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Natural dyeing with black cowpea seed coat. I. Dyeing properties of cotton and silk fabrics

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Abstract

A new trial to determine the dyeing properties of cotton and silk fabrics with a black cowpea seed coat as crop waste was investigated. The natural dye anthocyanins were extracted from a black cowpea seed coat in an aqueous solution and used to dye silk and cotton. The optimal conditions for colorant extraction were an aqueous solution of a dried seed coat of black cowpea in a 1:10 liquor ratio at 70 °C for 4 hours with pH of 4. The best dye-uptake of silk and cotton fabric were obtained when the pH was 3.5 and 3.0 respectively, the temperature was 80 °C for 1 hour and the liquor ratio of black cowpea was 1:20. Different colors as dusky brown, brown, faint yellow, light green, reddish brown, cyan and green could be obtained using a various kind of mordants. The depth and brightness of color tones were affected by different dyeing and mordanting pH conditions. The colors of the fabrics were examined using a computer color matching system in terms of the K/S values and CIELAB color-difference values. The dyeing was evaluated using standard light, wash and heat fastness tests. Good wash and heat fastness were obtained but the poor light fastness indicated the need for improvement to fulfill the requirement for textile applications.

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References

  1. B. H. Patel, B. J. Agarwal, and H. M. Patel, Colourage, 1, 21 (2003).

    Google Scholar 

  2. T. Becjtold, A. Mahmund-Ali, and B. Mussak, Dyes Pigments, 75, 287 (2007).

    Article  Google Scholar 

  3. R. Shankar and P. Vanker, Dyes Pigments, 74, 464 (2007).

    Article  Google Scholar 

  4. P. Vanker, R. Shankar, D. Mahanta, and C. C. Tiwavi, Dyes Pigments, 76, 207 (2008).

    Article  Google Scholar 

  5. H. Oda, Color Technol., 117, 204 (2001).

    Article  CAS  Google Scholar 

  6. C. E. Garland, “Color Technology in Textile Chemistry”, Inc. Gultekin Ed. AATCC, 1993.

    Google Scholar 

  7. Y. Choia, H. Jeonga, and J. Lee, Food Chemistry, 103, 130 (2007).

    Article  Google Scholar 

  8. G. W. Taylor, Rev. Prog. Coloration, 16, 53 (1986).

    Article  CAS  Google Scholar 

  9. El-Gamal, Tinctroria, 95, 48 (1998).

    CAS  Google Scholar 

  10. S. R. Kim, Y. S. Ahn, Y. B. Oh, M. N. Jung, and B. C. Jung, Korean Patent Appl. KR 2000-41654, 2000.

    Google Scholar 

  11. C. H. Chae and P. H. Choung, Korean Patent Appl KR 2000-47706, 2000.

    Google Scholar 

  12. J. J. Moses and N. Ravi, Man-made Textiles in India, 46, 295 (2003).

    CAS  Google Scholar 

  13. J. K. Chavon, S. S. Kadam, and D. K. Salunkhe, “Cowpea, in and Book of World Food Legumes”, Eds., CRC Press, Boca Raton, FL, 1989.

  14. T. Bechtold, R. Mussak, A. Mahmud-ali, E. Gannglberger, and S. Geissler, J. Sci. Food Agric., 86, 233 (2006).

    Article  CAS  Google Scholar 

  15. T. Bechtold, A. Mahmud-ali, and R. Mussak, J. Sci. Food Agric., 87, 2589 (2007).

    Article  CAS  Google Scholar 

  16. E. E. Burns and J. W. Winzer, Proc. Am. Soc. Hortic. Sci., 80, 449 (1962).

    CAS  Google Scholar 

  17. W. H. Culver and R. F. Cain, Tex. Agri. Exp. Stn. Bull., 748, 5 (1952).

    CAS  Google Scholar 

  18. T. J. Ha, M. H. Lee, Y. N. Jeong, J. H. Lee, S. I. Han, C. H. Park, S. B. Pae, C. H. Hwang, I. Y. Baek, and K. Y. Park, Food Sci. Biotechnol. 19, 821 (2010).

    Article  CAS  Google Scholar 

  19. G. Mazza and E. Miniati, “Anthocyanins in Fruits, Vegetables, and Grains”, CRC Press, Boca Raton, FL, 1993.

    Google Scholar 

  20. F. S. Hosseinian and T. Beta, J. Agric. Food Chem., 55, 10832 (2007).

    Article  CAS  Google Scholar 

  21. R. L. Prior and X. Wu, Free Radical Research, 40, 1014 (2006).

    Article  CAS  Google Scholar 

  22. R. Brouillard, “Chemical Structure of Anthocyanins as Food Colors” (P. Markakis Ed.), Academic Press, New York, 1982.

  23. G. Mazza and R. Brouillard, J. Agric. Food Chem., 35, 422 (1987).

    Article  CAS  Google Scholar 

  24. P. Kubelka, JOSA 38, 448 (1948).

    Article  CAS  Google Scholar 

  25. P. Kubelka, JOSA 44, 330 (1954).

    Article  Google Scholar 

  26. E. Sashina, A. Bochek, and N. Novoselov, Russian J. Appl. Chem., 79, 869 (2006).

    Article  CAS  Google Scholar 

  27. C. Kan, Fiber. Polym., 9, 317 (2008).

    Article  CAS  Google Scholar 

  28. A. Cheminat and R. Brouillard, Tetrahedron Lett. 27, 4457, Pergamon Press, Ltd., 1986.

    Article  CAS  Google Scholar 

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Correspondence to Do Gyu Bae.

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Jung, Y.S., Bae, D.G. Natural dyeing with black cowpea seed coat. I. Dyeing properties of cotton and silk fabrics. Fibers Polym 15, 138–144 (2014). https://doi.org/10.1007/s12221-014-0138-7

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  • DOI: https://doi.org/10.1007/s12221-014-0138-7

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