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Potential Typicality Marker of Volatile Composition of Commercial Sparkling Wines from the Caatinga Biome

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Abstract

The present research aimed to identify the volatile profile of sparkling wines from São Francisco Valley, which products will have soon the Geographical Indication requested by the producers. Volatile organic compounds from muscat, brut, brut rosé and demi-sec sparkling wines produced in the São Francisco Valley, located in the Caatinga region of Brazil, were extracted, separated and identified using the HS-SPME/GC–MS technique. The results reached the identification of a total of 109 compounds, classified in 13 chemical groups, being the main esters, terpenes, and alcohols. It was found that some compounds with expressive area are unique to each type of sparkling wine: a total of 23 in muscat, 9 in brut, 5 in brut rosé, and 4 in demi-sec. This suggests a strong association between the grape varieties and the technological processes of winemaking. The volatile profiles of each commercial sparkling wine in the São Francisco Valley present possible chemical markers of typicity which can be used to distinguish the commercial wines from the region.

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Data Availability

The datasets generated during and/or analysed during the current study are available from the corresponding author on reasonable request.

References

  • Arcanjo NMO, Bezerra TKA, da Silva FLH, Madruga MS (2015) Optimization of the HS-SPME-GC/MS technique for determining volatile compounds in red wines made from Isabel grapes (Vitis labrusca). Food Sci Technol 35(4):676–682

    Article  Google Scholar 

  • Arcanjo NMO, da Oliveira MES, daAraújo ÍBS, da Silva FLH, Madruga MS (2018) Red wine produced from the Isabella and Ives cultivar (Vitis Labrusca): Profile of volatiles and aroma descriptors. Food Sci Technol 38(2):271–279

    Article  Google Scholar 

  • Arias I, Lacau B, Astrain J, Barón C, Fenandez-Zurbano P, Ferreira V, Escudero A (2019) Effects of vineyard ‘potential’ and grape maturation on the aroma-volatile profile of Grenache wines. Oeno One 53(4):695–707

    Google Scholar 

  • Barbará JA, Nicolli KP, Souza-Silva ÉA, Biasoto ACT, Welke JE, Zini CA (2020) Volatile profile and aroma potential of tropical Syrah wines elaborated in different maturation and maceration times using comprehensive two-dimensional gas chromatography and olfactometry. Food Chem 308:125552

    Article  Google Scholar 

  • Barros EP, Moreira N, Pereira GE, Leite SGF, Rezende CM, de Pinho PG (2012) Development and validation of automatic HS-SPME with a gas chromatography-ion trap/mass spectrometry method for analysis of volatiles in wines. Talanta 101:177–186

    Article  Google Scholar 

  • Bellincontro A, Matarese F, D’Onofrio C, Accordini D, Tosi E, Mencarelli F (2016) Management of postharvest grape withering to optimise the aroma of the final wine: A case study on Amarone. Food Chem 213:378–387

    Article  CAS  PubMed  Google Scholar 

  • Benedetti MM, Curi N, Sparovek G, de Filho A, C., & Silva, S. H. G. (2011) Updated Brazilian’s Georeferenced Soil Database – an improvement for International Scientific Information Exchanging. Embrapa 1:309–332

    Google Scholar 

  • Bordiga M, Rinaldi M, Locatelli M, Piana G, Travaglia F, Coïsson JD, Arlorio M (2013) Characterization of Muscat wines aroma evolution using comprehensive gas chromatography followed by a post-analytic approach to 2D contour plots comparison. Food Chem 140(1–2):57–67

    Article  CAS  PubMed  Google Scholar 

  • Brasil (2004) Lei No 10.970, de 12 de novembro de 2004. Diário Oficial Da União

  • Caliari V, Panceri CP, Rosier JP, Bordignon-Luiz MT (2015) Effect of the Traditional, Charmat and Asti method production on the volatile composition of Moscato Giallo sparkling wines. LWT-Food Science and Technology 61(2):393–400

    Article  CAS  Google Scholar 

  • Capone DL, Jeffery DW, Sefton MA (2012) Vineyard and fermentation studies to elucidate the origin of 1,8-cineole in Australian red wine. J Agric Food Chem 60(9):2281–2287

