Skip to main content
SpringerLink
Log in

Microstructure Evolution and Dynamic Precipitation Behavior of Mg–10Gd–4Y–1Sm–0.5Zr Alloy During Backward Hot Extrusion

  • Published:
Metals and Materials International Aims and scope Submit manuscript

Abstract

The microstructure evolution and dynamic precipitation behavior of Mg–10Gd–4Y–1Sm–0.5Zr alloy during backward hot extrusion are studied. The results show that the equiaxed grains become polygonal grains and fine DRX grains are generated which form a “necklace structure” along the initial deformed grain boundaries. With further increase of deformation, DRX grains volume fraction significantly increases and finally almost fully DRX extruded microstructure is obtained in the completely hot-extruded sample. The extrusion deformation results in increase of dislocation density and formation of dislocation cells. The subgrain boundaries continue to absorb dislocations and finally change from the low angle grain boundaries to the high angle grain boundaries. Hot extrusion deformation results in formation of dynamic precipitated phase, β phase particle, i.e., Mg5(Gd,Y) phase, with diameter of 45–145 nm, which is incoherent relationship with the matrix. In process of increasing deformation, the shape of β phase changes from spindle shape to disc shape and the distribution of β phase transforms from strip distribution along grain boundary to discrete distribution.

Graphic Abstract

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5

Similar content being viewed by others

References

  1. Y.H. Ali, D. Qiu, B. Jiang, F.S. Pan, M.X. Zhang, J. Alloy. Compd. 619, 639 (2015)

    Article  CAS  Google Scholar 

  2. X.H. Tan, W. Chee, J. Chan, R. Kwok, M. Gupta, Met. Mater. Int. 23, 699 (2017)

    Article  CAS  Google Scholar 

  3. X.Y. Chen, Q.A. Li, J. Chen, L.M. Zhu, J. Rare Earths 37, 1351 (2019)

    Article  CAS  Google Scholar 

  4. B. Chen, Ch Lu, D.L. Lin, X.Q. Zeng, Met. Mater. Int. 20, 285 (2014)

    Article  CAS  Google Scholar 

  5. N.Y. Liu, Z.H.Y. Zhang, L.M. Peng, W.J. Ding, Mater. Sci. Eng. A 627, 223 (2015)

    Article  CAS  Google Scholar 

  6. X.Y. Xia, W.H. Sun, A.A. Luo, D.S. Stone, Acta Mater. 11, 335 (2016)

    Article  Google Scholar 

  7. X.P. Luo, D.Q. Fang, Q.S.H. Li, Y.S.H. Chai, J. Rare Earths 34, 1134 (2016)

    Article  CAS  Google Scholar 

  8. Y. Chen, Z. Xu, C. Smith, J. Sankar, Acta Biomater. 10, 4561 (2014)

    Article  CAS  Google Scholar 

  9. Y.S.H. Chai, Z.H.G. Gao, K.L. Cai, D.Q. Fang, Rare Met. Mater. Eng. 45, 287 (2016)

    Article  CAS  Google Scholar 

  10. J. Zheng, Q. Wang, Z. Jin, T. Peng, Mater. Sci. Eng. A 527, 1677 (2010)

    Article  Google Scholar 

  11. C. Xu, M.Y. Zheng, S.W. Xu, K. Wu, E.D. Wang, S. Kamado, G.J. Wang, Mater. Sci. Eng. A 559, 844 (2013)

    Article  CAS  Google Scholar 

  12. X.M. Zhang, L. Li, Y.L. Deng, N. Zhou, J. Alloy. Compd. 481, 296 (2013)

    Article  Google Scholar 

  13. J.F. Nie, Metall. Mater. Trans. A 43, 3891 (2012)

    Article  CAS  Google Scholar 

  14. S.V. Dobatkin, L.L. Rokhlin, E.A. Lukyanova, M.Y. Murashkin, T.V. Dobatkina, N.Y. Tabachkova, Mater. Sci. Eng. A 667, 217 (2016)

    Article  CAS  Google Scholar 

  15. L. Jun, Y. Hong, C.R. Shi, Mater. Sci. Eng. A 614, 88 (2014)

    Article  Google Scholar 

  16. J.P. Li, Z. Yang, T. Liu, Scripta Mater. 56, 137 (2007)

    Article  CAS  Google Scholar 

  17. M. Hong, S.S.A. Shah, D. Wu, R.S. Chen, X.H. Du, N.T. Hu, Y.F. Zhang, Met. Mater. Int. 22, 1091 (2016)

    Article  CAS  Google Scholar 

  18. S.M. He, X.Q. Zeng, L.M. Peng, X. Gao, J.F. Nie, W.J. Ding, J. Alloy. Compd. 427, 316 (2007)

    Article  CAS  Google Scholar 

  19. Y.P. Wu, H.Q. Xiong, Y.Z.H. Jia, S.H. Xie, G.F. Li, Trans. Nonferrous Met. Soc. China 29, 976 (2019)

    Article  CAS  Google Scholar 

  20. D.X. Zhang, Z. Tan, Q.H. Huo, Z.Y. Xiao, Z.W. Fang, X.Y. Yang, Mater. Sci. Eng. A 715, 389 (2018)

    Article  CAS  Google Scholar 

  21. Y.P. Wu, X.M. Zhang, Y.L. Deng, C.H.P. Tang, L. Yang, Y.Y. Zhong, Trans. Nonferrous Met. Soc. China 25, 1831 (2015)

    Article  CAS  Google Scholar 

  22. H. Zhou, W.Z. Xu, W.W. Jian, G.M. Cheng, X.L. Ma, W. Guo, S.N. Mathaudhu, Q.D. Wang, Y.T. Zhu, Philos. Mag. 94, 2403 (2014)

