Skip to main content
Log in

Fracture characteristics of SiC particle reinforced oxynitride glass using chevron-notch three-point bend specimens

  • Published:
International Journal of Fracture Aims and scope Submit manuscript

Abstract

The fracture toughness K1c and the effective fracture surface energy γeff, of oxynitride glass (m)/SiC(p) brittle particulate composites were measured by means of stable fracture tests, using chevron-notch three-point bend specimens. In comparison to oxide glasses, the oxynitride glass matrix is noticeably tougher: K1cm = 1.2 MPa.\(\sqrt m\) and γeff = 5 J/m2. The addition of SiC particles, 6 μm in diameter, results in a significant toughening: K1c = 2.5 MPa.\(\sqrt m\) and γeff = 9.1 J/m2 for the composite with 40 vol\% SiC. In such systems, with strong particle-matrix interfacial bonding, and where (Ep, K1cp, σrp) > (Em, K1cm, σrm), the main toughening contribution is due to a discrete pinning of the crack by particles near the crack tip in conjunction to bowing of the crack front between particles, and to a small scale bridging mechanism.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  • Baron, B., Chartier, T., Rouxel, T., Verdier, P. and Laurent, Y. (1997). SiC particle reinforced oxynitride glass: processing and mechanical properties. Journal of the European Ceramic Society 17, 773-780.

    Article  Google Scholar 

  • Bluhm, J.I. (1975). Slice synthesis of a three dimensional 'work of fracture' specimen. Engineering Fracture Mechanics 7, 593-604.

    Article  Google Scholar 

  • Boccaccini, A.R. and Trusty, P.A. (1996). Toughening and strengthening of glass by Al2O3 platelets. Journal of Materials Science Letters 15, 60-63.

    Article  Google Scholar 

  • Borom, M.P. (1977). Dispersion-strengthened glass matrices - glass-ceramics, a case in point. Journal of the American Ceramic Society 60, 17-21.

    Article  Google Scholar 

  • Bower, A.F. and Ortiz, M. (1991). A three-dimensional analysis of crack trapping and bridging by tough particles. Journal of Mechanics and Physics of Solids 39, 815-858.

    Article  MATH  Google Scholar 

  • Budiansky, B., Amazigo, J. and Evans, A. (1988). Small-scale crack bridging and the fracture toughness of particulate-reinforced ceramics. Journal of Mechanics and Physics of Solids 36, 167-187.

    Article  Google Scholar 

  • Chaim, R. and Talanker, V. (1995). Microstructure and mechanical properties of SiC platelet/cordierite glass-ceramic composites. Journal of the American Ceramic Society 78, 166-172.

    Article  Google Scholar 

  • Chen, C., Heng, Y. and Chih-Ying, C., (1974). The KI calibration of arc-shaped, edge-cracked 3 point bend specimens. Kexue Tongbao 19, 41-45.

    Google Scholar 

  • Faber, K.T. and Evans, A.G. (1983). Crack deflection processes - I. Theory. Acta Metallurgica 31, 565-576.

    Article  Google Scholar 

  • Gadkaree, K.P. and Chyung, K. (1986). Silicon-carbide-whisker-reinforced glass and glass-ceramic composites. American Ceramic Society Bulletin 65, 370.

    Google Scholar 

  • Green, D.G., Nicholson, P.S. and Embury, J.D. (1979). Fracture of a brittle particulate composite: I. Journal of Materials Science 14, 1413-1420.

    Article  Google Scholar 

  • Green, D.J. (1983). Fracture toughness predictions for crack bowing in brittle particulate composites. Communication to the Journal of the American Ceramic Society 66, C4-C5.

    Google Scholar 

  • Haber, R.A. and Anderson, R.M. (1991). Engineering properties of glass-matrix composites. In Engineering Materials Handbook Vol. 4 'Ceramics and Glasses' (S.J. Schneider ed., ASM International USA), 858-869.

  • Hasselman, D.P.H. and Fulrath, R.M. (1966). Proposed fracture theory of a dispersion-strengthened glass matrix. Journal of the American Ceramic Society 49, 68-72.

