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Controlling Corrosion Resistance of a Biodegradable Mg–Y–Zn Alloy with LPSO Phases via Multi-pass ECAP Process

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Acta Metallurgica Sinica (English Letters) Aims and scope

Abstract

Mg-RE (rear earth) alloys with long period stacking (LPSO) structures have great potential in biomedical applications. The present work focused on the microstructure and corrosion behaviors of Mg98.5Y1Zn0.5 alloys with 18R LPSO structure after equal channel angular pressing (ECAP). The results showed that the ECAP process changed the grain size and the distribution of LPSO particles thus controlled the total corrosion rates of Mg98.5Y1Zn0.5 alloys. During the ECAP process from 0p to 12p, the grain size reduced from 160–180 μm (as-cast) to 6–8 μm (12p). The LPSO structures became kinked (4p), then started to be broken into smaller pieces (8p), and at last comminuted to fine particles and redistributed uniformly inside the matrix (12p). The improvement in the corrosion resistance for ECAP samples was obtained from 0p to 8p, with the corrosion rate reduced from 3.24 mm/year (0p) to 2.35 mm/year (8p) in simulated body fluid, and the 12p ECAP alloy exhibited the highest corrosion rate of 4.54 mm/year.

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Acknowledgements

This work was supported by the National Natural Science Foundation of China (Nos. 51774109, 51979099 and 51901068), the Fundamental Research Funds for the Central Universities (No. 2018B690X14), the Natural Science Foundation of Jiangsu Province of China (No. BK20191303), the Postgraduate Research & Practice Innovation Program of Jiangsu Province (No. KYCX18_0570), the Key Research and Development Project of Jiangsu Province of China (No.BE2017148), and the Public Service Platform Program of Suqian City of China (No. M201614).

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Authors and Affiliations

  1. College of Mechanics and Materials, Hohai University, Nanjing, 210098, China

    Li-Sha Wang, Jing-Hua Jiang, Bassiouny Saleh, Qiu-Yuan Xie, Qiong Xu, Huan Liu & Ai-Bin Ma

  2. Suqian Institute, Hohai University, Suqian, 223800, China

    Li-Sha Wang & Ai-Bin Ma

  3. Production Engineering Department, Alexandria University, Alexandria, 21544, Egypt

    Bassiouny Saleh

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  1. Li-Sha Wang
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Correspondence to Jing-Hua Jiang or Huan Liu.

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Wang, LS., Jiang, JH., Saleh, B. et al. Controlling Corrosion Resistance of a Biodegradable Mg–Y–Zn Alloy with LPSO Phases via Multi-pass ECAP Process. Acta Metall. Sin. (Engl. Lett.) 33, 1180–1190 (2020). https://doi.org/10.1007/s40195-020-01042-y

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  • DOI: https://doi.org/10.1007/s40195-020-01042-y

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