    Article  CAS  PubMed  Google Scholar 

  • Coelho E, Rocha SM, Delgadillo I, Coimbra MA (2006) Headspace-SPME applied to varietal volatile components evolution during Vitis vinifera L. cv. “Baga” ripening. Analytica Chimica Acta 563(1–2):204–214

    Article  CAS  Google Scholar 

  • de Macêdo Morais S, de Sousa Galvão M, Olegario LS, de Carvalho LM, Pereira GE, de Andrade Lima LL, Madruga MS (2022) Identification of chemical markers of commercial tropical red wine candidates for the São Francisco Valley Geographical Indication. Food Anal Methods 1–19

  • Embrapa (2020) Indicações Geográficas de Vinhos do Brasil. https://www.embrapa.br/uva-e-vinho/indicacoes-geograficas-de-vinhos-do-brasil. Accessed 15 Aug 2020

  • Étievant PX (1991) Volatile compounds in foods and beverages. M. Dekker (Ed.), (1st ed.)

  • Fan W, Qian MC (2005) Headspace solid phase microextraction and gas chromatography olfactometry dilution analysis of young and aged Chinese “Yanghe Daqu” liquors. J Agric Food Chem 53:7931–7938

    Article  CAS  PubMed  Google Scholar 

  • Fan W, Xu Y, Jiang W, Li J (2010) Identification and quantification of impact aroma compounds in 4 nonfloral Vitis vinifera varieties grapes. J Food Sci 75:81–88

    Article  Google Scholar 

  • Fernandes NCM, Gomes F de CO, Garcia CF, Vieira M de LA, and Machado AM de R (2018) Use of solid phase microextraction to identify volatile organic compounds in brazilian wines from different grape varieties. Brazilian J Food Technol 21

  • Ferreira V, Ortín N, Escudero A, López R, Cacho J (2002) Chemical characterization of the aroma of Grenache rose wines: aroma extract dilution analysis, quantitative determination, and sensory reconstitution studies. J Agric Food Chem 50(14):4048–4054

    Article  CAS  PubMed  Google Scholar 

  • Gong M, Zhou Z, Yu Y, Liu S, Zhu S, Jian D, Cui P, Zhong F, and Mao J (2020) Investigation of the 5-hydroxymethylfurfural and furfural content of Chinese traditional fermented vinegars from different regions and its correlation with the saccharide and amino acid content. LWT, 124

  • Ibravin (2020a). Panorama Geral. https://www.ibravin.org.br/Panorama-Geral. Accessed 15 Aug 2020

  • Ibravin. (2020b) Regiões produtoras. https://www.ibravin.org.br/Regioes-Produtoras. Accessed 15 Aug 2020

  • Jackson RS (2008) Wine Science: Principles and Applications, Third Edition (3rd ed) San Diego: academic press

  • Jackson RS (2020) Wine sciene: principles and applications (5th ed.). Academic Press

  • Jagatić Korenika AM, Preiner D, Tomaz I, Jeromel A (2020) Volatile profile characterization of Croatian commercial sparkling wines. Molecules 25(18):4349

    Article  PubMed Central  Google Scholar 

  • Jiang B, Xi Z, Luo M, Zhang Z (2013) Comparison on aroma compounds in Cabernet Sauvignon and Merlot wines from four wine grape-growing regions in China. Food Res Int 51(2):482–489

    Article  CAS  Google Scholar 

  • Komes D, Ulrich D, Lovric T (2006) Characterization of odor-active compounds in Croatian Rhine Riesling wine, subregion Zagorje. Eur Food Res Technol 222(1):1–7

    Article  CAS  Google Scholar 

  • Kondjoyan N, Berdagué J-L (1996) A compilation of relative retention indices for the analysis of aromatic compounds. du Laboratoire Flaveur

  • Lambrechts MG, Pretorius IS (2000) Yeast and its importance to wine aroma - a review. South African J Enol Vitic 21(1)

  • Lampír L, Pavlousek P (2013) Influence of locality on content of phenolic compounds in white wines. Czech Journal Food Science 31(6):619–626

