Abstract
A program of work was conducted as a means to understand the basis of tensile property variation in a production run of ductile iron parts for a transport (rail) application. Tensile test bars cast with the parts were evaluated from 55 production heats. The ductile iron was manufactured exclusively from high-quality pig iron with up to 25% revert, and the chemical composition was close between each heat. The desired outcome of casting was a predominantly ferritic structure corresponding to the 400-12 grade alloy in accordance with Standard AS1831-1985. Non-compliant tensile results were observed wherever elongation was reduced below 12%. This condition also represented a concomitant increase in yield and tensile strength, corresponding to increases in pearlite. Some examples displayed outstanding combinations of mechanical properties in their own right. Although variability in the proportions of ferrite and pearlite existed naturally within the alloys, it was found that the area fraction of ferrite or pearlite present on the fracture surface appears to have an influence on the overall outcomes of testing and relative quality. The distribution of these phases on the fracture surface was remarkably inhomogeneous and did not necessarily correlate to the 2-dimensional micrograph. A quality model was evaluated based on the determination of true-stress true-strain flow curves that demonstrate how the inhomogeneous distribution of ferrite and pearlite on the fracture surface appears to play a role in the microstructural factors affecting tensile failure of ductile iron, and therein the apparent quality of the material.
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References
ASM Handbook, Volume 1A: Cast Iron Science and Technology, D. Stefanescu ed., ASM International, (2017)
M. Gagné, ed. The SorelMetal Book of Ductile Iron, Rio Tinto Iron and Titanium, Montreal, Canada, (2004)
M.F. Burdett, ed., Ductile Iron Handbook, AFS, Shaumberg, Illinois, USA, (2013)
G.M. Goodrich, ed., Iron Castings Engineering Handbook, AFS, Schaumberg, Illinois, (2008)
AFS, Foundrymen’s Guide to Ductile Iron Microstructures, Schaumberg, Illinois, USA, (1984)
A. E. Fathelbab, Cast Iron Defect Analysis, The Cast Metals Foundation of Australia, (2001)
I. Riposan, M. Chisamera, S. Stan, Influencing factors on As-cast and heat treated 400–18 ductile iron grade characteristics. China Foundry 4(4), 300–303 (2007)
F. Zanardi, F. Bonollo, G. Angella, N. Bonora, G. Iannitti, A. Ruggiero, A contribution to new material standards for ductile irons and austempered ductile irons. Inter Metalcast 11, 136–147 (2017). https://doi.org/10.1007/s40962-016-0095-6
F. Zanardi, C. Mapelli, S. Barella, Reclassification of spheroidal graphite ductile cast irons grades according to design needs. Inter Metalcast 14, 622–655 (2020). https://doi.org/10.1007/s40962-020-00454-x
G. Angella, M. Cova, G. Bertuzzi, F. Zanardi, Soundness discrimination in ferrite ductile irons through tensile data analysis. Inter Metalcast. 14, 816–826 (2020). https://doi.org/10.1007/s40962-020-00435-0
G. Angella, F. Zanardi, Validation of a new quality assessment procedure for ductile irons production based on strain hardening analysis. Metals 8, 837 (2019). https://doi.org/10.3390/met9080837
J. Tartaglia, Comparison of monotonic and cyclic properties of ductile irons in the AFS/DOE strain-life fatigue database for cast iron. Inter Metalcast 6, 7–22 (2012). https://doi.org/10.1007/BF03355524
J.M. Tartaglia, R.B. Gundlach, G.M. Goodrich, Optimizing structure-property relationships in ductile iron. Inter Metalcast 8, 7–38 (2014). https://doi.org/10.1007/BF03355592
D. Franzen, B. Pustal, A. Bührig-Polaczek, Influence of graphite-phase parameters on the mechanical properties of high-silicon ductile iron. Inter Metalcast (2022). https://doi.org/10.1007/s40962-022-00761-5
J.O.T. Adewara, C.R. Loper Jr., Effect of carbides on crack initiation and propagation in ductile iron. AFS Trans. 84, 507–512 (1976)
J C. Margerie, The Notion of Heredity in Cast Iron Metallurgy, The Metallurgy of Cast Iron. Proc. 2nd Int. Symp. on the Physical Metallurgy of Cast Iron. Saphorin: Georgi Publishing Company, pp. 545-558, (1975)
