Abstract
The sensitive, non-destructive constant wavelength (CW) and constant energy (CE) SFS techniques have been used for the simultaneous determination of 1-amino pyrene (AP) and 1-napthyl amine (NA) in their mixtures without prior separation via optimization of different experimental conditions (ΔλCW 70.0 nm, ΔνCE 4000.0 cm−1, scan rate 240.0 nm/min, 25.0 °C, methanol). Amplitude–concentration plots have been linear for 1-amino pyrene, AP (0.01–0.1 mg/L) and 1-napthyl amine, NA (0.1–1.0 mg/L). In aqueous methanolic binary mixtures, the mean recoveries (RSD, LOD and LOQ) of AP were found to be 100.09% (0.053, 0.008 mg/L and 0.034 mg/L) for emission, 100.11% (0.141, 0.008 mg/L, 0.034 mg/L) for CWSFS, 100.05% (0.109, 0.007 mg/L and 0.032 mg/L) for first derivative CWSFS, 100.00% (0.148, 0.007 mg/L and 0.031 mg/L) for CESFS, 99.99% (0.109, 0.008 mg/L and 0.035 mg/L) for first derivative CESFS modes respectively. Additionally, for NA the mean recoveries (RSD, LOD and LOQ) were 100.29% (0.360, 0.046 mg/L and 0.204 mg/L) for emission, 100.06% (0.089, 0.098 mg/L, 0.436 mg/L) for CWSFS, 100.09% (0.144, 0.065 mg/L and 0.288 mg/L) for first derivative CWSFS, 100.05% (0.178, 0.077 mg/L and 0.339 mg/L) for CESFS, 100.03% (0.181, 0.082 mg/L and 0.364 mg/L) for first derivative CESFS modes respectively. Considering their safety and greenness, these methods might be considered as green tools using analytical eco-scale approaches (eco-scale score 88.0).
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Acknowledgements
Financial assistance received from the URS Scholarship, University of Kalyani, DST-PURSE, New Delhi and RUSA grant is gratefully acknowledged. We are thankful to the University of Kalyani for providing infrastructural facilities.
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The funding has been received from University of Kalyani with Grant no. No. 1F-1/URS/ENVS/2019/DP-685, Date: 09.08.2019.
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Mukherjee, S., Dhar, S. Various non-destructive SFS techniques for simultaneous recognition and monitoring of 1-amino pyrene and 1-napthyl amine in the mixture. ANAL. SCI. 39, 1551–1560 (2023). https://doi.org/10.1007/s44211-023-00368-8
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DOI: https://doi.org/10.1007/s44211-023-00368-8