Abstract
The crystallographic structure of a novel camphanic amide 5 is disclosed by x-ray analysis. It crystallized in the space group P212121(#19) with a = 15.663(3), b = 17.848(3), c = 7.935(8) Å, V = 2209.5(6) Å3, Dcalc = 1.165 g/cm3, and Z = 4.
References
Bednarski, M.; Danishefsky, S. J. Am. Chem. Soc. 1983, 105, 3716. (b) Togni, A. Organometallics 1990, 9, 3106.
Schurig, V.; Weber, R. J. Chromatogr. 1981, 217, 51. (b) Schurig, V.; Bukle, W. J. Am. Chem. Soc. 1982, 104, 7573.
Goering, H.L. Eikenberry, J.N.; Koermer, G.S.; Lattimer, C.J. J. Am. Chem. Soc. 1974, 96, 1493. (b) Goering, H.L.; Eikenberry, J.N.; Koermer, G.S. J. Am. Chem. Soc. 1971, 93, 5913. (c) Sulliyan, G.R. Topics Stereochem. 1976, 10, 287.
Wei, H.-X., Wang, Z.-M.; Shi, M. Chem. Pharm. Bull. 1999, 47, 909.
Stevens R.V. Gaeta F.C.A.; Lawrence D.S. J. Am. Chem. Soc. 1983, 105, 7713.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Shi, M., Lei, GX. The crystallographic structure of a novel camphanic amide. Journal of Chemical Crystallography 29, 1211–1213 (1999). https://doi.org/10.1023/A:1009511802235
Issue Date:
DOI: https://doi.org/10.1023/A:1009511802235