D. Venugopalan, A. Alagarsamy, Effects of alloy additions on the microstructure and mechanical properties of commercial ductile iron. AFS Trans. 98, 395–400 (1990)
E.N. Pan, M.S. Lou, C.R. Loper, Effect of copper, tin and manganese on the euctectoid transformation of graphitic cast irons. AFS Trans. 95, 819–840 (1987)
J. Lacaze, S. Ford, C. Wilson, E. Dubu, Effects of alloying elements upon the eutectoid transformation in As-cast spheroidal graphite cast iron. Scand. J. Metall. 22, 300–309 (1993)
M.J. Lalich, C.R. Loper, Effects of pearlite promoting elements on the kinetics of the eutectoid transformation of ductile cast irons. AFS Trans. 81, 217–228 (1973)
G.F. Van Der Voort, ed., Atlas of time temperature diagrams for irons and steels, ASM International,pp. 754-766, (1991)
B. Karlsson, G. Lindén, Plastic deformation of eutectoid steel with different cementite morphology. Mater Sci. Eng 17, 153–164 (1975)
H.K.D.H Bhadesia, R.W.K. Honeycombe, Steels, microstructures and properties, 3rd edition, Butterworth Heinemann, Chapter 3, 39-70, (2006)
R.W. Cahn, W.C. Hagel, Theory of the Pearlite Reaction, In “The Selected Works of John W. Cahn. W. Craig Carter, William C Johnson eds. Pp. 127-198. (1998). https://doi.org/10.1002/9781118788295
B. Karlsson, G. Lindén, Pearlite structures in steel. Mater Sci. Eng 17, 209–219 (1975)
G. Langford, Deformation of pearlite. Met. Trans. A. 8A, 861–875 (1977)
Australian Standard AS1831-1985. Iron Castings- Spheroidal or Nodular Graphite Cast Iron, Standards Association of Australia, 2nd Edition, (1985)
Australian Standard AS1831-2002. Ductile Cast Iron, Standards Australia, MT-001, (2002)
International Standard ISO 1083-1987. Spheroidal Graphite Cast Irons – Classification, Edition 1, ISO/TC 25, (1987)
W. Siefer, K. Orths, Evaluation of ductile iron in terms of feasible properties of the material. AFS Trans. 78, 382–387 (1970)
D.L. Crews, Quality and specifications of ductile iron. AFS Trans. 82, 223–226 (1974)
C.R. Loper, R.M. Kotschi, Discussion-a new quality index for ductile cast iron. AFS Trans. 82, 226–228 (1974)
ASTM International, ASTM A536-84 (2019), Standard Specification for Ductile Iron Castings, (2019)
M. Drouzy, S. Jacob, M. Richard, Interpretation of tensile results by means of a quality index. AFS Int. Cast Metals J. 5, 43–50 (1980)
C.H. Cáceres, A rationale for the quality index of Al-7Si-0. 4Mg casting alloys. Int. J. Cast Metals Res. 10, 293–299 (1998)
C.H. Cáceres, A phenomenological approach to the quality index of Al-Si-Mg casting alloys. Int. J. Cast Metals Res. 12, 367–375 (2000)
C.H. Cáceres, B.I. Selling, Casting Defects and the tensile properties of an Al-SiMg Alloy, Mat. Sci. and Eng., A, 220/1-2, 109-116 (1996)
R.N. Lumley, N. Deeva, M. Gershenzon, An evaluation of quality parameters for high pressure die castings. Inter. Metalcast. 5, 37–56 (2011). https://doi.org/10.1007/BF03355517
R.N. Lumley, S.J. Bell, Derivation and experimental validation of a quality model for investment cast A357 alloy. AFS Trans. 121, 223–229 (2013)
Australian Standard AS1391-2020, Metallic Materials - Tensile Testing - Method of Test at Room Temperature MT-006 (2020)
International Standard ISO-945-1: 2019, Microstructure of Cast Irons-Part 1: Graphite Classification by Visual Analysis, ISO/TC 25 (2019)
J.O.T. Adewara, C.R. Loper, Effect of pearlite on crack initiation and propagation in ductile iron. AFS Trans. 84, 513–526 (1976)
J.O.T. Adewara, C.R. Loper, Crack initiation and propagation in fully ferritic ductile iron. AFS Trans. 84, 527–534 (1976)
Acknowledgements
The author would like to thank the AWBell foundry team for their efforts in making these castings and AWBell Pty. Ltd. for supporting the publication of this work. I would also like to thank Paul Hosking from Bureau Veritas for certified tensile testing, and Gary Savage from CSIRO for assistance with scanning electron microscopy.
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Lumley, R.N. Inhomogeneous Pearlite and Ferrite in Ductile Iron Sand Castings. Inter Metalcast 17, 1467–1492 (2023). https://doi.org/10.1007/s40962-022-00864-z
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DOI: https://doi.org/10.1007/s40962-022-00864-z