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Selective solid-phase extraction of aloe emodin from aloe by molecularly imprinted polymers

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Abstract

The extraction and separation of aloe emodin were optimized via selective molecularly imprinted solid-phase extraction. Molecularly imprinted polymer was prepared from the functional monomer, methacrylic acid and a mixture of ethanol/dodecanol(90/10, volume ratio) as porogen. It overcomes the common problems of imprinting biological polar compounds and shows high selectivity compared favorably with those of non-imprinted polymer and commercially available C18 and silica cartridges in similar aloe emodin tests. Good linearity was obtained between 0.002 and 2.5 mg/mL (r 2=0.998) with relative standard deviations below 3.3%.

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Authors and Affiliations

  1. College of Chemistry and Environmental Engineering, Yangtze University, Jingzhou, 434023, P. R. China

    Ming-lei Tian

  2. Department of Chemical Engineering, Inha University, Incheon, 402-751, Korea

    Ming-lei Tian, Yu-ri Lee & Kyung-ho Row

  3. Regional Innovation Center for Environmental Technology of Thermal Plasma, Inha University, Incheon, 402-751, Korea

    Dong-wha Park

Authors
  1. Ming-lei Tian
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  2. Yu-ri Lee
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  3. Dong-wha Park
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  4. Kyung-ho Row
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Corresponding author

Correspondence to Kyung-ho Row.

Additional information

Supported by the National Research Foundation(NRF) of Korea Funded by the Ministry of Education, Science and Technology (No.2012-0005250).

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Tian, Ml., Lee, Yr., Park, Dw. et al. Selective solid-phase extraction of aloe emodin from aloe by molecularly imprinted polymers. Chem. Res. Chin. Univ. 29, 663–666 (2013). https://doi.org/10.1007/s40242-013-2357-7

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  • DOI: https://doi.org/10.1007/s40242-013-2357-7

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