Skip to main content
SpringerLink
Log in

Characteristic of silver nanowires prepared by polyol method based on orthogonal experimental design

  • Published:
Bulletin of Materials Science Aims and scope Submit manuscript

Abstract

In this study, silver nanowires (AgNWs) were prepared by the polyol method using silver nitrate (AgNO3) as the silver source and polyvinylpyrrolidone (PVP) as the structure-directing agent under different reaction conditions. In order to obtain AgNWs with good uniformity and electrical conductivity, the orthogonal experiment method was adopted to design an experimental scheme. The scanning electron microscope, energy-dispersive X-ray spectrometer, X-ray diffraction, UV-2550 UV–Visible spectrophotometer, transmission electron microscope, Fourier transform infrared and Raman spectra were combined to characterize synthesized AgNWs. It can be concluded from experimental data that when the reaction temperature is 150°C, the ratio of AgNO3 to PVP is 1:3, the drop rate of PVP is 65 ml h–1, with the existence of ferric chloride (FeCl3), and the AgNWs exhibit optimal morphology with the diameter ranging from 60 to 200 nm. The results in this study will provide experimental guide for controllable formation of AgNWs.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6
Figure 7

Similar content being viewed by others

References

  1. Zhao B, Qi N, Zhang K Q and Gong X 2016 Phys. Chem. Chem. Phys. 18 15289

    Article  CAS  Google Scholar 

  2. Kim J, Lim J W, Mota F M, Lee J E, Boppella R, Lim K Y et al 2016 Nanoscale 8 18938

    Article  CAS  Google Scholar 

  3. Yu X M, Yu X, Zhang J J, Zhang D K, Ni J, Cai H K et al 2015 Mater. Lett. 145 219

    Article  CAS  Google Scholar 

  4. Wei Y, Chen S, Lin Y, Yuan X and Liu L 2015 J. Mater. Chem. C 4 935

    Article  Google Scholar 

  5. Zhang Z H, Chen L L, Yang X, Li T K, Chen X, Li X F et al 2019 IEEE Electron Device Lett. 40 111

    Google Scholar 

  6. Ji D, Wang Y, Chen S, Chen S G, Zhang Y L, Li L et al 2018 J. Solid State Electrochem. 22 2287

    Article  CAS  Google Scholar 

  7. Jorik V D G, Spinelli P and Polman A 2012 Nano Lett. 12 3138

    Article  Google Scholar 

  8. Cui S Q, Liu C and Yang Z S 2007 Mater. Des. 28 722

    Article  CAS  Google Scholar 

  9. Ilie A, Crampin S, Karlsson L and Wilson M 2012 Nano Res. 5 833

    Article  CAS  Google Scholar 

  10. Lin Y H, Chen K T and Ho J R 2011 Jpn. J. Appl. Phys. 50 065002

    Article  Google Scholar 

  11. Zhao T, Fan J B, Cui J, Liu J H, Xu X B and Zhu M Q 2011 Chem. Phys. Lett. 501 414

    Article  CAS  Google Scholar 

  12. Tsuji M, Matsumoto K, Jiang P, Matsuo R, Tang X L and Kamarudin K S N 2008 Colloids Surf. A Physicochem. Eng. Asp. 316 266

    Article  CAS  Google Scholar 

  13. Yang Y, Hu Y Y, Xiong X H and Qin Y Z 2013 RSC Adv. 3 8431

    Article  CAS  Google Scholar 

  14. Mohanty P, Yoon I, Kang T, Seo K, Varadwaj K S K, Choi W et al 2007 J. Am. Chem. Soc. 129 9576

    Article  CAS  Google Scholar 

  15. Zhu Q, Zhang Z, Sun Z, Cai B and Cai W J 2016 Appl. Phys. A 122 618

    Article  Google Scholar 

  16. Ashkarran A A and Derakhshi M 2015 J. Clust. Sci. 26 1901

    Article  CAS  Google Scholar 

  17. Chen D P, Qiao X L, Qiu X L, Chen J G and Jiang R Z 2011 J. Mater. Sci. Technol. 22 6

    Google Scholar 

  18. Jiu J, Sugahara T, Nogi M and Suganuma K 2013 J. Nanopart. Res. 15 1588

    Article  Google Scholar 

  19. Jones M R, Osberg K D, Macfarlane R J, Langille M R and Mirkin C A 2011 Chem. Rev. 111 3736

    Article  CAS  Google Scholar 

  20. Ahn K W, Lim J Y, Yang J H and Kim S G 2010 J. Nanopart. Res. 12 2457

    Article  CAS  Google Scholar 

  21. Korte K E, Skrabalak S E and Xia Y 2008 J. Mater. Chem. 18 437

    Article  CAS  Google Scholar 

  22. Meng X W, Mao Y Y, Yang Y W, Hu C Y, Guo J M and Li Y Q 2017 Precious Metals 38 2

    Google Scholar 

Download references

Acknowledgements

This study was gratefully supported by the Foundation project of Jiangsu Advanced Textile Engineering Technology Center (Grant No. XJFZ/2018/03) and Science and Technology Guiding Project of China National Textile and Apparel Council (Grant No. 2020064).

Author information

Authors and Affiliations

  1. National Engineering Laboratory for Modern Silk, College of Textile and Clothing Engineering, Soochow University, Suzhou, 215000, China

    Hui-mei Zhang, Yan Zhang, Jia-wen Zhang, Xu Ye, Yuan-yuan Li & Ping Wang

Authors
  1. Hui-mei Zhang
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Yan Zhang
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Jia-wen Zhang
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Xu Ye
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. Yuan-yuan Li
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. Ping Wang
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Ping Wang.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Zhang, Hm., Zhang, Y., Zhang, Jw. et al. Characteristic of silver nanowires prepared by polyol method based on orthogonal experimental design. Bull Mater Sci 44, 117 (2021). https://doi.org/10.1007/s12034-021-02395-5

Download citation

  • Received:

  • Accepted:

  • Published:

  • DOI: https://doi.org/10.1007/s12034-021-02395-5

Keywords

Search

Navigation