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Novel masonry grout incorporating high volumes of industrial by-products: microstructure characteristics and pursuance of durability properties

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Abstract

One solution to the high cost and scarcity of building materials is to use alternative and sustainable materials. The study presented herein developed an eco-friendly masonry grout using high volumes of palm oil clinker powder to replace cement and palm oil clinker to replace coarse aggregate. Several batches of grouts with different amounts of these materials were made to determine the technical viability of the grout. Scanning Electronic Microscope (SEM), X-Rays Diffraction (XRD), Energy Dispersive X-Ray (EDX) and Thermogravimetric Analyzer (TGA) analyses were conducted to investigate the microstructure characteristics of the grout, and water absorption, initial rate of absorption, sulphate attack and electrical resistivity tests were conducted to determine its durability. Compressive strength tests were conducted at different curing ages and the drying shrinkage of the grout was monitored for 180 days. The results indicate that the new grout is as good as a conventional grout but with added sustainable and economic benefits. The new grout can be used in masonry construction and can be used to alleviate the inadequate supply of affordable housing.

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References

  1. Fonseca FS, Godfrey RC, Siggard K (2015) Compressive strength of masonry grout containing high amounts of class F fly ash and ground granulated blast furnace slag. Constr Build Mater 94:719–727

    Article  Google Scholar 

  2. Pastor JL, Ortega JM, Flor M, López MP, Sánchez I, Climent MA (2016) Microstructure and durability of fly ash cement grouts for micropiles. Constr Build Mater 117:47–57

    Article  Google Scholar 

  3. Shamsuddoha M, Hüsken G, Schmidt W, Kühne H-C, Baeßler M (2018) Ternary mix design of grout material for structural repair using statistical tools. Constr Build Mater 189:170–180

    Article  Google Scholar 

  4. Bras A, Henriques FMA, Cidade MT (2010) Effect of environmental temperature and fly ash addition in hydraulic lime grout behaviour. Constr Build Mater 24(8):1511–1517

    Article  Google Scholar 

  5. Vintzileou E, Miltiadou-Fezans A (2008) Mechanical properties of three-leaf stone masonry grouted with ternary or hydraulic lime-based grouts. Eng Struct 30(8):2265–2276

    Article  Google Scholar 

  6. Vavričuk A, Bokan-Bosiljkov V, Kramar S (2018) The influence of metakaolin on the properties of natural hydraulic lime-based grouts for historic masonry repair. Constr Build Mater 172:706–716

    Article  Google Scholar 

  7. Silva RA, Domínguez-Martínez O, Oliveira DV, Pereira EB (2018) Comparison of the performance of hydraulic lime- and clay-based grouts in the repair of rammed earth. Constr Build Mater 193:384–394

    Article  Google Scholar 

  8. Çınar M, Karpuzcu M, Çanakcı H (2020) The measurement of fresh properties of cement-based grout containing waste marble powder. Measurement 150:106833

    Article  Google Scholar 

  9. Pachta V, Papadopoulos F, Stefanidou M (2019) Development and testing of grouts based on perlite by-products and lime. Constr Build Mater 207:338–344

    Article  Google Scholar 

  10. Nayaka RR, Alengaram UJ, Jumaat MZ, Yusoff SB, Ganasan R (2019) Performance evaluation of masonry grout containing high volume of palm oil industry by-products. J Clean Prod 220:1202–1214

    Article  Google Scholar 

  11. Karim MR, Hashim H, Abdul Razak H (2016) Assessment of pozzolanic activity of palm oil clinker powder. Constr Build Mater 127:335–343

    Article  Google Scholar 

  12. Kanadasan J, Razak HA (2015) Utilization of palm oil clinker as cement replacement material. Materials (Basel) 8(12):8817–8838

    Article  Google Scholar 

  13. Ahmmad R, Jumaat MZ, Alengaram UJ, Bahri S, Rehman MA, bin Hashim H (2016) Performance evaluation of palm oil clinker as coarse aggregate in high strength lightweight concrete. J Clean Prod 112:566–574

    Article  Google Scholar 

  14. Mohammed BS, Al-Ganad MA, Abdullahi M (2011) Analytical and experimental studies on composite slabs utilising palm oil clinker concrete. Constr Build Mater 25(8):3550–3560

