallography. Vol. 4, Kynoch Press: Birmingham, England, 1974; (a) Table 2.2B on pp 99–101; (b) Table 2.3.1 on pp 149–150; (c) Tables 5.5A and 5.5B on pp 325–328.

  12. Zachariasen, W.H. Acta Crystallogr. 1963, 16, 1139; (b) idem, ibid. 1967, 23, 558.

    Google Scholar 

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Churchill, M.R., Churchill, D.G., Huynh, M.H.V. et al. Crystal and molecular structure of the symmetrical bidentate ligand 3,3-di(1-pyrazolyl)pentane, CH3CH2C(C3H3N2)2CH2CH3. Journal of Chemical Crystallography 29, 463–467 (1999). https://doi.org/10.1023/A:1009523312846

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  • DOI: https://doi.org/10.1023/A:1009523312846

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