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Electroless Deposition: A Superficial Route to Synthesis of Highly Conductive Electrospun Nylon 6 Nanofibers

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Abstract

In this study, we report the synthesis of conductive Nylon 6 nanofibers (N6 NFs) using the electroless deposition (ELD) method. We fabricated the N6 NFs by electrospinning technique and modified the surface with [2-(methacryloyloxy) ethyl] trimethylammonium chloride (PMETAC). After surface modification of N6 NFs, copper metal was successfully deposited using the ELD process. Parameters including time, temperature, volume, and pH concentration were optimized for copper deposition. SEM images revealed smooth morphology of neat N6 NFs and copper-coated N6 NFs. EDX spectrum was performed on neat N6 NFs and copper-coated N6 NFs to ensure the qualitative and quantitative presence of copper nanoparticles. Furthermore, advance characterization methods such as FTIR, XPS, water contact angle, and tensile strength were performed to analyze the successful copper deposition on N6 NFs.

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References

  1. Y. Xu, K. Qian, D. Deng, L. Luo, J. Ye, H. Wu, and X. Feng, Carbohydr. Polym., 250, 116915 (2020).

    Article  CAS  PubMed  Google Scholar 

  2. A. Schwarz, J. Hakuzimana, A. Kaczynska, J. Banaszczyk, P. Westbroek, E. McAdams, and D. Tseles, Surf. Coat. Technol., 204, 1412 (2010).

    Article  CAS  Google Scholar 

  3. T. Kim and D. Kwak, Fiber. Polym., 13, 471 (2012).

    Article  CAS  Google Scholar 

  4. Y. Kim, Y. Song, and H. Kim, Fiber. Polym., 20, 466 (2019).

    Article  CAS  Google Scholar 

  5. E. Gasana, P. Westbroek, J. Hakuzimana, K. De Clerck, G. Priniotakis, P. Kiekens, and D. Tseles, Surf. Coat. Technol., 201, 3547 (2006).

    Article  CAS  Google Scholar 

  6. J. Jang and S. K. Ryu, J. Mater. Proc. Technol., 180, 66 (2006).

    Article  CAS  Google Scholar 

  7. P. A. Pandey, G. R. Bell, J. P. Rourke, A. M. Sanchez, M. D. Elkin, B. J. Hickey, and N. R. Wilson, J. Nano. Micro Small, 22, 3202 (2011).

    Google Scholar 

  8. A. Ponti, M. H. Raza, F. Pantò, A. M. Ferretti, C. Triolo, S. Patanè, and S. Santangelo, J. Langmuir, 36, 1305 (2020).

    Article  CAS  Google Scholar 

  9. Z. H. Ma, K. L. Tan, and E. T. Kang, J. Synth. Metal., 114, 17 (2000).

    Article  CAS  Google Scholar 

  10. R. H. Guo, S. X. Jiang, C. W. M. Yuen, M. C. F. Ng, J. W. Lan, and G. H. Zheng, Fiber. Polym., 13, 1037 (2012).

    Article  CAS  Google Scholar 

  11. R. H. Guo, S. X. Jiang, C. W. M. Yuen, M. C. F. Ng, J. W. Lan, Y. L. Yeung, and S. J. Lin, Fiber. Polym., 14, 752 (2013).

    Article  CAS  Google Scholar 

  12. S. Liang, Y. Li, T. Zhou, J. Yang, X. Zhou, T. Zhu, and C. He, Adv. Sci., 4, 1600313 (2017).

    Article  Google Scholar 

  13. Z. Liu, H. Hu, B. Yu, M. Chen, Z. Zheng, and F. Zhou, Electrochem. Commun., 11, 492 (2009).

    Article  CAS  Google Scholar 

  14. X. Cauchy, J. E. Klemberg-Sapieha, and D. Therriault, ACS Appl. Mater. Interf., 9, 29010 (2017).

    Article  CAS  Google Scholar 

  15. Y. Yu, C. Yan, and Z. Zheng, Adv. Mater., 26, 5508 (2014).

    Article  CAS  PubMed  Google Scholar 

  16. L. Petrik, Æ. P. Ndungu, and Æ. E. Iwuoha, J. Nanoscale Res. Lett., 5, 38 (2010).

    Article  CAS  Google Scholar 

  17. N. A. M. Barakat, M. A. Kanjwal, F. A. Sheikh, and H. Y. Kim, Polymer(Guildf), 50, 4389 (2009).

    CAS  Google Scholar 

  18. L. Sumin, D. Kimura, K. H. Lee, J. C. Park, and I. S. Kim, Text. Res. J., 80, 99 (2010).

    Article  CAS  Google Scholar 

  19. S. Ullah, M. Hashmi, D. Kharaghani, M. Q. Khan, Y. Saito, T. Yamamoto, J. Lee, and I. S. Kim, Int. J. Nanomed., 14, 2693 (2019).