    Article  Google Scholar 

  • Lukic I, Horvat I (2017) Differentiation of commercial PDO wines produced in istria (croatia) according to variety and harvest year based on HS-SPME-GC/MS volatile aroma compound profi ling. Food Technology and Biotechnology 55(1):95–108

    Article  CAS  PubMed  PubMed Central  Google Scholar 

  • Marcon ÂR, Delamare APL, Schwarz LV, Pasini L, Versari A, Parpinello GP, Echeverrigaray S (2021) Volatile and sensory composition of Brazilian Muscat sparkling wine and Asti. J Food Process Preserv 45(4):e15240

    Article  CAS  Google Scholar 

  • Martínez-García R, García-Martínez T, Puig-Pujol A, Mauricio JC, Moreno J (2017) Changes in sparkling wine aroma during the second fermentation under CO2 pressure in sealed bottle. Food Chem 237:1030–1040

    Article  PubMed  Google Scholar 

  • Muñoz-Redondo JM, Ruiz-Moren, MJ, Puertas B, Cantos-Villar E, and Moreno-Rojas JM (2020) Multivariate optimization of headspace solid-phase microextraction coupled to gas chromatography-mass spectrometry for the analysis of terpenoids in sparkling wines. Talanta 208

  • Nan L, Guo M, Chen S, Li Y, Cui C, Song Y, Huang J, Wine R (2019) Effect of peduncle on aroma of cabernet sauvignon dry red wine effect of Peduncle on Aroma of Cabernet Sauvignon Dry. International Conf Biotechnol Bioeng 2079(1):020008

    Google Scholar 

  • Nascimento AS, de Souza J, dos Lima M, S., & Pereira, G. E. (2018) Volatile profiles of sparkling wines produced by the traditional method from a semi-arid region. Beverages 4(4):103

    Article  Google Scholar 

  • Nicolli KP, Welke JE, Closs M, Caramão EB, Costa G, Manfroi V, Zini CA (2015) Characterization of the volatile profile of Brazilian moscatel sparkling wines through solid phase microextraction and gas chromatography. J Braz Chem Soc 26(7):1411–1430

    Google Scholar 

  • OIV (2020) State of the World Vitivinicultural Sector in 2019. International Organisation of Vine and Wine. http://www.oiv.int/js/lib/pdfjs/web/viewer.html?file=/public/medias/7298/oiv-state-of-the-vitivinicultural-sector-in-2019.pdf. Accessed 21 Oct 2020

  • Olegário LS, Andrade JKS, Andrade GRS, Denadai M, Cavalcanti RL, da Silva MAAP, Narain N (2019) Chemical characterization of four Brazilian brown propolis: an insight in tracking of its geographical location of production and quality control. Food Res Int 123:481–502

    Article  PubMed  Google Scholar 

  • Pereira GE, Guerra C, de Amorim FM, Souza JF, Lima LLA, Lima MS, Padilha CV, Protas JFS, Zanus MC, and Tonietto J (2018) Vinhos Tropicais do Semiárido do Brasil Desvendando o potencial Vitivinícola desta Nova Fronteira Geográfica do Vinho. Embrapa Uva e Vinho-Artigo Em Periódico Indexado (ALICE)

  • Pérez-Magariño S, Ortega-Heras M, Bueno-Herrera M, Martínez-Lapuente L, Guadalupe Z, Ayestarán B (2015) Grape variety, aging on lees and aging in bottle after disgorging influence on volatile composition and foamability of sparkling wines. LWT Food Sci Technol 61(1):47–55

    Article  Google Scholar 

  • Pherobase (2020) http://www.pherobase.com/database/kovats/kovatsindex.php.  Accessed 11 Nov 2020

  • Ruberto G, Renda A, Amico V, Tringali C (2008) Volatile components of grape pomaces from different cultivars of Sicilian Vitis vinifera L. Biores Technol 99(2):260–268

    Article  CAS  Google Scholar 

  • Ruiz J, Kiene F, Belda I, Fracassetti D, Marquina D, Navascués E, Calderón F, Benito A, Rauhut D, Santos A, Benito S (2019) Effects on varietal aromas during wine making: a review of the impact of varietal aromas on the flavor of wine. Appl Microbiol Biotechnol 103(18):7425–7450

