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Characterization and parameter optimization of a microcellular polypropylene electret under an external inertial load

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Abstract

In this study, microcellular polypropylene (PP) electrets were fabricated under various charge and process conditions. This was followed by thermally stimulated current (TSC) experiments to examine in a qualitative manner the charge stability of the electrets and the origin of the surface and space charges. In addition, a series of experiments was performed to obtain the effective piezoelectric constant in the thickness direction using an equation that considers external inertial loading effects. An optimization process using the Taguchi method was conducted to find the optimal conditions for the charging process and the electret properties that maximize the piezoelectric effects. To compare the contributions of signal parameters, a pooled analysis of variance (pooled ANOVA) was used. From these results, the factors that most significantly influence the piezoelectric effects were identified. A response surface was constructed to predict the optimal values of these factors to obtain the best piezoelectric effects. As a consequence, the applied voltage and the modified film thickness were turned out to be the most influential factors, and it was predicted that the optimal conditions are a 30-kV corona discharge and use of 60-µm-thick film.

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Abbreviations

x i :

coordinate axis in the i th direction; i th input variable

ϕ :

electric potential

d33*:

effective piezoelectric constant of film in x 3 direction

Q :

total amount of charge

h :

film thickness

u 3 (h) :

displacement of the film’s top surface in x 3 direction

A :

surface area of film

m :

mass of loading mass

g :

gravitational acceleration constant

τ3 (h) :

applied stress at the film’s top surface in x 3 direction

s 33 E* :

effective compliance of film in x 3 direction

s ij E :

tensor components of compliance

βi(j)(i, j=1,...,k):

regression coefficients

y ij :

ith response at the jth trial

n i :

replications for the i th response

ξ i :

ith independent variable

ξ 0i :

averages of the measured values of ξ i

c i :

constants to normalize ξ i

y :

output variable

ŷ :

estimated output function

S/N ratio i :

signal to noise ratio of the i th response

References

  1. Kim, Y., Kim, P. and Seok, J., “Piezoelectricity of a microcellular polypropylene electret under an external inertial load,” Jpn. J. Appl. Phys., Vol. 48, No. 3, pp. 031402, 2009.

    Article  Google Scholar 

  2. Hong, C.-U., Kim, J.-M., Kim, M.-H., Kim, S.-J., Kang, H.-S., Kim, J.-S. and Kim, G.-B., “Gas transfer and hemolysis in an intravascular lung assist device using a PZT actuator,” IJPEM, Vol. 10, No. 1, pp. 67–73, 2009.

    Google Scholar 

  3. Zhang, X., Hillenbrand, J. and Sessler, G. M., “Piezoelectric d33 coefficients of cellular polypropylene subjected to expansion by pressure treatment,” Appl. Phys. Lett., Vol. 85, No. 7, pp. 1226–1228, 2004.

    Article  Google Scholar 

  4. Zhang, X., Sessler, G. M. and Hillenbrand, J., “Improvement of piezoelectric coefficients of cellular polypropylene films by repeated expansions,” J. Electrostat., Vol. 65, No. 2, pp. 94–100, 2007.

    Article  Google Scholar 

  5. Wegener, M., Wirges, W. and Multhaupt, R. G., “Two-step inflation of cellular polypropylene films: void-thickness increase and enhanced electromechanical properties,” J. Phys. D: Appl. Phys., Vol. 37, No. 4, pp. 623–627, 2004.

    Article  Google Scholar 

  6. Zhang, X., Hillenbrand, J. and Sessler, G. M., “Improvement of piezoelectric activity of cellular polymers using a double-expansion process,” J. Phys. D: Appl. Phys., Vol. 37, No. 15, pp. 2146–2150, 2004.

    Article  Google Scholar 

  7. Zhang, X., Hillenbrand, J. and Sessler, G. M., “Thermally stable fluorocarbon ferroelectrets with high piezoelectric coefficients,” Appl. Phys. A: Mater. Sci. Proc., Vol. 84, No. 1–2, pp. 139–142, 2006.

    Google Scholar 

  8. Raizer, Y. P., “Gas discharge physics,” Springer, 1991.

  9. Kim, P., Kim, Y. S., Lee, J. and Seok, J., “TSC (Thermally Stimulated Current) characteristic analysis for cellular polypropylene film electret,” Proceeding of KSPE Autumn Conference, pp. 249–250, 2008.

  10. Mekishev, G. A., Yovcheva, T. A. and Viraneva, A. P., “Investigation of PP and PTFE film electrets stored at low pressure,” Non-Cryst. Solids, Vol. 353, No. 47–51, pp. 4453–4456, 2007.

    Article  Google Scholar 

  11. Yovcheva, T. A., Avramova, I. A., Mekishev, G. A. and Marinova, T. S., “Corona-charged polypropylene electrets analyzed by XPS,” J. Electrostat., Vol. 65, No. 10–11, pp. 667–671, 2007.

    Article  Google Scholar 

  12. Xia, Z., Ma, S., Qiu, X. and Zhang, Y., “Thermal stability of piezoelectricity for porous polytetrafluoroethlyene electrets film,” J. Electrostat., Vol. 58, No. 3–4, pp. 265–274, 2003.

    Article  Google Scholar 

  13. Yovcheva, T., Mekishev, G. and Nedev, St., “Corona electrets obtained in different gas media,” J. Optoelectron. Adv. Mater., Vol. 7, No. 1, pp. 237–240, 2005.

