Skip to main content
SpringerLink
Log in

Control of particle morphology and size of yttria powder prepared by hydro(solvo)thermal synthesis

  • Original Article
  • Published:
Journal of the Korean Ceramic Society Aims and scope Submit manuscript

Abstract

Yttria (Y2O3) is a representative material having excellent plasma resistance, and yttria powder, applied to semiconductor components and thermal spray coating, requires excellent sinterability and flowability, for which particle shape and size are important factors. In the present study, to synthesize yttria powder having various shape applicable to many industrial areas, the morphology of yttria particles was controlled through hydro(solvo)thermal synthesis. The yttria powder was synthesized using deionized water, ethylene glycol and glycerol as solvents. The precursor concentrations and the synthesis conditions such as synthesis temperature and time were examined. The particle shape and size of the yttria powder were adjusted to plate-type, rod-type and spherical-type depending on the applied solvent, precipitant and synthesis temperature. The thermal treatment following the hydro(solvo)thermal synthesis did not have a significant effect on the shape of the yttria particles. Cubic single-phase yttria was observed at a calcination temperature of 450 °C or higher, and the crystal phase further developed as the thermal treatment temperature increased. In the powder synthesized using deionized water, the crystal phase developed mostly on the [222] direction depending on the temperature during oriented attachment. On the other hand, in the powder synthesized using ethylene glycol and glycerol as a solvent, the crystal phase developed homogeneously in all crystalline directions.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13

Similar content being viewed by others

References

  1. J.H. Pee, J.C. Park, K.T. Hwang, S.R. Kim, W.S. Cho, Res. Chem. Intermed. 36, 801 (2010). https://doi.org/10.1007/s11164-010-0184-8

    Article  CAS  Google Scholar 

  2. J.H. Lee, S.H. Bea, Korean. J. Mater. Res. 27(8), 445 (2017). https://doi.org/10.3740/MRSK.2017.27.8.445

    Article  CAS  Google Scholar 

  3. H.W. Lee, H.I. JI, J.H. Lee, B.K. Kim, K.J. Yoon, J.W. Son, J. Korean Ceram. Soc. 56(2), 130 (2019). https://doi.org/10.4191/kcers.2019.56.2.04

    Article  CAS  Google Scholar 

  4. S.K. Rha, M.J. Lee, Y.S. Lee, J. Korean Ceram. Soc. 57, 338 (2020). https://doi.org/10.1007/s43207-020-00034-z

    Article  CAS  Google Scholar 

  5. W.K. Jung, H.J. Ma, S.W. Jung, D.K. Kim, J. Am. Ceram. Soc. 100, 1876 (2017). https://doi.org/10.1111/jace.14776

    Article  CAS  Google Scholar 

  6. W. Liu, L. Jin, S. Wang, Mater. Chem. Phys. 232, 471 (2019). https://doi.org/10.1016/j.matchemphys.2019.05.018

    Article  CAS  Google Scholar 

  7. X. Wang, Y. Hu, X. Meng, Y. Li, M. Zhu, H. Jin, J. Rare Earths 33(7), 706 (2015). https://doi.org/10.1016/S1002-0721(14)60474-9

    Article  CAS  Google Scholar 

  8. B.V. Hao, P.T. Huy, T.N. Khiem, N.T.T. Ngan, P.H. Duong, J. Phys. Conf. Ser. 187, 012074 (2009). https://doi.org/10.1088/1742-6596/187/1/012074

    Article  CAS  Google Scholar 

  9. D. Nunes, A. Pimentel, L. Santos, P. Barquinha, L. Pereira, E. Fortunato, R. Martins, Metal oxide nanostructures synthesis, properties and applications (Elsevier, Chisinau, 2019), pp. 37–39

    Google Scholar 

  10. M.G. Siahroudi, A.A. Daryakenari, Y.B. Molamahaleh, Q. Cao, M.A. Darayakenari, J.J. Delaunay, H. Siavoshi, F. Molaei, Int. J. Hydrogen Energy 45(55), 30357 (2020). https://doi.org/10.1016/j.ijhydene.2020.08.007

    Article  CAS  Google Scholar 

  11. V. Maheskumar, T. Selvaraju, B. Vidhya, Int. J. Hydrogen Energy 43(51), 22861 (2018). https://doi.org/10.1016/j.ijhydene.2018.09.072

