Abstract
Three resin cements, RelyX™ Ultimate, Panavia F2.0 and RelyX™ U200, were evaluated for their bond strengths between a mica glass-ceramic and human dentin. This research shows that a self-etch dental cement resin system, Panavia F2.0 provided the best bond strength. The glass-ceramic was produced and phases analysed. Biaxial flexural strength and hardness were measured and found to be comparable to that of human enamel and dentin. Bond strength was measured before and after thermocycling. Thermocycling was found to reduce the bond strength. Thermocycling reduced the shear bond strengths of all adhesives by 50–60%. The two-way ANOVA test was used to analyse the data (p = 0.05). Failure modes were analysed, showing failure predominately at the cement/glass-ceramic and dentin/resin cement interfaces. Failure modes changed after thermocycling. The resin cement bond between the dentin and mica glass-ceramics interfaces was examined for failure by optical microscopy (OM) and scanning electron microscopy (SEM).
This is a preview of subscription content, access via your institution.







References
Richard, V.N.: All-ceramic restorative: high-strength core ceramics. In: Alison, T., Fiona, C. (eds.) Introduction to dental materials, pp. 205–208. Mosby, Elsevier Inc., London (2013)
Rosenblum, M.A., Schulman, A.: A review of all-ceramic restorations. J. Am. Dent. Assoc. 128(3), 297–307 (1997). https://doi.org/10.14219/jada.archive.1997.0193
Stephen, R., Martin, L., Junhei, F.: Tooth preparation for all-ceramic restorations. In: John, D., Courtney, S. (eds.) Contemporary fixed prosthodontics, pp. 262–271. Mosby, Elsevier Inc., China (2006)
Ozer, A., Soygun, K., Bolayir, G.: The surface and phase analysis studies on dental bioceramics subjected to different mouthrinse solutions. J Aust Ceram Soc. (2018). https://doi.org/10.1007/s41779-018-0174-7
El-Meliegy, E., Noort, R.V.: Machinable Mica dental glass-ceramics. In: El-Meliegy, E., Noort, R.V. (eds.) Glasses and glass ceramics for medical applications, pp. 193–208. Springer, New York (2012)
Bai, J., Chaysuwan, D.: Nucleation, crystallization and characterization of mica-based glass-ceramics with fluorapatite. Adv Mater Res. 936, 164–169 (2014)
Bai, J., Chaysuwan, D.: Development of mica-based glass-ceramic with 4 Mol% of fluorapatite. Adv Mater Res. 1077, 8–13 (2015)
Chaysuwan, D., Sirinukunwattana, K., Kanchanatawewat, K., Heness, G., Yamashita, K.: Machinable glass-ceramics forming as a restorative dental material. Dent Mater J. 30(3), 358–367 (2011)
Srichumpong, T., Suputtamongkol, K., Chinpanuwat, W., Nampachoke, P., Bai, J., Angkulpipat, S., Prasertwong, S., Chaysuwan, D.: Effect of heat treatment time on properties of mica-based glass-ceramics for restorative dental materials. Key Eng Mater. 702, 23–27 (2016)
Wei, W., Yong, L., Tan, Y., Grover, L., Guo, Y., Bowei, L.: A mica/nepheline glass-ceramic prepared by melting and powder metallurgy at low temperatures. Mater. Today Commun. 11(Supplement C), 87–93 (2017). https://doi.org/10.1016/j.mtcomm.2017.02.007
ISO 6872:2015. Dentistry—ceramic materials. Geneva, Switzerland: International Organization for Standardization. (2015)
ASTM C1327-08. Standard test method for Vickers indentation hardness of advanced ceramics. West Conshohocken, PA: American Society for Testing and Materials. (2008)
Kim, B.-K., Bae, H.E.-K., Shim, J.-S., Lee, K.-W.: The influence of ceramic surface treatments on the tensile bond strength of composite resin to all-ceramic coping materials. J Prosthet Dent. 94(4), 357–362 (2005). https://doi.org/10.1016/j.prosdent.2005.08.012
Nagayassu, M.P., Shintome, L.K., Uemura, E.S., Araujo, J.E.: Effect of surface treatment on the shear bond strength of a resin-based cement to porcelain. Braz Dent J. 17(4), 290–295 (2006)
Holderegger, C., Sailer, I., Schuhmacher, C., Schlapfer, R., Hammerle, C., Fischer, J.: Shear bond strength of resin cements to human dentin. Dent Mater. 24(7), 944–950 (2008). https://doi.org/10.1016/j.dental.2007.11.021
Altintas, S., Eldeniz, A.U., Usumez, A.: Shear bond strength of four resin cements used to lute ceramic core material to human dentin. J Prosthodont. 17(8), 634–640 (2008). https://doi.org/10.1111/j.1532-849X.2008.00348.x
Kumbuloglu, O., Lassila, L.V., User, A., Toksavul, S., Vallittu, P.K.: Shear bond strength of composite resin cements to lithium disilicate ceramics. J Oral Rehabil. 32(2), 128–133 (2005). https://doi.org/10.1111/j.1365-2842.2004.01400.x
Kanchanavasita, W., Rungnava, P., Mat-Ran, S.: Microtensile bond strength between a lithium disilicateglass-ceramic or a Y-TZP zirconia ceramic bonded to dentin when using two self-etch, self-adhesive resin cements compared with an adhesive resin cement. Mahidol. Dent. J. 33(2), 65–72 (2013)
