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Experimental investigation and finite element simulation of the effect of surface roughness on nanoscratch testing

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Abstract

Nanoscratch testing is a highly reliable method used to extract a variety of film properties. It is proven that many of the experimental factors can influence the obtained results, such as the probe tilt, the scratch depth, etc. On the other hand, the surface roughness of the samples is an important parameter in nanoscratch and other similar tests, including the nanoindentation test. Thus, the effect of surface roughness on both the nanoscratch experiments and finite element simulations has been investigated. By performing scratch tests on gold and copper films and carrying out the finite element (FE) simulations on the rough and smooth surfaces, the importance of surface morphology was studied. The results indicate that the FE models consisting of the films with rough surfaces can lead to more accurate results, compatible with the experimental data. It was also revealed that the impact of surface morphology on the extracted friction coefficient tends to lose its significance in higher scratch depths. However, comparing the experimental results and simulation data, at lower scratch depths due to the presence of van der Waals forces the FE simulations will not lead to precise results.

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References

  1. Y. Sun, T. Bell and S. Zheng, Finite element analysis of the critical ratio of coating thickness to indentation depth for coating property measurements by nanoindentation, Thin Solid Films, 258 (1–2) (1995) 198–204.

    Article  Google Scholar 

  2. European Standard EN ISO 14577-1, Metallic materials, Instrumented indentation test for hardness and materials parameters, Part 1: Test method (2015).

  3. K. D. Bouzakis, N. Michailidis, S. Hadjiyiannis, G. Skordaris and G. Erkens, The effect of specimen roughness and indenter tip geometry on the determination accuracy of thin hard coatings stress-strain laws by nanoindentation, Materials Characterization, 49 (2002) 149–156.

    Article  Google Scholar 

  4. S. R. Pergande, A. A. Polycarpou and T. F. Conry, Use of nano-indentation and nano-scratch techniques to investigation near surface material properties associated with scuffing of engineering surface, ACRC TR-193, University of Illinois (2002).

    Google Scholar 

  5. H. Xie, J. Mead, S. Wang and H. Huang, The effect of surface texture on the kinetic friction of a nanowire on a substrate, Scientific Reports, 7 (2017) 44907.

    Article  Google Scholar 

  6. B. D. Beake, A. A. Ogwu and T. Wagner, Influence of experimental factors and film thickness on the measured critical load in the nanoscratch test, Materials Science and Engineering: A, 423 (1) (2006) 70–73.

    Article  Google Scholar 

  7. S. Lafaye and M. Troyon, On the friction behaviour in nanoscratch testing, Wear, 261 (7–8) (2006) 905–913.

    Article  Google Scholar 

  8. N. Tayebi, A. A. Polycarpou and T. F. Conry, Effects of substrate on determination of hardness of thin films by nanoscratch and nanoindentation techniques, J. of Materials Research, 19 (6) (2004) 1791–1802.

    Article  Google Scholar 

  9. Y. D. Yan, T. Sun and S. Dong, Study on effects of tip geometry on AFM nanoscratching tests, Wear, 262 (3–4) (2007) 477–483.

    Article  Google Scholar 

  10. Y. Geng, J. Zhang, Y. Yan, B. Yu, L. Geng and T. Sun, Experimental and theoretical investigation of crystallographic orientation dependence of nanoscratching of single crystalline copper, PLoS ONE, 10 (7) (2015) e0131886.

    Article  Google Scholar 

  11. J. Fu, S. Kamali-Bernard, F. Bernard and M. Cornen, Comparison of mechanical properties of CSH and portlandite between nano-indentation experiments and a modelling approach using various simulation techniques, Composites Part B: Engineering, 151 (2018) 127–138.

    Article  Google Scholar 

  12. M. Chamani, G. H. Farrahi and M. R. Movahhedy, Friction behavior of nanocrystalline nickel near the Hall-Petch breakdown, Tribology International, 107 (2017) 18–24.

    Article  Google Scholar 

  13. C. Shi, H. Zhao, H. Huang, S. Wan, Z. Ma, C. Geng and L. Ren, Effects of probe tilt on nanoscratch results: An investigation by finite element analysis, Tribology International, 60 (2013) 64–69.

