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Sulfonated Cross-Linked Poly(ether ether ketone) Films with Wrinkled Structures: Preparation and Vanadium Ions Permeability

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Abstract

Wrinkling patterns were fabricated by sulfonation of ion irradiated poly(ether ether ketone) (PEEK). A variety of wrinkling patterns in the micrometer to sub-micrometer range were observed and were controlled by the adsorbed dose and dose rate of the irradiated ions as well as the sulfonation time. Because of the properties of these micro-textured membranes, they are promising for a broad range of applications. In particular, the cross-linked membranes had a very low permeability of vanadium ions, i.e. 1.5 × 10−7 cm2 min−1 due to their wrinkled structures in combination with the Donnan exclusive effect.

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Authors and Affiliations

  1. Department of Chemistry, Atomic Energy Commission, Damascus, P.O. Box 6091, Syrian Arab Republic

    Abdul G. Al Lafi & Reem Hasan

  2. Department of Physics, Atomic Energy Commission, Damascus, P.O. Box 6091, Syrian Arab Republic

    Nedal Al-Kafri

Authors
  1. Abdul G. Al Lafi
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  2. Reem Hasan
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  3. Nedal Al-Kafri
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Correspondence to Abdul G. Al Lafi.

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Acknowledgment: The authors thank Prof. James N. Hay and Prof. David J. Parker for allowing the use of irradiation facility. Thanks are also due to Prof. I. Othman; the DG of the AEC of Syria and Prof. Z Ajji the Head of Chemistry Department for their support. The authors would also like to thank T. Hassan and J. Abo Hlal for their technical supports.

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Al Lafi, A.G., Hasan, R. & Al-Kafri, N. Sulfonated Cross-Linked Poly(ether ether ketone) Films with Wrinkled Structures: Preparation and Vanadium Ions Permeability. Macromol. Res. 27, 1239–1247 (2019). https://doi.org/10.1007/s13233-019-7166-5

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  • DOI: https://doi.org/10.1007/s13233-019-7166-5

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