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Synthesis, structure and optical properties of novel double penetration polypseudorotaxane compound templated by branched divalent cation template

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Abstract

This study is directed to branched cationic template, 1,3-bis(4-cyanopyridine) propane bromine salt (Bcpyp·2Br), which connected by metal pseudohalides to form novel double penetration polymeric compound: {(Bcpyp)[Cu2(SCN)3.33·Br0.68]·0.68H2O} (1). The structure was determined by single crystal X-ray diffraction analysis and further characterized by infrared spectra (IR), elemental analysis, powder X-ray diffraction (PXRD), and thermogravimetric (TG) analysis. Compound 1 also shows the better photocatalysis ability of degrading methylene blue (MB) than degrading rhodamine(RhB) and methyl orange(MO) in water under 500 W Xe vapor lamp irradiation.

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Acknowledgements

Research efforts in the Niu group are supported by the National Science Foundation of China (no. 21671177).

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Authors and Affiliations

  1. College of Chemistry and Molecular Engineering, Zhengzhou University, Henan, 450001, People’s Republic of China

    Fu-Rong Wang, Su-Min Li, Yun-Yin Niu & Hong-Wei Hou

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  1. Fu-Rong Wang
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  2. Su-Min Li
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  3. Yun-Yin Niu
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  4. Hong-Wei Hou
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Corresponding author

Correspondence to Yun-Yin Niu.

Electronic supplementary material

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13738_2018_1568_MOESM1_ESM.cif

Supporting information: important crystallographic data for 1. CCDC reference number: 1582772. This data can be obtained free of charge via http://www.ccdc.cam.ac.uk/conts/retrieving.html, or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK; Fax: t44 1223 336 033 or Email: deposit@ccdc.cam.ac.uk. (CIF 16 KB)

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Wang, FR., Li, SM., Niu, YY. et al. Synthesis, structure and optical properties of novel double penetration polypseudorotaxane compound templated by branched divalent cation template. J IRAN CHEM SOC 16, 939–944 (2019). https://doi.org/10.1007/s13738-018-1568-8

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  • DOI: https://doi.org/10.1007/s13738-018-1568-8

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