Abstract
The aim of this study is to identify improvements in the physical and rheological properties of asphalt binders when alumina microfibers are added in the role of modifiers. Modified asphalt binder composites were prepared using three different alumina microfiber percentages (0.05, 0.1 and 0.2%) by volume on PG70-10 standard asphalt binder grade. The performance properties of the materials were evaluated against standard performance measurements such as penetration, ductility, flash, fire and softening points along with Superpave test protocol. The results of the investigation demonstrated that the use of improved characterization methods is advantageous in assessing modified asphalt binder performance. One such method used is Scanning Electron Microscopy (SEM) imaging. Other methods that would help better characterize cracking and rutting resistance included the following: Multiple Stress Creep Recovery (MSCR) test, Glover-Rowe (G-R) parameter and delta Tc (∆Tc) parameter. The results of the MSCR test clarified the inconsistencies between the physical and rheological properties. The percent recovery (R) and the non-recoverable creep compliance (Jnr) changes with the addition of alumina microfiber caused an improvement in the asphalt binder’s rutting resistance while maintaining an acceptable fatigue cracking performance. Based on ΔTc and G-R parameters, it was found that the incorporation of alumina microfiber increased the asphalt binder’s ability to withstand additional aging without showing signs of cracking. As per fatigue cracking and thermal cracking routines, the optimum content of alumina microfiber was determined to be 0.1% for best performance against cracking as well as rutting. In addition, it was revealed statistically that alumina microfiber had a meaningful capability to improve physical and rheological properties of asphalt binders.
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig1_HTML.jpg)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig2_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig3_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig4_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig5_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig6_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig7_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig8_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig9_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig10_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig11_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs42947-021-00008-2/MediaObjects/42947_2021_8_Fig12_HTML.png)
Similar content being viewed by others
References
Chaturabong, P., & Bahia, H. U. (2018). Effect of moisture on the cohesion of asphalt mastics and bonding with surface of aggregates. Road Materials and Pavement Design, 19(3), 741–753
Masad, E., Roja, K. L., Rehman, A., & Abdala, A. (2020). A review of asphalt modification using plastics: a focus on polyethylene. TAMU Report. https://doi.org/10.13140/RG.2.2.36633.77920
Wang, D., Wang, L., Gu, X., & Zhou, G. (2013). Effect of basalt fiber on the asphalt binder and mastic at low temperature. Journal of materials in civil engineering, 25(3), 355–364
Wu, M. M., Li, R., Zhang, Y. Z., Fan, L., Lv, Y. C., & Wei, J. M. (2015). Stabilizing and reinforcing effects of different fibers on asphalt mortar performance. Petroleum Science, 12(1), 189–196
Wu, S., & Tahri, O. (2021). State-of-art carbon and graphene family nanomaterials for asphalt modification. Road Materials and Pavement Design, 22(4), 735–756
Chen, C., Podolsky, J. H., Williams, R. C., & Cochran, E. W. (2019). Determination of the optimum polystyrene parameters using asphalt binder modified with poly (styrene-acrylated epoxidised soybean oil) through response surface modelling. Road Materials and Pavement Design, 20(3), 572–591