Denry, I.L., Holloway, J.A., Nakkula, R.J., Walters, J.D.: Effect of niobium content on the microstructure and thermal properties of fluorapatite glass-ceramics. J. Biomed. Mater. Res. B. Appl. Biomater. 75(1), 18–24 (2005). https://doi.org/10.1002/jbm.b.30295
Chun, K.J., Choi, H.H., Lee, J.Y.: Comparison of mechanical property and role between enamel and dentin in the human teeth. J Dent Biomech. 5, 1–5 (2014). https://doi.org/10.1177/1758736014520809
Chen, H., Liu, Y.: Chapter 2 - teeth. In: James, Z.S., Tomaž, K. (eds.) Advanced ceramics for dentistry, pp. 5–21. Butterworth-Heinemann, Oxford (2014)
Carvalho, A.O., Ayres, A.P., de Almeida, L.C., Briso, A.L., Rueggeberg, F.A., Giannini, M.: Effect of peroxide bleaching on the biaxial flexural strength and modulus of bovine dentin. Eur. J. Dent. 9(2), 246–250 (2015). https://doi.org/10.4103/1305-7456.156845
Blatz, M.B., Sadan, A., Arch, G.H., Lang, B.R.: In vitro evaluation of long-term bonding of Procera AllCeram alumina restorations with a modified resin luting agent. J Prosthet Dent. 89(4), 381–387 (2003). https://doi.org/10.1067/mpr.2003.89
Ozcan, M., Kerkdijk, S., Valandro, L.F.: Comparison of resin cement adhesion to Y-TZP ceramic following manufacturers’ instructions of the cements only. Clin Oral Investig. 12(3), 279–282 (2008). https://doi.org/10.1007/s00784-007-0151-y
Özcan, M., Mese, A.: Adhesion of conventional and simplified resin-based luting cements to superficial and deep dentin. Clin Oral Investig. 16(4), 1081–1088 (2012). https://doi.org/10.1007/s00784-011-0594-z
Gürol, O., Funda, Y., Dilek, T., Nuran, O., Mustafa, O.: Shear bond strength of composite resin cements to ceramics. J. Marmara Univ. Dent. Fac. 2, 61–66 (2013)
Sirimongkolwattana, S., Phanpaisan, P., Jittidecharaks, S., Tagami, J.: Bond strength between self-adhesive cement and dentin using self-etch bonding. CM Dent. J. 36(2), 81–88 (2015)
Lee, S.-E., Bae, J.-H., Choi, J.-W., Jeon, Y.-C., Jeong, C.-M., Yoon, M.-J., Huh, J.-B.: Comparative shear-bond strength of six dental self-adhesive resin cements to zirconia. Materials. 8(6), 3306–3315 (2015). https://doi.org/10.3390/ma8063306
Secilmis, A., Ustun, O., Kecik Buyukhatipoglu, I.: Evaluation of the shear bond strength of two resin cements on different CAD/CAM materials. J Adhes Sci Technol. 30(9), 983–993 (2016). https://doi.org/10.1080/01694243.2015.1134866
Chen, C., He, F., Burrow, M., Xie, H., Zhu, Y., Zhang, F.: Bond strengths of two self-adhesive resin cements to dentin with different treatments. J. Med. Biol. Eng. 31, 73–77 (2011). https://doi.org/10.5405/jmbe.681
Stawarczyk, B., Hartmann, R., Hartmann, L., Roos, M., Ozcan, M., Sailer, I., Hammerle, C.H.: The effect of dentin desensitizer on shear bond strength of conventional and self-adhesive resin luting cements after aging. Oper Dent. 36(5), 492–501 (2011). https://doi.org/10.2341/10-292-l
Henriques, B., Gonçalves, S., Soares, D., Silva, F.S.: Shear bond strength comparison between conventional porcelain fused to metal and new functionally graded dental restorations after thermal–mechanical cycling. J. Mech. Behav. Biomed. Mater. 13(Supplement C), 194–205 (2012). https://doi.org/10.1016/j.jmbbm.2012.06.002
Amornporncharoen, M., N, A., Sirimongkolwa, S.: Surface treatment of all-ceramic crown. CM Dent. J. 30, 15–22 (2009)
Jain, G., Narad, A., Boruah, L.C., Rajkumar, B.: Comparative evaluation of shear bond strength of three resin based dual-cure core build-up materials: an in-vitro study. J Conserv Dent. 18(4), 337–341 (2015). https://doi.org/10.4103/0972-0707.159754
Rodrigues, R.F., Ramos, C.M., Francisconi, P.A.S., Borges, A.F.S.: The shear bond strength of self-adhesive resin cements to dentin and enamel: an in vitro study. J Prosthet Dent. 113(3), 220–227 (2015). https://doi.org/10.1016/j.prosdent.2014.08.008
Hiraishi, N., Yiu, C.K., King, N.M., Tay, F.R.: Effect of pulpal pressure on the microtensile bond strength of luting resin cements to human dentin. Dent Mater. 25(1), 58–66 (2009). https://doi.org/10.1016/j.dental.2008.05.005
Acknowledgments
The authors would like to thank the Graduate School, Kasetsart University Research and Development Institute (KURDI) and Faculty of Engineering, Kasetsart University for research funding and a student scholarship, as well as the Faculty of Dentistry, Mahidol University, Bangkok, for providing analytical instruments and workspace.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Srichumpong, T., Suputtamongkol, K., Thongpun, N. et al. Comparison of shear bond strengths between a mica-based glass-ceramic and human dentin using three different resin cements. J Aust Ceram Soc 55, 47–55 (2019). https://doi.org/10.1007/s41779-018-0209-0
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s41779-018-0209-0
Keywords
- Mica-based glass-ceramics
- Machinable
- Resin cement
- Shear bond strength
- Dental materials