    Article  CAS  Google Scholar 

  12. X. Li, Q. Li, J. Wang, J. Li, J. Lumin. 124(2), 351 (2007). https://doi.org/10.1016/j.jlumin.2006.04.007

    Article  CAS  Google Scholar 

  13. Towata, M. Sivakumar, K. Yasui, T. Tuziuti, T. Kozuka, Y. Iida (2008) J. Mater. Sci. 43:1214. https://doi.org/10.1007/s10853-007-2287-1

  14. Q. Tang, Z. Liu, S. Li, S. Zhanga, X. Liu, Y. Qian, J. Cryst. Growth 259(1–2), 208 (2003). https://doi.org/10.1016/S0022-0248(03)01590-2

    Article  CAS  Google Scholar 

  15. Z. Liu, B. Wu, D. Xiang, Y. Zhu, Mater. Res. Bull. 47(11), 3753 (2012). https://doi.org/10.1016/j.materresbull.2012.06.026

    Article  CAS  Google Scholar 

  16. M.W. Shafer, R. Roy, J. Am. Ceram. Soc. 42(11), 563 (1959). https://doi.org/10.1111/j.1151-2916.1959.tb13574.x

    Article  CAS  Google Scholar 

  17. H. Xian, J. Zhu, H. Tang, X. Liang, H. He, Y. Xi, CrystEngComm 18, 8823 (2016). https://doi.org/10.1039/C6CE01692H

    Article  CAS  Google Scholar 

  18. T. Liu, Z. Jin, J. Li, J. Wang, D. Wang, J. Lai, H. Du, CrystEngComm 15, 8903 (2013). https://doi.org/10.1039/C3CE41500G

    Article  CAS  Google Scholar 

  19. R.L. Penn, J.F. Banfield, Am. Assoc. Adv. Sci. 281(5379), 969 (1998). https://doi.org/10.1126/science.281.5379.969

    Article  CAS  Google Scholar 

  20. R.L. Penn, J.F. Banfield, Am. Mineral. 83(9–10), 1077 (1998). https://doi.org/10.2138/am-1998-9-1016

    Article  CAS  Google Scholar 

  21. R.L. Penn, J.F. Banfield, Geochim. Cosmochim. Acta 63, 1549 (1999). https://doi.org/10.1016/S0016-7037(99)00037-X

    Article  CAS  Google Scholar 

  22. J.A. Soltis, R.L. Penn, in Iron Oxides: From Nature to Applications, ed. By D. Faivre, R. B. Frankel (Wiley, New York, 2016), pp. 243–268. https://doi.org/10.1002/9783527691395.ch11

  23. W. He, K. Wen, Y. Niu, Nanocrystals from Oriented-Attachment for Energy Applications, (Springer, New York, 2018), pp. 1–13. https://doi.org/10.1007/978-3-319-72432-4

  24. X. Peng, L. Manna, W. Yang, J. Wickham, E. Scher, A. Kadavanich, A.P. Alivisatos, Nature 404, 59 (2000). https://doi.org/10.1038/35003535

    Article  CAS  Google Scholar 

  25. A.L. Patterson, Phys. Rev. 56, 978 (1939). https://doi.org/10.1103/PhysRev.56.978

    Article  CAS  Google Scholar 

  26. K. Nakashima, Y. Toshima, Y. Kobayashi, Y. Ishikawa, M. Kakihana, J. Asian. Ceram. Soc. 7(4), 544 (2019). https://doi.org/10.1080/21870764.2019.1683955

    Article  Google Scholar 

  27. J. Wu, X. Lü, L. Zhang, F. Huang, F. Xu, Eur. J. Inorg. Chem. 2009(19), 2789 (2009). https://doi.org/10.1002/ejic.200900199

    Article  CAS  Google Scholar 

Download references

Acknowledgements

This Research was supported by Research Funds of Mokpo National University in 2021.

Author information

Authors and Affiliations

  1. Department of Advanced Materials Science and Engineering, Mokpo National University, Muan, 58554, Republic of Korea

    Bok-Hyun Oh & Sang-Jin Lee

  2. Research Institute of Ceramic Industry and Technology, Mokpo National University, Muan, 58554, Republic of Korea

    Sang-Jin Lee

Authors
  1. Bok-Hyun Oh
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Sang-Jin Lee
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Sang-Jin Lee.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Oh, BH., Lee, SJ. Control of particle morphology and size of yttria powder prepared by hydro(solvo)thermal synthesis. J. Korean Ceram. Soc. 59, 436–443 (2022). https://doi.org/10.1007/s43207-022-00186-0

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s43207-022-00186-0

Keywords

Search

Navigation