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Hot Deformation and Subsequent Annealing on the Microstructure and Hardness of an Al0.3CoCrFeNi High-entropy Alloy

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Acta Metallurgica Sinica (English Letters) Aims and scope

Abstract

The influence of simple thermomechanical processing such as hot deformation and heat treatment on the microstructure and hardness of an Al0.3CoCrFeNi high-entropy alloy has been investigated. Results show that the relatively high deformation temperature can induce discontinuous dynamic recrystallization with fine grains initially nucleating at the elongated grain boundaries. The transition from partial recrystallization to fully recrystallization, as well as the precipitation behavior after annealing, has been described in detail. Both bcc precipitation and completely recrystallized grains can be observed after annealing at 1000 °C. Based on detailed microstructure analysis, the decrease in hardness value is shown to be related to both dynamic recrystallization and dynamic recovery which lead to softening.

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The raw/processed data required to reproduce these findings cannot be shared at this time as the data also form part of an ongoing study.

References

  1. E.P. George, D. Raabe, R.O. Ritchie, Nat. Rev. Mater. 4, 515 (2019)

    Article  CAS  Google Scholar 

  2. W. Zhang, P.K. Liaw, Y. Zhang, Sci. China Mater. 61, 2 (2018)

    Article  CAS  Google Scholar 

  3. Y. Zhang, T.T. Zuo, Z. Tang, M.C. Gao, K.A. Dahmen, P.K. Liaw, Z.P. Lu, Prog. Mater Sci. 61, 1 (2014)

    Article  CAS  Google Scholar 

  4. S. Gorsse, D.B. Miracle, O.N. Senkov, Acta Mater. 135, 177 (2017)

    Article  CAS  Google Scholar 

  5. Z. Wang, Q. Fang, J. Li, B. Liu, Y. Liu, J. Mater. Sci. Technol. 34, 349 (2018)

    Article  Google Scholar 

  6. T. Yang, Y.L. Zhao, Y. Tong, Z.B. Jiao, J. Wei, J.X. Cai, X.D. Han, D. Chen, A. Hu, J.J. Kai, K. Lu, Y. Liu, C.T. Liu, Science 362, 933 (2018)

    Article  CAS  Google Scholar 

  7. T. Yang, Y.L. Zhao, J.H. Luan, B. Han, J. Wei, J.J. Kai, C.T. Liu, Scr. Mater. 164, 30 (2019)

    Article  CAS  Google Scholar 

  8. O.N. Senkov, J.K. Jensen, A.L. Pilchak, D.B. Miracle, H.L. Fraser, Mater. Des. 139, 498 (2018)

    Article  CAS  Google Scholar 

  9. Z. Li, S. Zhao, R.O. Ritchie, M.A. Meyers, Prog. Mater Sci. 102, 296 (2019)

    Article  CAS  Google Scholar 

  10. X.D. Xu, P. Liu, Z. Tang, A. Hirata, S.X. Song, T.G. Nieh, P.K. Liaw, C.T. Liu, M.W. Chen, Acta Mater. 144, 107 (2018)

    Article  CAS  Google Scholar 

  11. B. Gwalani, S. Gangireddy, Y. Zheng, V. Soni, R.S. Mishra, R. Banerjee, Sci. Rep. 9, 6371 (2019)

    Article  CAS  Google Scholar 

  12. D. Wei, X. Li, S. Schönecker, J. Jiang, W.-M. Choi, B.-J. Lee, H.S. Kim, A. Chiba, H. Kato, Acta Mater. 181, 318 (2019)

    Article  CAS  Google Scholar 

  13. B. Gwalani, S. Gorsse, D. Choudhuri, Y. Zheng, R.S. Mishra, R. Banerjee, Scr. Mater. 162, 18 (2019)

    Article  CAS  Google Scholar 

  14. Y.T. Wang, J.B. Li, Y.C. Xin, X.H. Chen, M. Rashad, B. Liu, Y. Liu, Acta Metall. Sin. -Engl. Lett. 32, 932 (2019)

    Article  CAS  Google Scholar 

  15. Y. Yu, P. Shi, K. Feng, J. Liu, J. Cheng, Z. Qiao, J. Yang, J. Li, W. Liu, Acta Metall. Sin.-Engl. Lett. 33, 1077 (2020)

    Article  CAS  Google Scholar 

  16. H. Yang, J. Li, X. Pan, W.Y. Wang, H. Kou, J. Wang, J. Mater. Sci. Technol. 72, 1 (2020)

    Article  Google Scholar 

  17. C. Zhao, J. Li, Y. Liu, W.Y. Wang, H. Kou, E. Beaugnon, J. Wang, J. Mater. Sci. Technol. 73, 83 (2021)

    Article  Google Scholar 

  18. T. Zheng, X. Hu, F. He, Q. Wu, B. Han, C. Da, J. Li, Z. Wang, J. Wang, J.J. Kai, Z. Xia, C.T. Liu, J. Mater. Sci. Technol. 69, 156 (2020)

    Article  Google Scholar 

  19. F.G. Coury, M. Kaufman, A.J. Clarke, Acta Mater. 175, 66 (2019)

    Article  CAS  Google Scholar 

  20. B. Yin, F. Maresca, W.A. Curtin, Acta Mater. 188, 486 (2020)

    Article  CAS  Google Scholar 

  21. M. Komarasamy, T. Wang, K. Liu, L. Reza-Nieto, R.S. Mishra, Scr. Mater. 162, 38 (2019)

    Article  CAS  Google Scholar 

  22. J. Čížek, P. Haušild, M. Cieslar, O. Melikhova, T. Vlasák, M. Janeček, R. Král, P. Harcuba, F. Lukáč, J. Zýka, J. Málek, J. Moon, H.S. Kim, J. Alloys Compd. 768, 924 (2018)

