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Combustion synthesis and characterization of Ba2NdSbO6 nanocrystals

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Abstract

Nanocrystalline Ba2NdSbO6, a complex cubic perovskite metal oxide, powders were synthesized by a self-sustained combustion method employing citric acid. The product was characterized by X-ray diffraction, differential thermal analysis, thermogravimetric analysis, Fourier transform infrared spectroscopy, transmission electron microscopy and scanning electron microscopy. The as-prepared powders were single phase Ba2NdSbO6 and a mixture of polycrystalline spheroidal particles and single crystalline nanorods. The Ba2NdSbO6 sample sintered at 1500°C for 4 h has high density (∼ 95% of theoretical density). Sintered nanocrystalline Ba2NdSbO6 had a dielectric constant of ∼ 21; and dielectric loss = 8 × 10−3 at 5 MHz.

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Correspondence to P. R. S. Wariar.

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Kavitha, V.T., Jose, R., Ramakrishna, S. et al. Combustion synthesis and characterization of Ba2NdSbO6 nanocrystals. Bull Mater Sci 34, 661 (2011). https://doi.org/10.1007/s12034-011-0178-1

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  • DOI: https://doi.org/10.1007/s12034-011-0178-1

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