    Article  CAS  PubMed  Google Scholar 

  • Sacks GL, Gates MJ, Ferry FX, Lavin EH, Kurtz AJ, Acree TE (2012) Sensory threshold of 1, 1, 6-trimethyl-1, 2-dihydronaphthalene (TDN) and concentrations in young Riesling and non-Riesling wines. J Agric Food Chem 60(12):2998–3004

    Article  CAS  PubMed  Google Scholar 

  • Sánchez-Palomo E, Trujillo M, García Ruiz A, González Viñas MA (2017) Aroma profile of malbec red wines from La Mancha region: Chemical and sensory characterization. Food Res Int 100:201–208

    Article  PubMed  Google Scholar 

  • Serra-Cayuela A, Jourdes M, Riu-Aumatell M, Buxaderas S, Teissedre PL, López-Tamames E (2014) Kinetics of browning, phenolics, and 5-hydroxymethylfurfural in commercial sparkling wines. J Agric Food Chem 62(5):1159–1166

    Article  CAS  PubMed  Google Scholar 

  • Shinohara T (1985) Gas chromatographic analysis of volatile fatty acids in wines. Agric Biol Chem 49(7):2211–2212

    CAS  Google Scholar 

  • Siedenberg DR, Thaines AH, and Baggio DK (2017). Desenvolvimento Regional Sob a Ótica Do Reconhecimento Da Indicação Geográfica: O Case Do Vale Dos Vinhedos, a Partir Da Percepção Dos Atores Sociais. Gestão & Regionalidade 33(99)

  • Soares RD, Welke JE, Nicolli KP, Zanus M, Caramão EB, Manfroi V, Zini CA (2015) Monitoring the evolution of volatile compounds using gas chromatography during the stages of production of Moscatel sparkling wine. Food Chem 183:291–304

    Article  CAS  PubMed  Google Scholar 

  • Tao Y-S, Li H (2009) Active volatiles of Cabernet Sauvignon wine from Changli County. Nat Sci 1:176–182

    Google Scholar 

  • The good scents company (2020) http://www.thegoodscentscompany.com/search2.html. Accessed 11 Nov 2020

  • Torrens J, Riu-Aumatell M, Vichi S, Lopez-Tamames E, Buxaderas S (2010) Assessment of volatile and sensory profiles between base and sparkling wines. J Agric Food Chem 58(4):2455–2461

    Article  CAS  PubMed  Google Scholar 

  • Tufariello M, Pati S, D’Amico L, Bleve G, Losito I, Grieco F (2019) Quantitative issues related to the headspace-SPME-GC/MS analysis of volatile compounds in wines: the case of Maresco sparkling wine. LWT 108:268–276

    Article  CAS  Google Scholar 

  • Ubeda C, Kania-Zelada I, del Barrio-Galán R, Medel-Marabolí M, Gil M, Peña-Neira A (2019) Study of the changes in volatile compounds, aroma and sensory attributes during the production process of sparkling wine by traditional method. Food Res Int 119:554–563

    Article  CAS  PubMed  Google Scholar 

  • Vararu F, Moreno-García J, Zamfir CI, Cotea VV, Moreno J (2016) Selection of aroma compounds for the differentiation of wines obtained by fermenting musts with starter cultures of commercial yeast strains. Food Chem 197:373–381

    Article  CAS  PubMed  Google Scholar 

  • Voce S, Škrab D, Vrhovsek U, Battistutta F, Comuzzo P, Sivilotti P (2019) Compositional characterization of commercial sparkling wines from cv. Ribolla Gialla produced in Friuli Venezia Giulia. European Food Res Technol 245(10):2279–2292

    Article  CAS  Google Scholar 

  • Wang XC, Li AH, Dizy M, Ullah N, Sun WX, Tao YS (2017) Evaluation of aroma enhancement for “Ecolly” dry white wines by mixed inoculation of selected Rhodotorula mucilaginosa and Saccharomyces cerevisiae. Food Chem 228:550–559