Qing, Z., Qi-Cheng, L., Peng, L., Chuan-Sheng, C., & Jiang-Rong, K. (2020). Study on modification mechanism of nano-ZnO/polymerised styrene butadiene composite-modified asphalt using density functional theory. Road Materials and Pavement Design, 21(5), 1426–1438
Chen, C., Podolsky, J. H., Williams, R. C., & Cochran, E. W. (2020). Rheological properties and effects of aging on acrylated epoxidised soybean oil monomer-modified asphalt binder. Road Materials and Pavement Design, 21(2), 347–373
Azahar, N. M., Hassan, N. A., Jaya, R. P., Hainin, M. R., Yusoff, N. I. M., Kamaruddin, N. H. M., & Yaacob, H. (2019). Properties of cup lump rubber modified asphalt binder. Road Materials and Pavement Design, 1–21
Arabani, M., Mirabdolazimi, S. M., & Sasani, A. R. (2010). The effect of waste tire thread mesh on the dynamic behaviour of asphalt mixtures. Construction and Building Materials, 24(6), 1060–1068
Zare-Shahabadi, A., Shokuhfar, A., & Ebrahimi-Nejad, S. (2010). Preparation and rheological characterization of asphalt binders reinforced with layered silicate nanoparticles. Construction and Building Materials, 24(7), 1239–1244
Hamedi, G. H. (2017). Evaluating the effect of asphalt binder modification using nanomaterials on the moisture damage of hot mix asphalt. Road Materials and Pavement Design, 18(6), 1375–1394
Wan, J., Wu, S., Xiao, Y., Liu, Q., & Schlangen, E. (2016). Characteristics of ceramic fiber modified asphalt mortar. Materials, 9(9), 788
Aburkaba, E., & Muniandy, R. (2016). Experimental Study of High Temperature Properties and Rheological Behavior of Ceramic Modified Asphalt. Australian Journal of Basic and Applied Sciences, 10(6)
Arabani, M., & Shabani, A. (2019). Evaluation of the ceramic fiber modified asphalt binder. Construction and Building Materials, 205, 377–386
Eisa, M. S., Basiouny, M. E., & Daloob, M. I. (2021). Effect of adding glass fiber on the properties of asphalt mix. International Journal of Pavement Research and Technology, 14, 403–409. https://doi.org/10.1007/s42947-020-0072-6
Javani, M., Kashi, E., & Mohamadi, S. (2019). Effect of polypropylene fibers and recycled glass on AC mixtures mechanical properties. International Journal of Pavement Research and Technology, 12, 464–471. https://doi.org/10.1007/s42947-019-0056-6
Kar, S. S., Nagabhushana, M. N., & Jain, P. K. (2019). Performance of hot bituminous mixes admixed with blended synthetic fibers. International Journal of Pavement Research and Technology, 12, 370–379. https://doi.org/10.1007/s42947-019-0044-x
Bhat, F. S., & Mir, M. S. (2021). Rheological investigation of asphalt binder modified with nanosilica. International Journal of Pavement Research and Technology, 14, 276–287. https://doi.org/10.1007/s42947-020-0327-2
Mahali, I., & Sahoo, U. C. (2019). Rheological characterization of Nanocomposite modified asphalt binder. International Journal of Pavement Research and Technology, 12, 589–594. https://doi.org/10.1007/s42947-019-0070-8
Khasawneh, M. A., & Alyaseen, S. K. (2020). Analytic methods to evaluate bituminous mixtures enhanced with coir/coconut fiber of highway materials. Materials Today: Proceedings, 33, 1752–1757. https://doi.org/10.1016/j.matpr.2020.04.870
Khasawneh, M. A., Taamneh, M., Al-Omari, A. A., Harahsheh, T., & Al-Hosainat, A. (2019). Experimental and statistical evaluation of asphalt binders produced in jordan treated with different modifiers. Journal of Materials in Civil Engineering, American Society of Civil Engineers (ASCE). https://doi.org/10.1061/(ASCE)MT.1943-5533.0003003
Al-Omari, A. A., Khasawneh, M. A., Al-Rousan, T. M., & Al-Theeb, S. F. (2019). Static creep of modified superpave asphalt concrete mixtures using crumb tire rubber, microcrystalline synthetic wax, and nanosilica. International Journal of Pavement Engineering, 1–12.
