Application of Response Surface Methodology on Leaching of Iron from Partially Laterised Khondalite Rocks: A Bauxite Mining Waste

Abstract

In the present investigation, response surface methodology (RSM) is used for a quadratic model that continuously controls the process parameters. This model is used to optimize the removal of iron oxide from Partially Laterised Khondalite (PLK) rocks which is influenced by several independent variables namely acid concentration, time and temperature. Second order response functions are produced for leaching of iron oxide from PLK rocks-a bauxite mining waste. In RSM, Box–Behnken design is used for the process optimization to achieve maximum removal of iron oxide. The influence of the process variables of leaching of iron oxide is presented in the form of 3-D response graphs. The results of this investigation reveals that 3 M hydrochloric acid concentration, 240 min time and 373 K temperature are found to be the best conditions for removal of 99% Fe2O3. The product obtain at this condition contain 80% brightness which is suitable for ceramic and filler industry applications. The novelity of the work is that the waste can be a value added product after suitable physical beneficiation and chemical treatment.

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References

  1. 1.

    D.C. Montgomerry, Design and Analysis of Experiments, 5th edn. (Wiley, New York, 2001)

    Google Scholar 

  2. 2.

    N. Aslan, Y. Cebeci, Fuel 86, 90–97 (2007)

    Article  Google Scholar 

  3. 3.

    N. Aslan, Powder Technol. 174, 127–133 (2007)

    Article  Google Scholar 

  4. 4.

    N. Aslan, F. Cifcia, D. Yanb, Sep. Purif. Technol. 59, 9–16 (2008)

    Article  Google Scholar 

  5. 5.

    N. Aslan, Sep. Purif. Technol. 64, 237–241 (2008)

    Article  Google Scholar 

  6. 6.

    S.K. Tripathy, Y. Ramamuthy, C. Raghu Kumar, Powder Technol. 201, 181–186 (2010)

    Article  Google Scholar 

  7. 7.

    S. Ubaldini, L. Piga, P. Fornari, R. Massidda, Hydrometallurgy 40(3), 369–379 (1996)

    Article  Google Scholar 

  8. 8.

    V.R. Ambikadevi, M. Lalithambika, Appl. Clay Sci. 16, 133–145 (2000)

    Article  Google Scholar 

  9. 9.

    D. Guillermo, T. Calderon, J.I. Rodriguez, U. Ortiz-Mendez, T.-L. M. Martinez, Azojomo, J. Mater. Online, 1–10 (2005). www.azom.com

  10. 10.

    M. Ranjbar, E. Aghaie, M.R. Hosseini, M. Pazouki, F. Ghavipanjeh, Adv. Mater. Res. 20–21, 115–118 (2007)

    Article  Google Scholar 

  11. 11.

    C.I. Nwoye, C.S. Nwobodo, C. Nlebedim, U.C. Nwoye, R.A. Umana, G.C. Obasi, J. Miner. Mater. Charact. Eng. 8(7), 531–539 (2009)

    Google Scholar 

  12. 12.

    C.I. Nwoye, J.E.O. Ovri, J. Eng. Sci. Technol. 5(2), 151–164 (2010)

    Google Scholar 

  13. 13.

    G. Mohanty, L. Besra, S. Bhattacharjee, B.P. Singh, Mater. Res. Bull. 43, 1814–1828 (2008)

    Article  Google Scholar 

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Correspondence to Ranjita Swain.

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Swain, R., Bhima Rao, R. Application of Response Surface Methodology on Leaching of Iron from Partially Laterised Khondalite Rocks: A Bauxite Mining Waste. J. Inst. Eng. India Ser. D 99, 23–31 (2018). https://doi.org/10.1007/s40033-017-0144-1

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Keywords

  • Partially Laterised Khondalite (PLK) rocks
  • Response surface methodology
  • X-ray diffraction
  • Iron oxide
  • Ceramic
  • Filler