Skip to main content
Log in

Layer Thickness-Dependent Hardness and Strain Rate Sensitivity of Cu–Al/Al Nanostructured Multilayers

  • Published:
Acta Metallurgica Sinica (English Letters) Aims and scope

Abstract

Cu–Al/Al nanostructured metallic multilayers with Al layer thickness h Al varying from 5 to 100 nm were prepared, and their mechanical properties and deformation behaviors were studied by nanoindentation testing. The results showed that the hardness increased drastically with decreasing h Al down to about 20 nm, whereafter the hardness reached a plateau that approaches the hardness of the alloyed Cu–Al monolithic thin films. The strain rate sensitivity (SRS, m), however, decreased monotonically with reducing h Al. The layer thickness-dependent strengthening mechanisms were discussed, and it was revealed that the alloyed Cu–Al nanolayers dominated at h Al ≤ 20 nm, while the crystalline Al nanolayers dominated at h Al > 20 nm. The plastic deformation was mainly related to the ductile Al nanolayers, which was responsible for the monotonic evolution of SRS with h Al. In addition, the h Al-dependent hardness and SRS were quantitatively modeled in light of the strengthening mechanisms at different length scales.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6

Similar content being viewed by others

References

  1. J.W. Yan, X.F. Zhu, B. Yang, G.P. Zhang, Phys. Rev. Lett. 110, 155502 (2013)

    Article  Google Scholar 

  2. J.Y. Zhang, X. Zhang, R.H. Wang, S.Y. Lei, P. Zhang, J.J. Niu, G. Liu, G.J. Zhang, J. Sun, Acta Mater. 59, 7368 (2011)

    Article  Google Scholar 

  3. J.J. Niu, J.Y. Zhang, G. Liu, P. Zhang, S.Y. Lei, G.J. Zhang, J. Sun, Acta Mater. 60, 3677 (2012)

    Article  Google Scholar 

  4. Y.Y. Lu, R. Kotoka, J.P. Ligda, B.B. Cao, S.N. Yarmolenko, B.E. Schuster, Q. Wei, Acta Mater. 63, 216 (2014)

    Article  Google Scholar 

  5. R. Raghavan, T.P. Harzer, V. Chawla, S. Djaziri, B. Phillipi, J. Wehrs, J.M. Wheeler, J. Michler, G. Dehm, Acta Mater. 93, 175 (2015)

