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Caesalpinia Crista (Kanchaki) as Green Corrosion Inhibitor for Zinc in Hydrochloric Acid Solutions

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Abstract

A study aims to inspect the surface adsorption of Caesalpinia Crista seed (Kanchaki seed) extract as a developing anti-corrosion additive for zinc in acidizing solutions. The study utilizes various experimental approaches like the mass loss, electrochemical impedance spectroscopy (EIS), and potentio-dynamic polarization (PDP). The study achieves high inhibition efficiencies of 99.4%, 85.0%, and 94.8% in mass loss, potentiodynamic studies, and EIS, respectively at a higher concentration (2.0 g/L) of KSE and a temperature of 303 K. Impedance analyses revealed an increase in charge transfer at the zinc-solution interface upon the addition of the KSE. PDP measurements indicated a significant reduction in corrosion current density when using Kanchaki seed extract (KSE), suggesting its role as a mixed-type corrosion inhibitor. The adsorption of the KSE on the zinc substrate followed the Langmuir isotherm, involving a physical adsorption mechanism. Surface analysis, conducted through contact angle and scanning electron microscopy - energy dispersive X-ray (SEM-EDX) and atomic force microscopy (AFM) measurements, provided additional support for the adsorption of the inhibitor on the zinc substrate. Fourier transform infrared spectroscopy (FT-IR) was utilized to calculate the KSE’s functional groups. The experimental outcomes obtained from all the applied approaches show good agreement.

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Acknowledgements

The authors appreciate the lab and library resources provided by the Arts Science and Commerce College’s Chemistry Department in Kholwad, Surat, India.

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Authors and Affiliations

  1. Department of Chemistry, Department of Chemistry, Arts, Science and Commerce College, Kholwad, Kamrej Char Rasta. Dist., Surat, Gujarat, 394185, India

    P. S. Desai

  2. Shri J. S. Bhakta and Shri K. M. Bhakta Arts, Shri A. N. Shah Science and Shri N. F. Shah Commerce College, Kholwad, Kamrej Char Rasta, Surat, Gujarat, 394185, India

    Bhumika B. Parmar

  3. Shri M. R. Desai Arts and EELK Commerce College, Chikhli Dist., Navsari, Gujarat, 396521, India

    F. P. Desai

  4. Department of Chemistry, Sir P. T. Sarvajanik College of Science, Surat, Gujarat, India

    Adarsh M. Patel

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Desai, P.S., Parmar, B.B., Desai, F.P. et al. Caesalpinia Crista (Kanchaki) as Green Corrosion Inhibitor for Zinc in Hydrochloric Acid Solutions. Chemistry Africa 7, 2173–2187 (2024). https://doi.org/10.1007/s42250-023-00874-2

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