    Article  Google Scholar 

  15. Mohammed BS, Foo WL, Hossain KMA, Abdullahi M (2013) Shear strength of palm oil clinker concrete beams. Mater Des 46:270–276

    Article  Google Scholar 

  16. Mohammed BS, Foo WL, Abdullahi M (2014) Flexural strength of palm oil clinker concrete beams. Mater Des 53:325–331

    Article  Google Scholar 

  17. Huda MN, Bin Jumat MZ, Islam ABMS (2016) Flexural performance of reinforced oil palm shell & palm oil clinker concrete (PSCC) beam. Constr Build Mater 127:18–25

    Article  Google Scholar 

  18. Kanadasan J, Razak HA (2014) Mix design for self-compacting palm oil clinker concrete based on particle packing. Mater Des 56:9–19

    Article  Google Scholar 

  19. Abutaha F, Abdul Razak H, Kanadasan J (2016) Effect of palm oil clinker (POC) aggregates on fresh and hardened properties of concrete. Constr Build Mater 112:416–423

    Article  Google Scholar 

  20. Kanadasan J, Razak HA (2015) Utilization of Palm Oil Clinker as Cement Replacement Material. Materials (Basel) 8:8817–8838

    Article  Google Scholar 

  21. Kanadasan J (2016) Feasibility study of palm oil clinker as environmentally friendly self-compacting concrete. University of Malaya

  22. Kanadasan J, Abdul Razak H (2015) Engineering and sustainability performance of self-compacting palm oil mill incinerated waste concrete. J Clean Prod 89:78–86

    Article  Google Scholar 

  23. Kanadasan J, Razak HA, Subramaniam V (2018) Properties of high flowable mortar containing high volume palm oil clinker (POC) fine for eco-friendly construction. J Clean Prod 170:1244–1259

    Article  Google Scholar 

  24. Kanadasan J, Razak HA, Subramaniam V (2018) Properties of high flowable mortar containing high volume palm oil clinker (POC) fine for eco-friendly construction. J Clean Prod 170:1244–1259

    Article  Google Scholar 

  25. Ibrahim HA, Abdul Razak H (2016) Effect of palm oil clinker incorporation on properties of pervious concrete. Constr Build Mater 115:70–77

    Article  Google Scholar 

  26. Ibrahim HA, Abdul Razak H, Abutaha F (2017) Strength and abrasion resistance of palm oil clinker pervious concrete under different curing method. Constr Build Mater 147:576–587

    Article  Google Scholar 

  27. Abutaha F, Razak HA, Ibrahim HA, Ghayeb HH (2018) Adopting particle-packing method to develop high strength palm oil clinker concrete. Resour Conserv Recycl 131:247–258

    Article  Google Scholar 

  28. ASTM C150–14 (2014) Standard Specification for Portland Cement. ASTM International, West Conshohocken

    Google Scholar 

  29. Nayaka RR, Alengaram UJ, Jumaat MZ, Yusoff SB, Alnahhal MF (2018) High volume cement replacement by environmental friendly industrial by-product palm oil clinker powder in cement – lime masonry mortar. J Clean Prod 190:272–284

    Article  Google Scholar 

  30. Tasdemir C (2003) Combined effects of mineral admixtures and curing conditions on the sorptivity coefficient of concrete. Cem Concr Res 33(10):1637–1642

    Article  Google Scholar 

  31. ASTM C618–14 (2014) Standard Specification for Coal Fly Ash and Raw or Calcined Natural Pozzolan for Use in Concrete. ASTM International, West Conshohocken

    Google Scholar 

  32. Rassineux AMF, Petit JC (1989) Ancient analogues of modern cement: calcium hydrosilicates in mortars and concretes from Gallo-Roman thermal baths of Western France. J Am Ceram Soc 72(6):1026–1032

    Article  Google Scholar 

  33. Şahmaran M, Özkan N, Keskin SB, Uzal B, Yaman İÖ, Erdem TK (2008) Evaluation of natural zeolite as a viscosity-modifying agent for cement-based grouts. Cem Concr Res 38(7):930–937

