Abstract
Nanocrystalline Ba2NdSbO6, a complex cubic perovskite metal oxide, powders were synthesized by a self-sustained combustion method employing citric acid. The product was characterized by X-ray diffraction, differential thermal analysis, thermogravimetric analysis, Fourier transform infrared spectroscopy, transmission electron microscopy and scanning electron microscopy. The as-prepared powders were single phase Ba2NdSbO6 and a mixture of polycrystalline spheroidal particles and single crystalline nanorods. The Ba2NdSbO6 sample sintered at 1500°C for 4 h has high density (∼ 95% of theoretical density). Sintered nanocrystalline Ba2NdSbO6 had a dielectric constant of ∼ 21; and dielectric loss = 8 × 10−3 at 5 MHz.
Similar content being viewed by others
References
Corsmit A F, Hoefdraad H F and Blasse G 1972 J. Inorg. Nucl. Chem. 34 3401
Gleiter H 2000 Acta Mater. 48 1
Jose R, James J, John A M, Sundararaman D, Divakar R and Koshy J 1999 Nanostruct. Mater. 11 623
Jose R, James J, John A M, Divakar R and Koshy J 2000 J. Mater. Res. 15 2125
John A M, Jose R, Divakar R and Koshy J 2002 J. Nanosci. Nanotechnol. 2 107
Kimura T and Tokura Y 2000 Ann. Rev. Mater. Sci. 30 451
Karagedov G R and Lyakhov N Z 1999 Nanostruct. Mater. 11 559
Lichtenburg F, Herrnberger A, Weidenmann K and Mannhart J 2001 Prog. Solid State Chem. 29 1
Nyguist R N and Kagel R O 1971 Infrared spectra of inorganic compounds (New York: Academic Press)
Nakamoto K 1986 Infrared and Raman spectra of inorganic and coordination compounds (New York: Wiley) 4th edn
Ravichandran D, Roy R, Ravindranathan P and White W 1999 J. Am. Ceram. Soc. 82 1082
Suryanarayana C 1994 Bull. Mater. Sci. 17 307
Saberi A, Golestani-Fard F, Sarpoolaky H, Willert-Porada M, Gerdes T and Simon R 2008 J. Alloy. Comp. 462 142
Vivekanandhan S, Venkateswarlu M and Satyanarayana N 2008 J. Alloy. Comp. 462 328
Wariar P R S, Kurian J, Sajith P K, Babu T G N and Koshy J 1997 Modern Phys. Lett. B11 889
Wang J, Dongmei W, Jumin X and Beng N W 1999 J. Am. Ceram. Soc. 82 477
Yu J, Liu S, Xiu Z, Yu W and Feng G 2008 J. Alloy. Comp. 461 L17
Zheng W, Pang W and Meng G 1998 Mater. Lett. 37 276
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Kavitha, V.T., Jose, R., Ramakrishna, S. et al. Combustion synthesis and characterization of Ba2NdSbO6 nanocrystals. Bull Mater Sci 34, 661 (2011). https://doi.org/10.1007/s12034-011-0178-1
Received:
Revised:
Published:
DOI: https://doi.org/10.1007/s12034-011-0178-1