    Article  Google Scholar 

  • Himsolt, G., Munz, D. and Fett, T. (1987). Modified chevron specimen for ceramic materials. Journal of the American Ceramic Society 6, C-133-135.

    Google Scholar 

  • Hyde, A.R., Partridge, G. and Vignesoult, S. (1993). Comparison of particulate and platelet reinforcement of a lithium disilicate glass-ceramic. British Ceramic Transactions 92, 55-61.

    Google Scholar 

  • Krstic, V.D. and Khaund, A.K. (1981). Conditions for toughening of particulate brittle composites. In 'Advances in Fracture Research' Vol. 4 (Edited by D. François, Pergamon Press), 1577-1585.

  • Lange, F.F. (1970). The interaction of a crack front with a second-phase dispersion. Philosophical Magazine 22, 983-992.

    Google Scholar 

  • Lange, F.F. (1971). Fracture energy and strength behavior of a sodium borosilicate glass-Al2O3 composite system. Journal of the American Ceramic Society 54, 614-620.

    Article  Google Scholar 

  • Marshall, D.B. and Evans, A.G. (1981). Reply to 'Comment on elastic/plastic indentation damage in ceramics: the median/radial crack system'. Journal of the American Ceramic Society 64, C-182-183.

    Google Scholar 

  • Miyata, N., Ichikawa, S., Monji, H. and Jinno, H. (1985). Fracture behavior of brittle matrix, particulate composites with thermal expansion mismatch. In Fracture Mechanics of Ceramics 7 (Edited by R.C. Bradt, A.G. Evans, D.P.H. Hasselman and F.F. Lange, Plenum Press New-York), 87-102.

    Google Scholar 

  • Munz, D., Bubsey, R.T. and Shannon, J.L. (1980). Fracture toughness determination of Al2O3 using four-point-bend specimens with straight-through and chevron notches. Journal of the American Ceramic Society 63, 300-305.

    Article  Google Scholar 

  • Pezzotti, G. (1993). On the actual contribution of crack deflection in toughening platelet-reinforced brittle-matrix composites. Acta Metallurgica et Materialia 41, 1825-1839.

    Article  Google Scholar 

  • Pezzotti, G., Okamoto, Y., Nishida, T. and Sakai, M. (1996). On the near-tip toughening by crack-face bridging in particulate and platelet-reinforced ceramics. Acta Materialia 44, 899-914.

    Article  Google Scholar 

  • Rouxel, T., Wakai, F., Brito, M.E., Iwamoto, A. and Izaki, K. (1993). Intragranular crack deflection and crystallographic slip in Si3N4/SiC nanocomposites. Journal of the European Ceramic Society 11, 431-438.

    Article  Google Scholar 

  • Rouxel, T., Lavelle, C., Garnier, C., Verdier, P. and Laurent, Y. (1994). Mechanical evaluation of SiC particle reinforced oxynitride glass and glass-ceramic composites. Scripta Metallurgica et Materialia. 31, 15-20.

    Article  Google Scholar 

  • Rouxel, T. and Verdier, P. (1996). SiC particle reinforced oxynitride glass and glass-ceramic composites: crystallization and viscoplastic forming ranges. Acta Materialia 44, 2217-2225

    Article  Google Scholar 

  • Sakai, M. and Inagaki, M. (1989). Dimensionless load-displacement relation and its application to crack propagation problems. Journal of the American Ceramic Society 72, 388-394.

    Article  Google Scholar 

  • Selsing, J. (1961). Internal stresses in ceramics. Journal of the American Ceramic Society 44, 419.

    Article  Google Scholar 

  • Sih, G.C. Handbook of Stress Intensity Factors. Lehigh Univ. Press, Pennsylvania PA.

  • Vekinis, G., Ashby, M.F. and Beaumont, P.W.R. (1990). R-curve behaviour of Al2O3 ceramics. Acta Metallurgica et Materialia 38, 1151-1162.

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Rouxel, T., Laurent, Y. Fracture characteristics of SiC particle reinforced oxynitride glass using chevron-notch three-point bend specimens. International Journal of Fracture 91, 83–101 (1998). https://doi.org/10.1023/A:1007474415485

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1023/A:1007474415485

Navigation