    Article  CAS  Google Scholar 

  23. Á. Vida, Z. Maksa, D. Molnár, S. Huang, J. Kovac, L.K. Varga, L. Vitos, N.Q. Chinh, J J. Alloys Compd. 743, 234 (2018)

    Article  CAS  Google Scholar 

  24. J.C. Rao, H.Y. Diao, V. Ocelík, D. Vainchtein, C. Zhang, C. Kuo, Z. Tang, W. Guo, J.D. Poplawsky, Y. Zhou, P.K. Liaw, J.T.M. De Hosson, Acta Mater. 131, 206 (2017)

    Article  CAS  Google Scholar 

  25. S. Wang, Y. Zhao, X. Xu, P. Cheng, H. Hou, Mater. Chem. Phys. 244, 122700 (2020)

    Article  CAS  Google Scholar 

  26. C. Haase, L.A. Barrales-Mora, Acta Mater. 150, 88 (2018)

    Article  CAS  Google Scholar 

  27. R.R. Eleti, T. Bhattacharjee, A. Shibata, N. Tsuji, Acta Mater. 171, 132 (2019)

    Article  CAS  Google Scholar 

  28. Y. Zhang, J. Li, J. Wang, W.Y. Wang, H. Kou, E. Beaugnon, J. Alloys Compd. 757, 39 (2018)

    Article  CAS  Google Scholar 

  29. Y. Zhang, J. Li, J. Wang, S. Niu, H. Kou, Metals 6, 277 (2016)

    Article  Google Scholar 

  30. N.N. Guo, L. Wang, L.S. Luo, X.Z. Li, R.R. Chen, Y.Q. Su, J.J. Guo, H.Z. Fu, Mater. Sci. Eng. A 651, 698 (2016)

    Article  CAS  Google Scholar 

  31. J. Yang, J.W. Qiao, S.G. Ma, G.Y. Wu, D. Zhao, Z.H. Wang, J. Alloys Compd. 795, 269 (2019)

    Article  CAS  Google Scholar 

  32. H. Yang, J. Li, T. Guo, W.Y. Wang, H. Kou, J. Wang, Met. Mater. Int. 25, 1145 (2019)

    Article  CAS  Google Scholar 

  33. Y.F. Kao, T.J. Chen, S.K. Chen, J.W. Yeh, J. Alloys Compd. 488, 57 (2009)

    Article  CAS  Google Scholar 

  34. B. Gwalani, V. Soni, M. Lee, S.A. Mantri, Y. Ren, R. Banerjee, Mater. Des. 121, 254 (2017)

    Article  CAS  Google Scholar 

  35. M. Annasamy, N. Haghdadi, A. Taylor, P. Hodgson, D. Fabijanic, Mater. Sci. Eng. A 754, 282 (2019)

    Article  CAS  Google Scholar 

  36. N.D. Stepanov, D.G. Shaysultanov, N.Y. Yurchenko, S.V. Zherebtsov, A.N. Ladygin, G.A. Salishchev, M.A. Tikhonovsky, Mater. Sci. Eng. A 636, 188 (2015)

    Article  CAS  Google Scholar 

  37. M. Tikhonova, A. Belyakov, R. Kaibyshev, Mater. Sci. Eng. A 564, 413 (2013)

  38. W.R. Wang, W.L. Wang, J.W. Yeh, J. Alloys Compd. 589, 143 (2014)

    Article  CAS  Google Scholar 

  39. B. Gwalani, D. Choudhuri, K. Liu, J.T. Lloyd, R.S. Mishra, R. Banerjee, Mater. Sci. Eng. A 771, 138620 (2020)

    Article  CAS  Google Scholar 

  40. T. Guo, J. Li, J. Wang, W.Y. Wang, Y. Liu, X. Luo, H. Kou, E. Beaugnon, Mater. Sci. Eng. A 729, 141 (2018)

    Article  CAS  Google Scholar 

  41. C.W. Tsai, Y.L. Chen, M.H. Tsai, J.W. Yeh, T.T. Shun, S.K. Chen, J. Alloys Compd. 486, 427 (2009)

    Article  CAS  Google Scholar 

  42. P.P. Bhattacharjee, G.D. Sathiaraj, M. Zaid, J.R. Gatti, C. Lee, C.W. Tsai, J.W. Yeh, J. Alloys Compd. 587, 544 (2014)

    Article  CAS  Google Scholar 

  43. K.Y. Tsai, M.H. Tsai, J.W. Yeh, Acta Mater. 61, 4887 (2013)

    Article  CAS  Google Scholar 

Download references

Acknowledgements

This work was financially supported by the Natural Science Foundation of China (No. 51774240), the Natural Science Foundation of Chongqing, China (No. cstc2020jcyj-msxmX0976), the Innovation Capability Support Program of Shaanxi (No. 2020KJXX-073) and the Fundamental Research Funds for the Central Universities.

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Correspondence to Jun Wang.

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Wang, J., Li, H., Yang, H. et al. Hot Deformation and Subsequent Annealing on the Microstructure and Hardness of an Al0.3CoCrFeNi High-entropy Alloy. Acta Metall. Sin. (Engl. Lett.) 34, 1527–1536 (2021). https://doi.org/10.1007/s40195-021-01251-z

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  • DOI: https://doi.org/10.1007/s40195-021-01251-z

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