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Zirconia-Based Nanomaterials for Alternative Energy Application: Concept of Research in Smart Laboratory

  • Research Article-Chemical Engineering
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Abstract

The engineering of doped zirconia nanoparticles (NPs) for energy application is realized in concept Research Smart Laboratory. To improve nanomaterials’ engineering, correlations of “salt concentration—powder dispersity” and “calcined temperature—particle’s sizes” were built. The correlation of “materials structure—materials functionality” is made. The technology forming ceramics with varying grain sizes and densities under the same thermodynamic conditions (1350 °C) from NPs with different sizes is developed. The impedance spectroscopy with the distribution of relaxation time analysis is used for ionic conductivity ceramic investigation in range 240–900 °C. The activation energies of the grain and grain boundary oxygen diffusion are calculated. It was shown that the energy activation of bulk oxygen diffusion does not depend on ceramic grain size (Ea = 0.9 eV). The energies activation of grain boundary oxygen diffusion estimated in the framework of the bricklayer model show a weak growth with the rising of ceramic grains sizes. The values of the volume activation energy are close to the grain-boundary activation energy for ceramics obtained from nanoparticles smaller than 18 nm. It was found that the grain boundary space contains two types of elements with different geometries. The size of NPs used for ceramic determines the size of grain boundaries elements. It was shown that the density of sintered ceramic has a more substantial effect on its electrophysical properties than grain size. The NPs sizes of 18–24 nm are optimal for forming pressed powder compacts and sintered ceramics with high density.

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Abbreviations

CPE:

Constant phase element

C g, C gb1, C gb2 :

Capacity of grain and grain boundary spaces

DRS:

Distribution of relaxation time analysis

E a :

Energy activation

gb1, gb2:

Grain boundary spaces

NPs:

Nanoparticles

R :

Resistor

S sa :

Specific surface area

S msa :

External and mesoporous specific surface area

SEM:

Scanning electron microscopy

SOFC:

Solid oxide fuel cell

T cal :

Calcined temperature

U max :

Maximum of voltage

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Acknowledgements

The authors are thankful the H2020-MSCA-RISE-2019 Program, project 871284 SSHARE for partial support of this work.

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Authors and Affiliations

  1. Donetsk National Technical University, Pokrovsk, Ukraine

    Anton Gorban & Sergii Tsololo

  2. Material Science Department, Donetsk Institute for Physics and Engineering Named After O.O. Galkin NAS of Ukraine, Kiev, Ukraine

    Artem Shylo, Viktoriia Dmitrenko, Leonid Akhkozov, Valery Burkhovetsky, Oksana Gorban & Igor Danilenko

  3. REQUIMTE, Faculdade de Ciencias e Technologia, Universidade Nova de Lisboa, Quina de Torre, 2829-516, Caparica, Portugal

    Olesya Shapovalova

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Correspondence to Oksana Gorban.

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Gorban, A., Shylo, A., Dmitrenko, V. et al. Zirconia-Based Nanomaterials for Alternative Energy Application: Concept of Research in Smart Laboratory. Arab J Sci Eng 48, 8453–8469 (2023). https://doi.org/10.1007/s13369-022-06976-2

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  • DOI: https://doi.org/10.1007/s13369-022-06976-2

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