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Stability Studies of Agrifood Reference Materials Under Different Conditions of Storage by Near-Infrared Spectroscopy

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Abstract

Reference materials (RM) play an increasingly important role for laboratories. The aim of this work is to compare different conditions of storage and assess the stability of agrifood external reference materials (ERM). These materials could be used as tools by laboratories notably for their quality control procedure. However, as the other RM, their stability must be assessed during stability studies. The determination of the limiting date of stability (LDS), defined as the period during which analytes called marker of stability are still considered as stable, is used on this purpose. The influences of the environmental factor were tested by the application of full experimental designs with two tested environmental factors: the temperature (storage at +4 °C or +20 ± 10 °C) and the composition of the atmosphere (absence or presence of gases in the packaging). Thus, the setting under vacuum increases clearly the stability for the studied analyte. Almost all ERM stored in the best conditions have a determined LDS higher than those stored in current condition of storage. Indeed, the bread wheat ERM LDS is higher than the current storage of 24 months

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References

  • Akaike H (1974) Factor analysis and AIC. Psychometrica 52:317–332

    Article  Google Scholar 

  • Amigo JM, Arana G, Etxebarria N, Fernández LÁ (2004) Emerging needs for sustained production of laboratory reference materials. Trends Anal Chem 23(1):80–85

    Article  CAS  Google Scholar 

  • Axon TG, Brown R, Hammond SV, Maris SJ (1998) Focusing near infrared spectroscopy on the business objectives of modern pharmaceutical production. J Near Infrared Spectrosc. 6:13–19

    Google Scholar 

  • Blanco M, Villarroya I (2002) NIR spectroscopy: a rapid-response analytical tool. Trends Anal Chem 21:240–250

    Article  CAS  Google Scholar 

  • Bertrand D (2002) La spectroscopie proche infrarouge et ses applications dans les industries de lalimentation animale INRA Prod Anim. INRA Prod Anim 15(3):209–219

    CAS  Google Scholar 

  • Büning-Pfaue H (2003) Analysis of water in food by near infrared spectroscopy. Food Chem 82:107–115

    Article  Google Scholar 

  • Cocchi M, Durante C, Foca G, Marchetti A, Tassi L, Ulrici A (2006) Durum wheat adulteration detection by NIR spectroscopy multivariate calibration. Talanta 68:1505–1511

    Article  CAS  Google Scholar 

  • Deplagne J, Vial J, Pichon V, Lalere B, Hervouet G, Hennion MC (2006) Feasibility study of a reference material for water chemistry : Long term stability of triazine and phenylurea residues stored in vials or on polymeric sorbents. J Chromatogr A 112(1):31–37

    Article  Google Scholar 

  • Emons H, Linsinger TPJ, Gawlik BM (2004) Reference materials: terminology and use. Can’t one see the forest for the trees? Trends Anal Chem 23(6):442–449

    Article  CAS  Google Scholar 

  • Emons H, Fajgelj A, Van der Veen AMH, Watters R (2006) New definitions on reference materials. Accredit Qual Assur 10:576–578

    Article  CAS  Google Scholar 

  • Esteve MJ, Frigola A, Rodrigo C, Rodrigo D (2005) Effect of storage period under variable conditions on the chemical and physical composition and colour of Spanish refrigerated orange juices. Food Chem Toxicol 43(9):1413–1422

    Article  CAS  Google Scholar 

  • ISO Guide 30 (1989) Terms and definitions used in connection with reference materials. ISO, Geneva

  • ISO 13528 (2005) Statistical methods for use in proficiency testing by interlaboratory comparisons, ISO, Geneva

  • ISO 5725-5 (2005) Accuracy (trueness and precision) of measurement methods and results—Part 5: Alternative methods for the determination of the precision of a standard measurement method ISO, Geneva

  • Kiermeier A, Jarrett RG, Verbyla AP (2004) A new approach to estimating shelf-life. Pharm Stat 3:03–11

    Article  Google Scholar 

  • Lafargue ME, Feinberg M, Daudin JJ, Rutledge DN (2003) Detection of heterogeneous wheat samples using near infrared spectroscopy. J Near Infrared Spectrosc 11:109–121

    CAS  Google Scholar 

  • Linsinger TPJ, Pauwels J, Van der Veen AMH, Schimmel H, Lamberty A (2001) Estimating the uncertainty of stability for matrix CRMs. Accredit Qual Assur 6(20):20–25

    Article  CAS  Google Scholar 

  • Næs T, Isaksson T, Fearn T, Davies T (2002) A user-friendly guide to multivariate calibration and classification. NIR Publication, Chichester

    Google Scholar 

  • NF FD V03-115 (1996). Analyse des produits agricoles et alimentaires-Guide pour l’utilisation des matériaux de référence, AFNOR Paris la Défense

  • Nyati H (2000) An evaluation of the effect of storage and processing temperatures on the microbiological status of sous vide extended shelf-life products. Food Control 11(6):471–476

    Article  Google Scholar 

  • Özogul F, Polat A, Özogul Y (2006) Quality assessment of wild European eel (Anguilla anguilla) stored in ice. Food Chem 85(1):49–57

    Article  Google Scholar 

  • Quevauviller P (2002) Matériaux de référence pour l’environnement. Paris, Edition TEC et DOC

    Google Scholar 

  • Quevauviller P, Cámara C, Kramer KJM (1999) EC initiatives for quality assurance training in analytical chemistry. Trends Anal Chem 18(9-10):644–649

    Article  CAS  Google Scholar 

  • Sarembaud JA, Feinberg M (2007) Comparison of shelf-life appraisal techniques for the estimation of the limiting date of stability for agrifood reference materials. Accredit Qual Assur 12(2):75–83

    Article  CAS  Google Scholar 

  • Schwartz G (1978) Estimating the dimension of a model. Ann Statist 6:2745–2756

    Google Scholar 

  • Some IT, Bogaerts P, Hanus R, Hanocq M, Dubois J (1999) Incorporating batch effects in the estimation of drug stability parameters using an Arrhenius model. Int J Pharm 184(2):165–172

    Article  CAS  Google Scholar 

  • Van der Veen AMH, Linsinger TPJ, Lamberty A, Pauwels J (2001) Uncertainty calculations in the certification of reference materials 4. Characterisation and certification. Accredit Qual Assur 6:257–263

    Article  Google Scholar 

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Correspondence to Max Feinberg.

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Sarembaud, J., Platero, G. & Feinberg, M. Stability Studies of Agrifood Reference Materials Under Different Conditions of Storage by Near-Infrared Spectroscopy. Food Anal. Methods 1, 227–235 (2008). https://doi.org/10.1007/s12161-008-9034-3

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