Abstract
In this study we have investigated the effects of the chain length of hydrolyzable groups in two isocyanato silane coupling agents, 3-isocyanatopropyltrimethoxysilane and 3-isocyanatopropyltriethoxysilane, on the shear bond strength of resin attached to silicatized zirconia. In addition, the effects of varying the silane concentration (at 0.1 vol% and 1.0 vol%) with or without the addition of a cross-linking silane (0.05 vol% or 0.5 vol% bis-1,2-(triethoxysilyl)ethane) were assessed. It was concluded that the use of the experimental primer of 3-isocyanatopropyltrimethoxysilane at either 0.1 vol% or 1 vol% with cross-linking silane resulted in significantly higher shear bond strengths than the use of primer without the cross-linking silane.
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Open Access This is an open access article distributed under the terms of the Creative Commons Attribution Noncommercial License (https://creativecommons.org/licenses/by-nc/2.0), which permits any noncommercial use, distribution, and reproduction in any medium, provided the original author(s) and source are credited.
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Lung, C.Y.K., Matinlinna, J.P. Resin Bonding to Silicatized Zirconia with Two Isocyanatosilanes and a Cross-linking Silane. Part I: Experimental. Silicon 2, 153–161 (2010). https://doi.org/10.1007/s12633-010-9044-9
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DOI: https://doi.org/10.1007/s12633-010-9044-9