Abstract
Lipophilic calix[4]resorcinarenes, derived from lauryl aldehyde and resorcinol, are strongly adsorbed on the modified silica gel RP-18 for HPLC chromatography, while their solutions are passed through the column. The calix[4]resorcinarene-coated RP-18 phases were found to be useful beds for HPLC separation of uracil, thymine and cytosine.
Similar content being viewed by others
References
J. Snopek and E. Smolkova-Keulemansova: Cyclodextrins in analytical separation methods, in J.-M. Lehn (ed.), Comprehensive Supramolecular Chemistry, Vol. 3, Chap. 18. Pergamon Press (1996), and references cited therein.
A. Harada and B. Zsadon: Separation, removal, or enrichment of components on a preparative scale, in J.-M. Lehn (ed.), Comprehensive Supramolecular Chemistry, Vol. 3, Chap. 19. Pergamon Press (1996), and references cited therein.
D. Sybilska and J.Żukowski: in A. M. Krustlovic (ed.), Chiral Separation, Chap. 7, New York (1989), p. 147.
D. Sybilska, A. Bielejewska, R. Nowakowski, K. Duszczyk, and J. Jurczak.: J. Chromatogr. 625, 349 (1992).
R. Nowakowski, A. Bielejewska, K. Duszczyk, and Sybilska D.: J. Chromatogr A. 782, 1 (1997).
J. Żukowski, M. Pawłowska, and M. Pietraszkiewicz: Chromatographia 32, 82 (1991).
T. Shinbo, T. Yamaguchi, K. Nishimura, and M. Sugiura: J. Chromatogr. 405, 145 (1987).
J. P. Joly and B. Bross: Tetrahedron Lett. 30, 4231 (1989).
G. D. Y. Sogah and D. J. Cram: J. Am. Chem. Soc. 101, 3035 (1979).
R. M. I. Izatt, J. S. Bradshaw, R. L. Bruening, B. J. Tarbet, and M. L. Bruening: Selective separation using supported devices, in J.-M. Lehn (ed.), Comprehensive Supramolecular Chemistry, Vol. 10, Chap. 1, Pergamon Press (1996), and references cited therein.
J. D. Lamb and R. G. Smith: Applications of macrocyclic ligands to high-performance analysis, in J.-M. Lehn (ed.), Comprehensive Supramolecular Chemistry, Vol. 10, Chap. 4, Pergamon Press (1996), and references cited therein.
R. Ungaro, A. Pochini, A. Mangia, and G. D. Andreetti: Anal. Lett. 16, 1027 (1983).
D. Glennon, K. O'Connor, R. Srijaranai, K. Manley, S. J. Harris, and M. A. McKervey: Anal. Lett. 26, 153 (1993).
M. Pietraszkiewicz, O. Pietraszkiewicz, and M. Koźbiał: Polish J. Chem. 72, 1963 (1998).
O. Pietraszkiewicz and M. Pietraszkiewicz.: Polish J. Chem. 72, 2418 (1998).
F. Davis, L. O'Toole, R. Short, and C. J. M. Stirling: Langmuir 12, 1892 (1996).
F. Davis and C. J. M. Stirling: Langmuir 12, 5365 (1996).
Y. Aoyama, Y. Tanaka, H. Toi, and H. Ogoshi: J. Am. Chem. Soc. 110, 634 (1988).
K. Kobayashi, Y. Asakawa, Y. Kato, and Y. Aoyama: J. Am. Chem. Soc. 114, 10307 (1992).
H. Klein, and R. Leubolt: J. Chromatogr. 640, 259 (1993).
S. Yonekura, M. Iwasaki, M. Kai, and Y. Ohkura: J. Chromatogr. B 654, 19 (1994).
A. F. Danil de Namor, M. T. Garrido Pardo, D. A. P. Tanaka, F. J. S. Velarde, and J. D. C. Garcia: J. Chem. Soc., Faraday Trans. 89, 2727 (1993).
K. Kurihara, K. Ohto, Y. Tanaka, Y. Aoyama, and T. Kunitake: J. Am. Chem. Soc. 113, 444 (1991).
L. R. MacGillivray and J. L.Atwood: J. Am. Chem. Soc. 119, 6931 (1997).
Rights and permissions
About this article
Cite this article
Pietraszkiewicz, O., Pietraszkiewicz, M. Separation of Pyrimidine Bases on a HPLC Stationary RP-18 Phase Coated with Calix[4]resorcinarene. Journal of Inclusion Phenomena 35, 261–270 (1999). https://doi.org/10.1023/A:1008151100076
Issue Date:
DOI: https://doi.org/10.1023/A:1008151100076