    Article  CAS  PubMed  Google Scholar 

  • Welke JE, Zanus M, Lazarotto M, Pulgati FH, Zini CA (2014) Main differences between volatiles of sparkling and base wines accessed through comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometric detection and chemometric tools. Food Chem 164:427–437

    Article  CAS  PubMed  Google Scholar 

  • Wu J, Liu Y, Zhao H, Huang M, Sun Y, Zhang J, Sun B (2021) Recent advances in the understanding of off-flavors in alcoholic beverages: generation, regulation, and challenges. J Food Compos Anal 103:104117

    Article  CAS  Google Scholar 

  • Zhao P, Gao J, Qian M, Li H (2017) Characterization of the key aroma compounds in Chinese syrah wine by gas chromatography-olfactometry-mass spectrometry and aroma reconstitution studies. Molecules 22:1045

    Article  PubMed Central  Google Scholar 

  • Ziółkowska A, Wąsowicz E, Jeleń HH (2016) Differentiation of wines according to grape variety and geographical origin based on volatiles profiling using SPME-MS and SPME-GC/MS methods. Food Chem 213:714–720

    Article  PubMed  Google Scholar 

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Acknowledgements

The authors thank the winery for the partnership

Funding

The National Council for Scientific and Technological (Conselho Nacional de Desenvolvimento Científico e Tecnológico-CNPq) provided financial support to this study.

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Authors and Affiliations

  1. Department of Gastronomy, Federal University of Paraíba, João Pessoa, Paraiba, 58058-600, Brazil

    Samara de Macêdo MORAIS

  2. Department of Food Engineering, Federal University of Paraíba, João Pessoa, Paraiba, 58051-900, Brazil

    Mércia de Sousa GALVÃO, Leila Moreira de CARVALHO, Lary Souza OLEGARIO & Marta Suely MADRUGA

  3. Brazilian Agricultural Research CorporationEmbrapa Grape & Wine, Bento Gonçalves, Rio Grande do Sul, 95701-008, Brazil

    Giuliano Elias PEREIRA

  4. Department of Rural Technology, Rural Federal University of Pernambuco, Recife, Pernambuco, 52171-900, Brazil

    Luciana Leite de Andrade LIMA

  5. Department of Chemical Engineering, Federal University of Paraíba, João Pessoa, , Paraiba, 58051-900, Brazil

    Flávio Luiz Honorato da SILVA

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  1. Samara de Macêdo MORAIS
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Contributions

Samara de Macêdo Morais: methodology, validation, formal analysis, investigation, data curation, writing—original draft, writing—review & editing, visualization.

Mércia de Sousa Galvão: validation, formal analysis, data curation.

Leila Moreira de Carvalho: validation, formal analysis, data curation.

Lary Souza Olegario: data curation, writing—original draft, writing—review & editing, visualization.

Giuliano Elias Pereira: supervision, writing—review & editing, funding acquisition.

Luciana Leite de Andrade Lima: term, resources, supervision, writing—review & editing.

Flávio Luiz Honorato da Silva: term, resources, supervision, writing—review & editing.

Marta Suely Madruga: term, conceptualization, resources, writing—review & editing, supervision, project administration, funding acquisition.

Corresponding author

Correspondence to Lary Souza OLEGARIO.

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Conflict of interest

Samara de Macêdo MORAIS declares she has no conflict of interest. Mércia de Sousa GALVÃO declares she has no conflict of interest. Leila Moreira de CARVALHO declares she has no conflict of interest. Lary Souza OLEGARIO declares he has no conflict of interest. Giuliano Elias PEREIRA declares he has no conflict of interest. Luciana Leite de Andrade LIMA declares she has no conflict of interest. Flávio Luiz Honorato da SILVA declares he has no conflict of interest. Marta Suely MADRUGA declares she has no conflict of interest.

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de Macêdo MORAIS, S., de Sousa GALVÃO, M., de CARVALHO, L.M. et al. Potential Typicality Marker of Volatile Composition of Commercial Sparkling Wines from the Caatinga Biome. Food Anal. Methods 15, 3346–3364 (2022). https://doi.org/10.1007/s12161-022-02374-4

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