Abstract
In this study we have assessed the effect of long-term water storage at 37oC on silane-aided adhesion promotion. Five experimental silane blends were evaluated as adhesion-promoters. First, five functional organosilane monomers (silicon esters), 3-acryloxypropyltrimethoxysilane, 3-methacryloxypropyltrimethoxysilane, 3-glycidoxypropyltrimethoxysilane, tetrakis-(2-methacryloxyethoxy)silane and bis-[3-(triethoxysilyl)propyl]tetrasulfide, were diluted to 1% (v/v) in 95% ethanol and blended with a non-functional cross-linking silane, bis-1,2-(triethoxysilyl)ethane (1%). A commercially available pre-activated silane product was used as the control. After activation by hydrolysis, each primer blend was applied to silica-coated Ti coupons. Stubs of experimental bis-phenol-A-diglycidyldimethacrylate (bis-GMA)-based resin were bonded by photo-polymerization onto the pretreated Ti coupons. Half of the specimens were stored in deionized water for 6 months and half for 12 months. The primer containing 3-acryloxypropyltrimethoxysilane and bis-1,2-(triethoxysilyl)ethane produced significantly higher shear bond strengths than the control silane and other experimental silane primers after both periods of storage.
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Open Access This is an open access article distributed under the terms of the Creative Commons Attribution Noncommercial License (https://creativecommons.org/licenses/by-nc/2.0), which permits any noncommercial use, distribution, and reproduction in any medium, provided the original author(s) and source are credited.
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Matinlinna, J.P., Lassila, L.V. Experimental Novel Silane System in Adhesion Promotion between Dental Resin and Pretreated Titanium. Part II: Effect of Long-Term Water Storage. Silicon 2, 79–85 (2010). https://doi.org/10.1007/s12633-010-9039-6
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DOI: https://doi.org/10.1007/s12633-010-9039-6