    Article  CAS  Google Scholar 

  20. A. W. Jatoi, Jatoi, F. Ahmed, M. Khatri, A. Tanwari, Z. Khatri, H. Lee, and I. K. Kim, Ultrason. Sonochem., 39, 34 (2017).

    Article  CAS  PubMed  Google Scholar 

  21. X. Wang, C. Yan, H. Hu, X. Zhou, R. Guo, X. Liu, X. Xie, Z. Huang, and Z. Zheng, J. Chem.-An Asian, 9, 2170 (2014).

    Article  CAS  Google Scholar 

  22. G. S. Chen, R. J. Tau, J. S. Fang, Y. L. Cheng, and Y. C. Chen, Appl. Surf. Sci., 527, 146816 (2020).

    Article  CAS  Google Scholar 

  23. Y. Shacham-Diamand, V. Dubin, and M. Angyal, J. Thin Solid Films, 262, 93 (1995).

    Article  CAS  Google Scholar 

  24. U. A. Qureshi, Z. Khatri, F. Ahmed, A. S. Ibupoto, M. Khatri, F. K. Mahar, and I. S. Kim, J. Mol. Liq., 244, 478 (2017).

    Article  CAS  Google Scholar 

  25. L. A. Díaz-Alejo, E. C. Menchaca-Campos, J. Uruchurtu Chavarín, R. Sosa-Fonseca, and M. A. García-Sánchez, Int. J. Polym. Sci., https://doi.org/10.1155/2013/323854(2013).

  26. L. Liu, Y. Yu, C. Yan, K. Li, and Z. Zheng, Nat. Commun., 6, 1 (2015).

    CAS  Google Scholar 

  27. X. Gan, Y. Wu, L. Liu, B. Shen, and W. Hu, Surf. Coat. Technol., 201, 7018 (2007).

    Article  CAS  Google Scholar 

  28. X. Li, Y. Li, T. Guan, F. Xu, J. Sun, and J. Durable, ACS Appl. Mater. Interf., 10, 12042 (2018).

    Article  CAS  Google Scholar 

  29. A. Demir, E. Bozaci, T. Gülümser, and M. Sarikanat, Tekstil ve Konfeksiyon, 26, 256 (2016).

    Google Scholar 

  30. C. Wang, H. Yang, F. Chen, L. Peng, H.-F. Gao, and L.-P. Zhao, Results in Phys., 10, 891 (2018).

    Article  Google Scholar 

  31. N. Politakos, S. Azinas, and S. E. Moya, Macromol. Rapid Commun., 37, 662 (2016).

    Article  CAS  PubMed  Google Scholar 

  32. S. Liu, M. Hu, and J. Yang, J. Mater. Chem. C, 4, 1320 (2016).

    Article  CAS  Google Scholar 

  33. A. J. Wagner, G. M. Wolfe, and D. H. Fairbrother, Appl. Surf. Sci., 219, 317 (2003).

    Article  CAS  Google Scholar 

  34. F. K. Mahar, M. Mehdi, U. A. Qureshi, K. M. Brohi, B. Zahid, F. Ahmed, and Z. Khatri, J. Mol. Liq., 248, 911 (2017).

    Article  CAS  Google Scholar 

  35. K. Wei, T. Ohta, B. S. Kim, K. W. Kim, K. H. Lee, M. S. Khil, and I. S. Kim, Polym. Adv. Technol., 21, 746 (2010).

    Article  CAS  Google Scholar 

  36. H. Bak, S. Y. Cho, Y. S. Yun, and H. J. Jin, Current Appl. Phys., 10, S468 (2010).

    Article  Google Scholar 

  37. M. Havel, K. Behler, G. Korneva, and Y. Gogotsi, Adv. Funct. Mater., 18, 2322 (2008).

    Article  CAS  Google Scholar 

  38. Y. L. Huang, A. Baji, H. W. Tien, Y. K. Yang, S. Y. Yang, C. C. M. Ma, H. Y. Liu, Y. W. Mai, and N. H. Wang, Nanotechnology, 22, 475603 (2011).

    Article  PubMed  Google Scholar 

  39. D. M. Mihut, K. Lozano, and H. Foltz, J. Vac. Sci. Technol. A: Vacuum, Surfaces, and Films, 32, 061401 (2014).

    Article  Google Scholar 

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Hussain, N., Yousif, M., Mehdi, M. et al. Electroless Deposition: A Superficial Route to Synthesis of Highly Conductive Electrospun Nylon 6 Nanofibers. Fibers Polym 23, 680–689 (2022). https://doi.org/10.1007/s12221-022-3288-z

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  • DOI: https://doi.org/10.1007/s12221-022-3288-z

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