Abstract
Agave fibers were extracted mechanically without the use of solvents or water, through a lyophilization-assisted method. Then, the internal arrangement of the fibrils was studied in order to elaborate a hierarchical growing model, using this information to explain the outstanding properties of these natural fibers. We found that the lyophilized fibers have an initial modulus of 36.7 g/den, a breaking tenacity of 1.45 g/den and an elongation of 17 %, while the fibers washed with water after extraction presented a similar value of initial modulus (31.1 g/den), but the breaking tenacity (2.59 g/den), and the elongation (34 %) increased nearly two times, showing the embrittling effect of the freeze-drying on the fibers behavior.
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J. T. Kuttruff, S. G. DeHart, and M. J. O’Brien, Science, 281, 72 (1998).
P. Colunga-Garcia, A. Larqué, L. Eguiarte, and D. Zizumbo-Villarreal, “En lo ancestral hay futuro: del tequila, los mezcales y otros agaves”, p.304, Conabio, México, 2007.
A. Bismarck, A. K. Mohanty, I. Aranberri-Askargorta, S. Czapla, M. Misra, G. Hinrichsen, and J. Springer, Green Chem., 3, 100 (2001).
L. Chávez-Guerrero, S. Sepúlveda-Guzmán, J. Silva-Mendoza, C. Aguilar-Flores, and O. Pérez-Camacho, Carbohydr. Polym., 181, 642 (2018).
L. Chávez-Guerrero and M. Hinojosa, Fuel, 89, 4049 (2010).
G. Iñiguez-Covarrubias, S. E. Lange, and R. M. Rowell, Bioresour. Technol., 77, 25 (2001).
J. R. González-López, J. F. Ramos-Lara, A. Zaldivar-Cadena, L. Chávez-Guerrero, R. X. Magallanes-Rivera, and O. Burciaga-Díaz, Fuel Process. Technol., 133, 35 (2015).
L. Chávez-Guerrero, J. A. Salinas-Montelongo, and A. Esquivias-Fierro, Mater. Lett., 221, 220 (2018).
J. R. Aguirre Rivera, H. Charcas Salazar, and J. L. Flores Flores, “El maguey Mezcalero Potosino”, COPOCyT Gobierno del estado de San Luis Potosí, México, 2001.
A. Bunde and S. Havlin, “Fractals in Science”, pp.23–89, Springer-Verlag, Germany, 1994.
D’Arcy Thompson, “On Growth and Form”, pp.23–226, Cambrigde University Press, United Kingdom, 1961.
M. E. Alves Fidelis, T. V. Castro Pereira, O. da Fonseca Martins Gomes, F. de Andrade Silva, and R. D. Toledo Filho, J. Mater. Res. Technol., 2, 149 (2013).
H. M. Hernández-Hernández, J. J. Chanona-Pérez, A. Vega, Pablo Ligero, R. R. Farrera-Rebollo, J. A. Mendoza-Pérez, G. Calderón-Domínguez, and N. Güemes Vera, Microsc. Microanal., 22, 1084 (2016).
M. Jaouadi, S. M’sahli, and F. Sakli, Text. Res. J., 79, 110 (2009).
C. Gómez Hoyos, V. A. Alvarez, P. Gañán Rojo, and A. Vázquez, Fiber. Polym., 13, 632 (2012).
Y. Chaabouni, J. Y. Drean, S. Msahli, and F. Sakli, Text. Res. J., 76, 367 (2006).
J. T. Corredor González, A. J. Pinheiro Dillon, A. R. Pérez-Pérez, R. Fontana, and C. Pérez Bergmann, Fiber. Polym., 16, 2112 (2015).
K. L. Pickering, M. G. Aruan Efendy, and T. M. Le, Compos. Part A-Appl. Sci. Manuf., 83, 98 (2016).
A. El Oudiani, Y. Chaabouni, S. Msahli, and F. Sakli, Text. Res. J., 78, 631 (2008).
M. Shahid, F. Mohammad, G. Chen, R. C. Tang, and T. Xing, Green Chem., 18, 2256 (2016).
L. Segal, J. J. Creely, A. E. Martin, and C. M. Conrad, Text. Res. J., 29, 786 (1959).
J. M. Ouyang and S. P. Deng, Dalton Trans., 2846 (2003).
J. A. Perez-Pimienta, M. G. Lopez-Ortega, J. A. Chavez-Carvayar, P. Varanasi, V. Stavila, G. Cheng, S. Singh, and B. A. Simmons, Biomass Bioenergy, 75, 180 (2015).
M. M. Kerssens, P. Matousek, K. Rogers, and N. Stone, Analyst, 135, 3156 (2010).
L. Chávez-Guerrero, J. Silva-Mendoza, S. Sepúlveda-Guzmán, N. A. Medina-Aguirre, S. Vazquez-Rodriguez, M. E. Cantú-Cárdenas, and N. A. García-Gómez, Carbohydr. Polym., 210, 85 (2019).
M. Hidalgo-Reyes, M. Caballero-Caballero, L. H. Hernández-Gómez, and G. Urriolagoitia-Calderón, Bot. Sci., 93, 807 (2015).
S. Msahli, Y. Chaabouni, S. Faouzi, and J. Y. Drean, J. Appl. Sci., 7, 3951 (2007).
A. El Oudiani, B. Sghaier, S. Msahli, Y. Chaabouni, and F. Sakli, Text. Res. J., 79, 166 (2009).
T. Huber, J. Müssig, O. Curnow, S. Pang, S. Bickerton, and M. P. Staiger, J. Mater. Sci., 47, 1171 (2012).
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Chávez-Guerrero, L., Esneider, M., Bonilla, J. et al. Eco-friendly Extraction of Fibrils with Hierarchical Structure Assisted by Freeze-Drying Using Agave Salmiana Leaves as a Raw Material. Fibers Polym 21, 66–72 (2020). https://doi.org/10.1007/s12221-020-9078-6
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DOI: https://doi.org/10.1007/s12221-020-9078-6