    Article  Google Scholar 

  6. Y.P. Li, G.P. Zhang, Acta Mater. 58, 3877 (2010)

    Article  Google Scholar 

  7. N. Jia, M.W. Zhu, Y.R. Zheng, T. He, X. Zhao, Acta Metall. Sin. (Engl. Lett.) 28, 600 (2015)

  8. S.L. Lehoczky, Phys. Rev. Lett. 41, 1814 (1978)

    Article  Google Scholar 

  9. J.Y. Zhang, S. Lei, J. Niu, Y. Liu, G. Liu, X. Zhang, J. Sun, Acta Mater. 60, 4054 (2012)

    Article  Google Scholar 

  10. Y.X. Zhao, W.S. Lai, Acta Metall. Sin. (Engl. Lett.) 25, 141 (2012)

  11. A. Misra, J.P. Hirth, R.G. Hoagland, Acta Mater. 53, 4817 (2005)

    Article  Google Scholar 

  12. J.Y. Zhang, X. Zhang, G. Liu, G.J. Zhang, J. Sun, Scr. Mater. 63, 101 (2010)

    Article  Google Scholar 

  13. Y.Q. Wang, J.Y. Zhang, X.Q. Liang, K. Wu, G. Liu, J. Sun, Acta Mater. 95, 132 (2015)

    Article  Google Scholar 

  14. P. Zhang, J.Y. Zhang, J. Li, G. Liu, K. Wu, Y.Q. Wang, J. Sun, J. Mater. Sci. 50, 1901 (2014)

    Article  Google Scholar 

  15. P. Zhang, J.Y. Zhang, J. Li, G. Liu, K. Wu, Y.Q. Wang, J. Sun, Acta Mater. 76, 221 (2014)

    Article  Google Scholar 

  16. R. Saha, W.D. Nix, Acta Mater. 50, 23 (2002)

    Article  Google Scholar 

  17. D. Pan, A. Inoue, T. Sakurai, M.W. Chen, Proc. Natl. Acad. Sci. 105, 14769 (2008)

    Article  Google Scholar 

  18. J.Y. Zhang, Y. Liu, J. Chen, Y. Chen, G. Liu, X. Zhang, J. Sun, Mater. Sci. Eng. A 552, 392 (2012)

    Article  Google Scholar 

  19. Y. Liu, D. Bufford, H. Wang, C. Sun, X. Zhang, Acta Mater. 59, 1924 (2011)

    Article  Google Scholar 

  20. Y. Chen, Y. Liu, C. Sun, K.Y. Yu, M. Song, H. Wang, X. Zhang, Acta Mater. 60, 6312 (2012)

    Article  Google Scholar 

  21. P.A. Gruber, J. Böhm, F. Onuseit, A. Wanner, R. Spolenak, E. Arzt, Acta Mater. 56, 2318 (2008)

    Article  Google Scholar 

  22. M. Chen, E. Ma, K.J. Hemker, H. Sheng, Y. Wang, X. Cheng, Science 300, 1275 (2003)

    Article  Google Scholar 

  23. J.Y. Zhang, G. Liu, R.H. Wang, J. Li, J. Sun, E. Ma, Phys. Rev. B 81, 172104 (2010)

    Article  Google Scholar 

  24. M. Wang, D. Wang, T. Kups, P. Schaaf, Mater. Sci. Eng. A 644, 275 (2015)

    Article  Google Scholar 

  25. H.J. Choi, S.W. Lee, J.S. Park, D.H. Bae, Scr. Mater. 59, 1123 (2008)

    Article  Google Scholar 

  26. H. Miyamoto, K. Ota, T. Mimaki, Scr. Mater. 54, 1721 (2006)

    Article  Google Scholar 

  27. A.J. Kalkman, A.H. Verbruggen, S. Radelaar, J. Appl. Phys. 92, 6612 (2002)

    Article  Google Scholar 

  28. R.W. Hayes, D. Witkin, F. Zhou, E.J. Lavernia, Acta Mater. 52, 4259 (2004)

    Article  Google Scholar 

  29. J.Y. Zhang, Y.Q. Wang, K. Wu, P. Zhang, G. Liu, G.J. Zhang, J. Sun, Mater. Sci. Eng. A 612, 28 (2014)

    Article  Google Scholar 

  30. P. Gu, M. Dao, R.J. Asaro, S. Suresh, Acta Mater. 59, 6861 (2011)

    Article  Google Scholar 

  31. Q. Wei, S. Cheng, K.T. Ramesh, E. Ma, Mater. Sci. Eng. A 381, 71 (2004)

    Article  Google Scholar 

  32. R.J. Asaro, S. Suresh, Acta Mater. 53, 3369 (2005)

    Article  Google Scholar 

Download references

Acknowledgments

This work was supported by the National Natural Science Foundation of China (Grant Nos. 51321003, 51322104 and 51201123), the National Basic Research Program of China (Grant No. 2010CB631003) and the 111 Project of China (Grant No. B06025). G. Liu thanks the support from the Fundamental Research Funds for the Central Universities and the Tengfei Scholar project. J.Y. Zhang thanks the Natural Science Basic Research Plan in Shaanxi Province of China (Program No. 2015JM5158) and the Shaanxi Province Postdoctoral Scientific Research Project for partial financial support.

Author information

Authors and Affiliations

Authors

Corresponding authors

Correspondence to Gang Liu or Jun Sun.

Additional information

Available online at http://link.springer.com/journal/40195

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Wang, YQ., Hou, ZQ., Zhang, JY. et al. Layer Thickness-Dependent Hardness and Strain Rate Sensitivity of Cu–Al/Al Nanostructured Multilayers. Acta Metall. Sin. (Engl. Lett.) 29, 156–162 (2016). https://doi.org/10.1007/s40195-016-0372-7

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s40195-016-0372-7

Keywords

Navigation