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Gallium-Based Metallic Pastes: Preparation from Powder Mixture by In Situ Synthesis of Liquid Component

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Abstract

The paper presents a method for the synthesis of metal pastes and diffusion-hardening alloys based on gallium by intensive vibrational mixing of powder components: solid gallium and a complex of filler powders. Using this method (with a specially selected fractional composition of powdered components), a series of samples of Cu–Ga–Sn alloys were obtained—one of the “classic” systems used (with various additives) as metal solder adhesives and dental filling materials. Structural, thermochemical (DSC), physical and mechanical properties, phase composition of initial and hardened samples are presented. When mixing, dosing and storing the components of the initial powder mixture, there is no noticeable segregation, contact-reactive melting of the components. The production of gallium pastes in this work includes the synthesis of the liquid metal component in situ, in the process of vibration treatment of the powder mixture. In addition to ease of use, this method, apparently, can provide new opportunities for the design of the structure of gallium pastes, putties, hard metal solder adhesives and filling materials.

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Funding

The work was carried out according to the state assignment for IMET UB RAS, using equipment of the Collaborative usage center «Ural-M».

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  1. Laboratory of Metallurgical Melts, Institute of Metallurgy of the Ural Branch of the Russian Academy of Sciences, 101 Amundsena Street, Ekaterinburg, Russia, 620016

    Alexey Shubin & Ivan Gilev

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  1. Alexey Shubin
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  2. Ivan Gilev
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Contributions

AS contributed to conceptualization, methodology, writing—original draft preparation and resources; AS and IG contributed to writing—review and editing, synthesis and investigations and theoretical analysis; and IG contributed to project administration. All authors have read and agreed to the published version of the manuscript.

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Correspondence to Ivan Gilev.

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Shubin, A., Gilev, I. Gallium-Based Metallic Pastes: Preparation from Powder Mixture by In Situ Synthesis of Liquid Component. Trans Indian Inst Met 77, 1063–1070 (2024). https://doi.org/10.1007/s12666-023-03235-2

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