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In-situ synthesis of Ti3SiC2 via FHP method

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Abstract

MAX phase Ti3SiC2 has been synthesized via fast hot pressing (FHP) based on the raw materials of Ti, Si, TiC and Al powders with a molar ratio of 1:1.2:2.3:0.3. The theoretical thermodynamic calculation and DSC test were adopted to verify the feasibility of the synthetic route and sintering temperature. The X-ray diffraction (XRD) result indicated that there were few impurity phases except Ti3SiC2 formed in the sintered sample. The sectional morphology was observed by scanning electron microscope with almost all the platelike-shaped phases, which conformed to the morphology feature of Ti3SiC2. Transmission electron microscopy has been brought to demonstrate the accurate phase composition as Ti3SiC2 combined with the PDF card of XRD analysis.

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Acknowledgements

The study was financially supported by Funding for school-level research projects of Yancheng Institute of Technology (No. xjr2021040, xjr2021058), Yancheng basic research project (No. YCBK202249) and Opening fund of Yancheng Polytechnic College (No. YGKF202003).

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Authors and Affiliations

  1. School of Intelligent Manufacturing, Yancheng Polytechnic College, Yancheng, 224005, China

    Liu Zhang & Nengjun Ben

  2. School of Materials Science and Engineering, Yancheng Institute of Technology, Yancheng, 224001, China

    Liu Zhang, Zirun Yang, Wenhao Gu, Kai Luo & Fang Yu

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  1. Liu Zhang
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  2. Zirun Yang
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  3. Nengjun Ben
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Correspondence to Liu Zhang.

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Zhang, L., Yang, Z., Ben, N. et al. In-situ synthesis of Ti3SiC2 via FHP method. Bull Mater Sci 47, 31 (2024). https://doi.org/10.1007/s12034-023-03110-2

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  • DOI: https://doi.org/10.1007/s12034-023-03110-2

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