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Journal of Sol-Gel Science and Technology

, Volume 19, Issue 1–3, pp 671–676 | Cite as

Lead Zirconate Titanate Stable Stock Solution: Characterization and Applications

  • Aiying Wu
  • Isabel M. Miranda Salvado
  • Paula M. Vilarinho
  • João L. Baptista
  • Armando J.D. Silvestre
Article

Abstract

Lead zirconate titanate (PZT) thin films were prepared by the sol-gel process using acetic acid and 1,2-propanediol as solvents. Acetone was used as final solvent and in this way a stable stock sol (for more than 12 months) was obtained. The PZT sols prepared were reproducible and suitable for the preparation of PZT thin films. To study the sol structure evolution gas chromatography mass spectrum (GC-MS) and Fourier-transform-infrared (FT-IR) spectra were recorded and analyzed on each step of the synthesis. The rheological behavior and the stability of the stock sol were checked using a rheometer. It is observed that the addition of acetone leads to a very stable stock sol. The preliminary investigation of the electric properties of the obtained PZT thin films showed that the crystallized films deposited from a fresh prepared sol and a 12 months aged sol exhibit similar ferroelectric properties and comparable to those reported in the literature.

PZT thin films precursor chemistry electrical properties 

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Copyright information

© Kluwer Academic Publishers 2000

Authors and Affiliations

  • Aiying Wu
    • 1
  • Isabel M. Miranda Salvado
    • 2
  • Paula M. Vilarinho
    • 2
  • João L. Baptista
    • 2
  • Armando J.D. Silvestre
    • 3
  1. 1.Department of Ceramic and Glass Engineering, UIMCUniversity of AveiroAveiroPortugal
  2. 2.Department of Ceramic and Glass Engineering, UIMCUniversity of AveiroAveiroPortugal
  3. 3.Department of ChemistryUniversity of AveiroAveiroPortugal

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