Khasawneh, M. A., Taamneh, M. M., & Albatayneh, O. (2019). Evaluation of static creep of FORTA-FI strengthened asphalt mixtures using experimental, statistical and feed-forward back-propagation ANN techniques. International Journal of Pavement Research and Technology, 12(1), 43–53
Al-Omari, A., Taamneh, M., Khasawneh, M. A., & Al-Hosainat, A. (2020). Effect of crumb tire rubber, microcrystalline synthetic wax, and nano silica on asphalt rheology. Road Materials and Pavement Design, 21(3), 757–779
Al-Omari, A. A., Khedaywi, T. S., & Khasawneh, M. A. (2018). Laboratory characterization of asphalt binders modified with waste vegetable oil using SuperPave specifications. International Journal of Pavement Research and Technology, 11(1), 68–76
American Association of State Highway and Transportation Officials. (2019) Multiple Stress Creep Recovery (MSCR) Test of Asphalt Binder Using a Dynamic Shear Rheometer (DSR), AASHTO designation: T350.
American Association of State Highway and Transportation Officials. (2013) Standard specification for performance- graded asphalt binder, AASHTO designation: MP 19.
Anderson, R. M., King, G. N., Hanson, D. I., & Blankenship, P. B. (2011). Evaluation of the relationship between asphalt binder properties and non-load related cracking. Journal of the Association of Asphalt Paving Technologists, 80.
Rowe, G. M. (2011). Prepared Discussion following the Anderson AAPT paper cited previously. In AAPT (Vol. 80, pp. 649–662).
Glover, C. J., Davison, R. R., Domke, C. H., Ruan, Y., Juristyarini, P., Knorr, D. B., & Jung, S. H. (2005). Development of a new method for assessing asphalt binder durability with field validation. Texas Dept Transport, 1872, 1–334.
ASTM D5, D5M-13. (2013). Standard test method for penetration of bituminous materials. West Conshohocken, PA: ASTM International.
ASTM D36, D36M-14e1. (2014). Standard test method for softening point of bitumen (ring-and-ball apparatus). West Conshohocken, PA: ASTM International.
ASTM D92–16b. (2016). Standard test method for flash and fire points by cleveland open cup tester. West Conshohocken, PA: ASTM International.
ASTM D113–07. (2007). Standard test method for ductility of bituminous materials (Withdrawn 2016). West Conshohocken, PA: ASTM International.
ASTM D4402, D4402M-15. (2015). Standard test method for viscosity determination of asphalt at elevated temperatures using a rotational viscometer. West Conshohocken, PA: ASTM International.
ASTM D7175–15. (2015). Standard test method for determining the rheological properties of asphalt binder using a dynamic shear rheometer. West Conshohocken, PA: ASTM International.
ASTM D6648–08. (2016). Standard test method for determining the flexural creep stiffness of asphalt binder using the Bending beam rheometer (BBR). West Conshohocken, PA: ASTM International.
Bahia, H. U., & Anderson, D. A. (1995). Strategic highway research program binder rheological parameters: background and comparison with conventional properties. Transportation research record, (1488).
Anderson, D. A., & Kennedy, T. W. (1993). Development of SHRP binder specification (with discussion). Journal of the Association of Asphalt Paving Technologists, 62.
Al-Malak, B. (2019). Assessing the Use of Alumina Microfibers to Enhance Physical and Rheological Properties of Asphalt Binders. Master Thesis. Jordan University of Science and Technology.
Bennert, T., Pezeshki, D., Shaarbafan, N., & Euler, C. (2016). Warm-mix asphalt trials in New York State: Laboratory and field performance. Transportation Research Record: Journal of the Transportation Research Board, 2575, 175–186
Acknowledgements
This work was funded by the deanship of scientific research at Jordan University of Science and Technology (Grant No. 121/2018) and laboratory work was conducted in the highway laboratory at Jordan University of Science and Technology. Authors greatly appreciate this financial support and the help of all technicians.
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
Conflict of Interest
Authors declare that there is no conflict of interest.
Supplementary Information
Below is the link to the electronic supplementary material.
Rights and permissions
About this article
Cite this article
Khasawneh, M.A., Al-Jarrah, M.T. & Al-Malak, B.A.M. Assessing the Use of Alumina Microfibers as Modifiers to Enhance the Physical and Rheological Properties of Asphalt Binders. Int. J. Pavement Res. Technol. 15, 284–302 (2022). https://doi.org/10.1007/s42947-021-00008-2
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s42947-021-00008-2