    Article  Google Scholar 

  14. A. Chatterjee, A. A. Polycarpou, J. R. Abelson and P. Bellon, Nanoscratch study of hard HfB2 thin films using experimental and finite element techniques, Wear, 268 (5–6) (2010) 677–685.

    Article  Google Scholar 

  15. S. Roy, E. Darque-Ceretti, E. Felder, F. Raynal and I. Bispo, Experimental analysis and finite element modelling of nano-scratch test applied on 40–120 nm SiCN thin films deposited on Cu/Si substrate, Thin Solid Films, 518 (2010) 3859–3865.

    Article  Google Scholar 

  16. H. R. Chamani and M. R. Ayatollahi, The effect of Berkovich tip orientations on friction coefficient in nano-scratch testing of metals, Tribology International, 103 (2016) 25–36.

    Article  Google Scholar 

  17. H. R. Chamani and M. R. Ayatollahi, Prediction of friction coefficients in nanoscratch testing of metals based on material flow lines, Theoretical and Applied Fracture Mechanics, 94 (2018) 186–196.

    Article  Google Scholar 

  18. R. Hu, C. Prakash, V. Tomar, M. Harr, I. E. Gunduz and C. Oskay, Experimentally-validated mesoscale modeling of the coupled mechanical-thermal response of AP-HTPB energetic material under dynamic loading, International J. of Fracture, 203 (1) (2017) 277–298.

    Article  Google Scholar 

  19. A. Wagih and A. Fathy, Experimental investigation and FE simulation of nano-indentation on Al-Al2O3 nanocomposites, Advanced Powder Technology, 27 (2) (2016) 403–410.

    Article  Google Scholar 

  20. C. H. Sacre, F. Lani, P. Guaino, L. Libralesso, A. Favache and T. Pardoen, Effect of polymer interlayer on scratch resistance of hard film, Experiments and finite element modeling, Wear, 378 (2017) 136–144.

    Article  Google Scholar 

  21. W. C. Oliver and G. M. Pharr, An improved technique for determining hardness and elastic-modulus using load and displacement sensing indentation experiments, J. of Materials Research, 7 (1992) 1564–1583.

    Article  Google Scholar 

  22. S. H. Hong, K. S. Kim, Y. M. Kim, J. H. Hahn, C. S. Lee and J. H. Park, Characterization of elastic moduli of Cu thin films using nanoindentation technique, Composites Science and Technology, 65 (9) (2005) 1401–1408.

    Article  Google Scholar 

  23. E. T. Lilleodden, J. A. Zimmerman, S. M. Foiles and W. D. Nix, Atomistic simulations of elastic deformation and dislocation nucleation during nanoindentation, J. of the Mechanics and Physics of Solids, 51 (5) (2003) 901–920.

    Article  MATH  Google Scholar 

  24. D. Tabor, The Hardness of Metals, 1st Ed., Oxford Clarendon Press (1951).

    Google Scholar 

  25. A. C. Fischer-Cripps, Nanoindentation, 2st Edition, Mechanical Engineering Series, Springer (2011).

    Book  Google Scholar 

  26. A. F. Jankowski and H. T. Ahmed, The nanoscratch hardness of a gold-nickel nanocrystalline nanolaminate at high strain rate, Materials Letters, 77 (2012) 103–106.

    Article  Google Scholar 

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Correspondence to Mohammad Chamani.

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Recommended by Associate Editor Dong-Weon Lee

M. Nazemian received his M.Sc. in Mechanical Engineering at Sharif University of technology in 2014. His major research interests are numerical methods, fatigue and fracture mechanics, nanomechanics and materials science.

M. Chamani received his Ph.D. in Mechanical Engineering at Sharif University of technology in 2016. His core research interests include nanotechnology, molecular dynamics and wind turbine. He is working as a researcher at Niroo Research Institute.

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Nazemian, M., Chamani, M. Experimental investigation and finite element simulation of the effect of surface roughness on nanoscratch testing. J Mech Sci Technol 33, 2331–2338 (2019). https://doi.org/10.1007/s12206-019-0432-9

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  • DOI: https://doi.org/10.1007/s12206-019-0432-9

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