    Article  Google Scholar 

  34. BergHK, Von W (1991) Fresh mortar and concrete with fly ash. aylor Fr 24–41

  35. ASTM C191–14 (2014) Standard Test Methods for Time of Setting of Hydraulic Cement by Vicat Needle. West Conshohocken

  36. ASTM C404 – 14 (2014) Standard Specification for Aggregates for Masonry Grout

  37. ASTM C128 – 2004 (2004) Standard Test Method for Density, Relative Density (Specific Gravity), and Absorption of Fine Aggregate. ASTM International

  38. ASTM C136–14 (2014) Standard Test Method for Sieve Analysis of Fine and Coarse Aggregates. ASTM International, West Conshohocken

    Google Scholar 

  39. ASTM C476 – 14 (2014) Standard Specification for Grout for Masonry. West Conshohocken.

  40. ACI 211.2 – 98 (1998) Standard Practice for Selecting Proportions for Structural Lightweight Concrete New York

  41. ASTM C1019 – 14 (2014) Standard Test Method for Sampling and Testing Grout. West Conshohocken

  42. Hong L, Gu X, Lin F (2014) Influence of aggregate surface roughness on mechanical properties of interface and concrete. Constr Build Mater 65:338–349

    Article  Google Scholar 

  43. Banthia N, Gupta R (2006) Influence of polypropylene fiber geometry on plastic shrinkage cracking in concrete. Cem Concr Res 36(7):1263–1267

    Article  Google Scholar 

  44. Kumar PJMMMP (2015) Concrete: microstructure, properties, and materials, 3rd Edit. McGraw-Hill Publishing, New York

    Google Scholar 

  45. Klemm WA (2005) Cement soundness and the autoclave expansion: test-an update of the literature

  46. Sua-Iam G, Makul N (2014) Utilization of high volumes of unprocessed lignite-coal fly ash and rice husk ash in self-consolidating concrete. J Clean Prod 78:184–194

    Article  Google Scholar 

  47. Karim MR, Hashim H, Abdul Razak H, Yusoff S (2017) Characterization of palm oil clinker powder for utilization in cement-based applications. Constr Build Mater 135:21–29

    Article  Google Scholar 

  48. Alnahhal M, Alengaram MF, Jumaat UJ, Alqedra MZ, Mo MA, Sumesh KH (2017) Evaluation of Industrial By-Products as Sustainable Pozzolanic Materials in Recycled Aggregate Concrete. Sustainability 9(5):767

    Article  Google Scholar 

  49. Choi YW, Kim YJ, Shin HC, Moon HY (2006) An experimental research on the fluidity and mechanical properties of high-strength lightweight self-compacting concrete. Cem Concr Res 36(9):1595–1602

    Article  Google Scholar 

  50. Jegathish K (2016) Feasibility study of palm oil clinker as environmentally friendly self-compacting concrete/Jegathish Kanadasan. Doctoral dissertation, University of Malaya

  51. Heikal M, Zohdy KM, Abdelkreem M (2013) Mechanical, microstructure and rheological characteristics of high performance self-compacting cement pastes and concrete containing ground clay bricks. Constr Build Mater 38:101–109

    Article  Google Scholar 

  52. Malhotra VM (1976) Testing hardened concrete: nondestructive methods. CRC Press

  53. Lynn CJ, Dhir OBE RK, Ghataora GS (2016) Municipal incinerated bottom ash characteristics and potential for use as aggregate in concrete. Constr Build Mater 127:504–517

    Article  Google Scholar 

  54. Topçu İB, Uygunoğlu T (2010) Effect of aggregate type on properties of hardened self-consolidating lightweight concrete (SCLC). Constr Build Mater 24(7):1286–1295

    Article  Google Scholar 

  55. Neville AM (1995) Properties of concrete, 4th edn. Longman, London

    Google Scholar 

  56. Dogan UA, Ozkul MH (2015) The effect of cement type on long-term transport properties of self-compacting concretes. Constr Build Mater 96:641–647

    Article  Google Scholar 

  57. Corinaldesi V, Moriconi G (2009) Behaviour of cementitious mortars containing different kinds of recycled aggregate. Constr Build Mater 23(1):289–294