    Article  CAS  Google Scholar 

  23. E. Nes, Acta Mater. 43, 2189 (1995)

    Article  CAS  Google Scholar 

  24. Y. Deng, Z.M. Yin, J.W. Huang, Mater. Sci. Eng. A 528, 1780 (2011)

    Article  Google Scholar 

  25. A. Galiyev, R. Kaibyshev, G. Gottestein, Acta Mater. 49, 1199 (2001)

    Article  CAS  Google Scholar 

  26. L. Gao, S.M. Liang, R.S. Chen, E.H. Han, Trans. Nonferrous Met. Soc. China 20, 1585 (2010)

    Article  CAS  Google Scholar 

  27. WSh Liu, D.L. Liu, YZh Ma, J. Wang, B.P. Yang, Trans. Nonferrous Met. Soc. China 25, 308 (2015)

    CAS  Google Scholar 

  28. C.Y. Nam, J.H. Han, Y.H. Chung, M.C. Shin, Mater. Sci. Eng. A 347, 253 (2003)

    Article  Google Scholar 

  29. K. R. Cardoso, D. N. Travessa, W. J. Botta, A. M. Jorge Jr., Mater. Sci. Eng., A528, 5804 (2011)

  30. W. Guo, Q. Wang, B. Ye, H. Zhou, J. Alloy. Compd. 558, 164 (2013)

    Article  CAS  Google Scholar 

  31. S.K. Das, Y.B. Kang, T.K. Ha, I.H. Jung, Acta Mater. 71, 164 (2014)

    Article  CAS  Google Scholar 

  32. W. Xu, D.P. Edwards, X. Wu, M. Stoica, M. Calin, U. Kühn, J. Eckert, K. Xia, Scr. Mater. 68, 67 (2013)

    Article  CAS  Google Scholar 

  33. K. Mathis, J. Gubicza, N.H. Nam, J. Alloy. Compd. 394, 194 (2005)

    Article  CAS  Google Scholar 

  34. S.M. He, X.Q. Zeng, L.M. Peng, X. Gao, J.F. Nie, W.J. Ding, J. Alloy. Compd. 421, 309 (2006)

    Article  CAS  Google Scholar 

  35. X. Gao, S.M. He, X.Q. Zeng, L.M. Peng, W.J. Ding, J.F. Nie, Mater. Sci. Eng. A 431, 322 (2006)

    Article  Google Scholar 

  36. J.F. Nie, B.C. Muddle, Acta Mater. 48, 1691 (2000)

    Article  CAS  Google Scholar 

  37. T.T. Sasaki, K. Oh-ishi, T. Ohkubo, K. Hono, Scr. Mater. 55, 251 (2006)

    Article  CAS  Google Scholar 

  38. J.B. Clark, Acta Mater. 16, 141 (1968)

    Article  CAS  Google Scholar 

  39. L.L. Rokhlin, N.I. Nitikina, T.V. Dobatkina, J. Alloy. Compd. 239, 209 (1996)

    Article  CAS  Google Scholar 

  40. G. Sha, Y.B. Wang, X.Z. Liao, Z.C. Duan, S.P. Ringer, T.G. Langdon, Acta Mater. 57, 3123 (2009)

    Article  CAS  Google Scholar 

Download references

Acknowledgements

This work is supported by National Natural Science Foundation of China through Projects No. 51571084 and No. 51171059).

Author information

Authors and Affiliations

  1. School of Material Science and Engineering, Henan University of Science and Technology, Luoyang, 471023, China

    L. P. Yan, Q. A. Li & X. Y. Chen

  2. Provincial and Ministerial Co-construction of Collaborative Innovation Center for Non-Ferrous Metal New Materials and Advanced Processing Technology, Luoyang, 471023, China

    Q. A. Li

Authors
  1. L. P. Yan
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Q. A. Li
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. X. Y. Chen
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Q. A. Li.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Yan, L.P., Li, Q.A. & Chen, X.Y. Microstructure Evolution and Dynamic Precipitation Behavior of Mg–10Gd–4Y–1Sm–0.5Zr Alloy During Backward Hot Extrusion. Met. Mater. Int. 27, 3522–3528 (2021). https://doi.org/10.1007/s12540-020-00661-5

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s12540-020-00661-5

Keywords

Search

Navigation