Skip to main content
Log in

Separation of Pyrimidine Bases on a HPLC Stationary RP-18 Phase Coated with Calix[4]resorcinarene

  • Published:
Journal of inclusion phenomena and macrocyclic chemistry Aims and scope Submit manuscript

Abstract

Lipophilic calix[4]resorcinarenes, derived from lauryl aldehyde and resorcinol, are strongly adsorbed on the modified silica gel RP-18 for HPLC chromatography, while their solutions are passed through the column. The calix[4]resorcinarene-coated RP-18 phases were found to be useful beds for HPLC separation of uracil, thymine and cytosine.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. J. Snopek and E. Smolkova-Keulemansova: Cyclodextrins in analytical separation methods, in J.-M. Lehn (ed.), Comprehensive Supramolecular Chemistry, Vol. 3, Chap. 18. Pergamon Press (1996), and references cited therein.

  2. A. Harada and B. Zsadon: Separation, removal, or enrichment of components on a preparative scale, in J.-M. Lehn (ed.), Comprehensive Supramolecular Chemistry, Vol. 3, Chap. 19. Pergamon Press (1996), and references cited therein.

  3. D. Sybilska and J.Żukowski: in A. M. Krustlovic (ed.), Chiral Separation, Chap. 7, New York (1989), p. 147.

  4. D. Sybilska, A. Bielejewska, R. Nowakowski, K. Duszczyk, and J. Jurczak.: J. Chromatogr. 625, 349 (1992).

    Google Scholar 

  5. R. Nowakowski, A. Bielejewska, K. Duszczyk, and Sybilska D.: J. Chromatogr A. 782, 1 (1997).

    Google Scholar 

  6. J. Żukowski, M. Pawłowska, and M. Pietraszkiewicz: Chromatographia 32, 82 (1991).

    Google Scholar 

  7. T. Shinbo, T. Yamaguchi, K. Nishimura, and M. Sugiura: J. Chromatogr. 405, 145 (1987).

    Google Scholar 

  8. J. P. Joly and B. Bross: Tetrahedron Lett. 30, 4231 (1989).

    Google Scholar 

  9. G. D. Y. Sogah and D. J. Cram: J. Am. Chem. Soc. 101, 3035 (1979).

    Google Scholar 

  10. R. M. I. Izatt, J. S. Bradshaw, R. L. Bruening, B. J. Tarbet, and M. L. Bruening: Selective separation using supported devices, in J.-M. Lehn (ed.), Comprehensive Supramolecular Chemistry, Vol. 10, Chap. 1, Pergamon Press (1996), and references cited therein.

  11. J. D. Lamb and R. G. Smith: Applications of macrocyclic ligands to high-performance analysis, in J.-M. Lehn (ed.), Comprehensive Supramolecular Chemistry, Vol. 10, Chap. 4, Pergamon Press (1996), and references cited therein.

  12. R. Ungaro, A. Pochini, A. Mangia, and G. D. Andreetti: Anal. Lett. 16, 1027 (1983).

    Google Scholar 

  13. D. Glennon, K. O'Connor, R. Srijaranai, K. Manley, S. J. Harris, and M. A. McKervey: Anal. Lett. 26, 153 (1993).

    Google Scholar 

  14. M. Pietraszkiewicz, O. Pietraszkiewicz, and M. Koźbiał: Polish J. Chem. 72, 1963 (1998).

    Google Scholar 

  15. O. Pietraszkiewicz and M. Pietraszkiewicz.: Polish J. Chem. 72, 2418 (1998).

    Google Scholar 

  16. F. Davis, L. O'Toole, R. Short, and C. J. M. Stirling: Langmuir 12, 1892 (1996).

    Google Scholar 

  17. F. Davis and C. J. M. Stirling: Langmuir 12, 5365 (1996).

    Google Scholar 

  18. Y. Aoyama, Y. Tanaka, H. Toi, and H. Ogoshi: J. Am. Chem. Soc. 110, 634 (1988).

    Google Scholar 

  19. K. Kobayashi, Y. Asakawa, Y. Kato, and Y. Aoyama: J. Am. Chem. Soc. 114, 10307 (1992).

    Google Scholar 

  20. H. Klein, and R. Leubolt: J. Chromatogr. 640, 259 (1993).

    Google Scholar 

  21. S. Yonekura, M. Iwasaki, M. Kai, and Y. Ohkura: J. Chromatogr. B 654, 19 (1994).

    Google Scholar 

  22. A. F. Danil de Namor, M. T. Garrido Pardo, D. A. P. Tanaka, F. J. S. Velarde, and J. D. C. Garcia: J. Chem. Soc., Faraday Trans. 89, 2727 (1993).

    Google Scholar 

  23. K. Kurihara, K. Ohto, Y. Tanaka, Y. Aoyama, and T. Kunitake: J. Am. Chem. Soc. 113, 444 (1991).

    Google Scholar 

  24. L. R. MacGillivray and J. L.Atwood: J. Am. Chem. Soc. 119, 6931 (1997).

    Google Scholar 

Download references

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Pietraszkiewicz, O., Pietraszkiewicz, M. Separation of Pyrimidine Bases on a HPLC Stationary RP-18 Phase Coated with Calix[4]resorcinarene. Journal of Inclusion Phenomena 35, 261–270 (1999). https://doi.org/10.1023/A:1008151100076

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1023/A:1008151100076

Navigation