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Integral valorization of two-phase olive mill waste: extraction of cellulose and lignin and their characterization

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Abstract

The increased awareness regarding the economic and environmental impact of olive oil production waste has motivated a notable interest in reusing byproducts within the industry. By mitigating ecological risks associated with olive mill waste, this research addresses concerns about waste disposal and contributes to sustainable practices within the olive oil industry. This study focuses on extracting and characterizing two key biopolymers, cellulose and lignin, obtained from locally sourced two-phase olive mill waste. The development of a straightforward yet efficient extraction protocol yielded promising results, with 11.72% cellulose and 12.5% lignin successfully isolated from the waste material. The extracted biopolymers underwent thorough characterization utilizing advanced analytical techniques, such as Fourier-transformed spectroscopy, thermogravimetric analysis (TGA/DTG), X-ray diffraction (XRD), and scanning electron microscopy (SEM). These methods provided comprehensive insights into the structural and thermal properties of cellulose and lignin, confirming the success of the extraction process. Furthermore, the isolated biopolymers hold significant potential for diverse applications, further expanding the possibilities for their utilization. This comprehensive approach emphasizes the importance of repurposing byproducts to enhance economic and environmental sustainability in olive oil production.

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Data availability

The authors declare that the data supporting the findings of this study are available within the paper. The dataset used and/or analyzed during the current study is available from the authors on reasonable request.

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Acknowledgements

This work is supported by the Moroccan Ministry of Higher Education, Scientific Research and Innovation and the OCP Foundation, which funded this work through the APRD research program. The authors express their gratitude to Dr. Mehdi Mennani for his invaluable contribution in improving the quality of this paper and for his assistance in preparing the economic review, the authors also are grateful to Professor Jones Alami, head of Materials Science and Nanoengineering Department (MSN) at Mohammed VI Polytechnic University (UM6P) Ben guerir for supporting this work at MSN.

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Authors and Affiliations

Authors

Contributions

L.A.: conceptualization, methodology, investigation, formal analysis, writing—original draft, and writing—review and editing. Z.K.: supervision, conceptualization, methodology, validation, and review and editing. M.J.: methodology and formal analysis. A.M.: methodology and formal analysis. K.E.H.: supervision and review and editing. M.E.A.: supervision, conceptualization, methodology, resources, validation and review and editing. A.A.: supervision, conceptualization, resources, and review and editing.

Corresponding authors

Correspondence to Zineb Kassab, Mounir El Achaby or Adil Aboulkas.

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The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Additional information

Communicated by Walid Elfalleh.

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Azaryouh, L., Kassab, Z., Jaouahar, M. et al. Integral valorization of two-phase olive mill waste: extraction of cellulose and lignin and their characterization. Euro-Mediterr J Environ Integr (2024). https://doi.org/10.1007/s41207-024-00521-3

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  • DOI: https://doi.org/10.1007/s41207-024-00521-3

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