    Google Scholar 

  14. Sahli, S., Bellel, A., Ziari, Z., Kahlouche, A. and Segui, Y., “Measure and analysis of potential decay in polypropylene films after negative corona charge deposition,” J. Electrostat., Vol. 57, No. 2, pp. 169–181, 2003.

    Article  Google Scholar 

  15. Taguchi, G., Elsayed, E. A. and Hsiang, T., “Quality engineering in production systems,” McGraw-Hill, 1989.

  16. Yovcheva, T. A., Mekishev, G. A. and Marinov, A. T. “A percolation theory analysis of surface potential decay related to corona charged polypropylene (PP) electrets,” J. Phys.: Condens. Matter., Vol. 16, No. 3, pp. 455–464, 2004.

    Article  Google Scholar 

  17. Giacometti, J. A. and Carvalho Campos, J. S., “Constant current corona triode with grid voltage control. Application to polymer foil charging,” Rev. Sci. Instrum., Vol. 61, No. 3, pp. 1143–1150, 1990.

    Article  Google Scholar 

  18. Kacprzyk, R., “Polarization of porous PE foil,” Proc. of 11th International Symposium on Electrets, pp. 207–210, 2002.

  19. Kim, Y., “Characterization of a cellular polypropylene electret and its optimization,” MS thesis, School of Mechanical Engineering, Chung-Ang University, 2008.

  20. Chen, Q., “Negative corona charge stability in plasma treated polytetrafluoroethylene teflon films,” J. Phys. D: Appl. Phys., Vol. 37, No. 5, pp. 715–720, 2004.

    Article  Google Scholar 

  21. Gray, S., “A letter from Mr. Stephen Gray to Dr. Mortimer, Secr. R. S. Containing a farther account of his experiments concerning electricity,” Phil. Trans., Vol. 37, pp. 285–291, 1732.

    Article  Google Scholar 

  22. Jain, V. and Mittal, A., “Charge storage studies of unstretched and stretched polypropylene film electrets using short circuit TSDC technique,” J. of Mater. Sci. Lett., Vol. 19, No. 22, pp. 1991–1994, 2000.

    Article  Google Scholar 

  23. Pan, L. K., Wang, C. C., Hsiao, Y. C. and Ho, K. C., “Optimization of Nd: YAG laser welding onto magnesium alloy via Taguchi analysis,” Opt. Laser Technol., Vol. 37, No. 1, pp. 33–42, 2005.

    Google Scholar 

  24. Kumar, P. and Gaindhar, J. L., “Vacuum-sealed molding process: a review,” Proc. of 7th National Convention of Production Engineering Conference, pp. 35–40, 1998.

  25. Chen, J. and Davidson, J. H., “Electron density and energy distributions in the positive DC Corona: Interpretation for corona-enhanced chemical reactions,” Plasma Chem. Plasma Process., Vol. 22, No. 2, pp. 199–224, 2002.

    Article  Google Scholar 

  26. Chen, J. and Davidson, J. H., “Ozone production in the positive DC corona discharge: Model and comparison to experiments,” Plasma Chem. Plasma Process., Vol. 22, No. 4, pp. 495–522, 2002.

    Article  Google Scholar 

  27. Chen, J. and Davidson, J. H., “Model of the negative DC corona plasma: Comparison to the positive DC corona plasma,” Plasma Chem. Plasma Process., Vol. 23, No. 1, pp. 83–102, 2003.

    Article  Google Scholar 

  28. Lu, T. J., “Charging temperature effect for corona charged Teflon FEP electrets,” Proc. 7th Int. Symp. Electrets, pp. 287–292, 1991.

  29. Gross, B., Giacometti, J. A. and Leal Ferreira, G. F., “Constant schubweg for hole transport in corona charged fluorethylenepropylene,” Appl. Phys. A, Vol. 37, No. 2, pp. 89–94, 1985.

    Article  Google Scholar 

  30. Oliveira, O. N. Jr. and Leal Ferreira, G. F., “Electron transport in corona charged 12 µm teflon FEP with saturable deep traps,” Appl. Phys. A, Vol. 42, No. 3, pp. 213–217, 1987.

    Article  Google Scholar 

  31. Multhaupt, R. G., “Less can be more: Holes in polymers lead to a new paradigm of piezoelectric materials for electret transducers,” IEEE Trans. Diel. Electr. Insul., Vol. 9, No. 5, pp. 850–859, 2002.

    Article  Google Scholar 

  32. Myers, R. C., “Response surface methodology,” Allyn and Bacon Inc., 1971.

  33. Sessler, G. M., “Electrets,” Springer Verlag, pp.118–142, 1980.

  34. Turnhout, J., Staal, R. E., Wubbenhorst, M. and Haan, P. H., “Distribution and stability of charges in porous polypropylene films,” 10th International Symposium on Electrets, pp. 785–788, 1999.

  35. Roy, R. K., “A primer on the Taguchi method,” Van Nostrand Reinhold, 1990.

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Correspondence to Jongwon Seok.

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Kim, Y., Kim, P., Lee, J. et al. Characterization and parameter optimization of a microcellular polypropylene electret under an external inertial load. Int. J. Precis. Eng. Manuf. 10, 97–106 (2009). https://doi.org/10.1007/s12541-009-0100-6

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  • DOI: https://doi.org/10.1007/s12541-009-0100-6

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