    Article  Google Scholar 

  58. Al-Amoudi OSB (1995) Performance of 15 reinforced concrete mixtures in magnesium-sodium sulphate environments. Constr Build Mater 9(3):149–158

    Article  Google Scholar 

  59. T AASHTO (2011) Standard Method of Test for Surface Resistivity Indication of Concrete’s Ability to Resist Chloride Ion Penetration. In AASHTO Provisional Standards, 2011 Edition

  60. Kanadasan J, Abdul Razak H (2015) Engineering and sustainability performance of self-compacting palm oil mill incinerated waste concrete. J Clean Prod 89:78–86

    Article  Google Scholar 

  61. Naganathan S, Razak HA, Hamid SNA (2013) Corrosivity and leaching behavior of controlled low-strength material (CLSM) made using bottom ash and quarry dust. J Environ Manage 128:637–641

    Article  Google Scholar 

  62. Dhir KAPRK, Dyer TD, Halliday JE (2002) Value added recycling of incinerator ashes,” DETR Research Contract No 39/3/476 CC 1683

  63. van der Wegen J, Hofstra G, Speerstra U (2013) Upgraded MSWI bottom ash as aggregate in concrete. Waste Biomass Valoriz 4(4):737–743

    Article  Google Scholar 

  64. A. C596–01 (2001) Standard Test Method for Drying Shrinkage of Mortar Containing Hydraulic Cement

  65. Nayaka, R. R., Alengaram, U. J., Jumaat, M. Z., & Yusoff, S. B. (2018). Microstructural investigation and durability performance of high volume industrial by-products-based masonry mortars. Construction and Building Materials189, 906-923.

  66. Nayaka, R. R., Alengaram, U. J., Jumaat, M. Z., Fonseca, F. S., & Banerjee, A. (2021). Structural performance of masonry prisms, wallettes and walls containing high volume of industrial by-products–Sustainable housing perspective. Construction and Building Materials303, 124439.

  67. Nayaka, R. R., Alengaram, U. J., Jumaat, M. Z., Yusoff, S., & Ganasan, R. (2021). Performance Evaluation of Engineering Properties, Radiation Shielding, and Sustainability of Hollow Masonry Blocks Produced Using a High Volume of Industrial By-Products. Journal of Materials in Civil Engineering33(3), 04021003.

  68. Sumesh, M., Alengaram, U. J., Jumaat, M. Z., Mo, K. H., Singh, R., Nayaka, R. R., & Srinivas, K. (2021). Chemo-physico-mechanical characteristics of high-strength alkali-activated mortar containing non-traditional supplementary cementitious materials. Journal of Building Engineering, 103368.

  69. Alnahhal, M. F., Alengaram, U. J., Jumaat, M. Z., Abutaha, F., Alqedra, M. A., & Nayaka, R. R. (2018). Assessment on engineering properties and CO2 emissions of recycled aggregate concrete incorporating waste products as supplements to Portland cement. Journal of cleaner production203, 822-835.

  70. Nayaka, R. R., Alengaram, U. J., Jumaat, M. Z., Yusoff, S. B., & Sumesh, M. (2018, October). Influence of palm oil clinker powder on the fresh and mechanical properties of masonry mortars. In IOP Conference Series: Materials Science and Engineering (Vol. 431, No. 8, p. 082002). IOP Publishing.

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Acknowledgements

The research funds Science and Engineering Research Board (SERB) “EEQ/2020/000499- Innovative Development of Sustainable White clay and Graphene Composite Ventilation Wall Cladding Tiles to Curtail the Heat Ingress” Science and Engineering Research Board (SERB), NIT Warangal, Government of India and University of Malaya, Malaysia Faculty Grant bearing project grant number- GPF050A-2020 to conduct this research work are acknowledged.

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Correspondence to R. Ramesh Nayaka.

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Nayaka, R.R., Alengaram, U.J., Pancharathi, R.K. et al. Novel masonry grout incorporating high volumes of industrial by-products: microstructure characteristics and pursuance of durability properties. Archit. Struct. Constr. 1, 125–142 (2021). https://doi.org/10.1007/s44150-021-00012-x

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