Abstract
Determination of the thickness of a nanometer thin film is an important topic in the nanostructure characterization field. Currently, the X-ray photoelectron spectroscopy and the ellipsometer have been used to analyze the film thickness. This work proposes another thickness measurement method based on secondary electron (SE) and backscattered electron (BE) yields which are produced by an electron beam with a certain energy. Through comprehensively analyzing a lot of simulated data of the ratio of SE to BE yields at different primary energies and overlayer thicknesses for a variety of overlayer/substrate structures, a semiempirical formula was obtained for the film thickness determination (up to 5 nm). According to the formula, the film thickness can be obtained based on the measured ratio of SE to BE yields. A specific example shows a good agreement is reached between the simulated and experimental measurements in the case of the Be/Pt systems.
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References
G E J Jr et al Thin Solid Films 4 40 (1996)
T M Merklein et al Appl. Opt. 4 505 (1990)
J Zemek et al Surf. Interface Anal. 38 615 (2010)
S F Mao et al Surf. Interface Anal. 40 728 (2010)
M V C Riglos and A Tolley Appl. Surf. Sci. 254 420 (2007)
Z Y Tan and Y Y Xia Scanning 24 257 (2002)
P Zhang Pramana – J. Phys. 90 81 (2018)
P Zhang Moscow Univ. Phys. Bull. 73 89 (2018)
C Li et al J. Phys. D Appl. Phys. 51 16531 (2018)
P Zhang, S Mao and Z J Ding European Physical Journal Applied Physics 69 3 (2015)
P Zhang et al Scanning 34 145 (2012)
Z M Zhang and Z J Ding SPIE Defense, Security, and Sensing (2013)
Z Ruan et al e-J. Surf. Sci. Nanotech. 12 247 (2014)
Z J Ding and R Shimizu Scanning 18 92 (2010)
Z J Ding, X D Tang and R Shimizu J. Appl. Phys. 89 718 (2001)
Z J Ding et al Appl. Phys. A 78 585 (2004)
Z J Ding et al J. Appl. Phys. 96 4598 (2004)
Z Zhang et al Surf. Interface Anal. 35 403 (2010)
D R Penn Phys. Rev. B Condens. Matter 35 482 (1987)
E D Palik Boston Academic Press 1 77 (1991)
C J Powell and A Jablonski J. Surf. Anal. 9 322 (2002)
I M Bronshtein and B B Segal Soviet Phys. Solid State 1 1365 (1960)
Acknowledgements
This work was supported by the Youth Project of Science and Technology Research Program of Chongqing Education Commission of China (KJQN201901407), the start-up research funding of Yangtze Normal University (No. 2017KYQD113), 2017 Youth Research Talent Supporting Program (2017QNRC18).
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Zhang, P. Thickness analysis of nanometer thin films based on electron yields. Indian J Phys 95, 61–66 (2021). https://doi.org/10.1007/s12648-019-01673-7
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DOI: https://doi.org/10.1007/s12648-019-01673-7