Abstract
A new method was developed which enabled us to obtain high-resolution images of the distribution of an oil-borne stain in a saw-textured plywood surface. The method involved treating 90 μm thick plywood sections, which had been cut transversely through the wood-coating interface using a sliding microtome, with osmium tetroxide (OsO4) prior to examination with a field-emission scanning electron microscope (FE-SEM) operating in backscattered electron imaging (BEI) mode. The combination of OsO4 staining and use of FE-SEM-BEI afforded excellent contrast differentiation between the coating and wood cell walls, revealing coating penetration into even nano-size cell wall cracks and delaminations formed during band-sawing of the plywood. The novel technique described adds a new dimension to probing wood–coating interface.
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References
Williams RS, Feist WC, Effect of Preweathering, Surface Roughness and Wood Species on the Performance of Paint and Stains J. Coat. Technol. 66, 109–121 (1994)
Richter K, Feist WC, Knaebe MT, The Effect of Surface Roughness on the Performance of Finishes. Part 1. Roughness Characterization and Stain Performance Forest Prod. J., 45, 91–97 (1995)
Dawson BSW, Gottgens A, Hora G, Natural Weathering Performance of Exterior Wood Coatings on Pinus sylvestris and Pinus radiata in Germany and New Zealand J. Coat. Technol. Res., 2, 539–546 (2005)
Singh AP, Dawson BSW, Microscopic Assessment of the Effect of Saw-textured Pinus radiata Plywood Surface on the Distribution of a Film-Forming Acrylic Stain J. Coat. Technol. Res. 3, 193–201 (2006)
Feist WC, Weathering Performance of Painted Wood Pretreated with Water-Repellant Preservatives Forest Prod. J. 40, 21–26 (1990)
Singh AP, Dawson BSW, Confocal Microscope—A Valuable Tool for Examining Wood-Coating Interface J. Coat. Technol. Res., 1, 236–237 (2004)
Feist WC, Weathering Performance of Finished Southern Pine Plywood Siding Forest Prod. J., 38, 22–28 (1988)
Carter, HW, “Backscattered Electron Imaging of Biological Specimens.” In: Proceedings of the 14th Annual Conference of the Microbeam Analysis Society, San Antonio, 1–2, 1979
Harris LG, ap Gwynn I, Richards RG, Contrast Optimization for Backscattered Electron Imaging of Resin Embedded Cells Scanning Microsc. 13, 71–81 (1999)
Richards RG, Owen GRh, ap Gwynn I, Low Voltage Backscattered Electron Imaging (<5 kV) using Field Emission Scanning Electron Microscopy Scanning Microsc. 13, 55–60 (1999)
Herzog B, Goodell B, Lopez-Anido R, Electron Microprobe Imaging for the Characterization of Polymer Matrix Composites Composites: Part A, 35, 1075–1080 (2004)
DeNee, PB, Carpenter, RL, “Application of Heavy Metal Staining (OsO4)/Backscattered Electron Imaging Technique to the Study of Organic Aerosols.” In: Proceedings of the 14th Annual Conference of the Microbeam Analysis Society, San Antonio, 8–10, 1979
Schraufnagel DE, Ganesan DP, Tracers in Vascular Casting Resins Enhance Backscattering Brightness Scanning Microsc. 12, 631–639 (1998)
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Singh, A.P., Ratz, A. & Dawson, B.S.W. A novel method for high-resolution imaging of coating distribution within a rough-textured plywood surface. J Coat Technol Res 4, 207–210 (2007). https://doi.org/10.1007/s11998-007-9019-y
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DOI: https://doi.org/10.1007/s11998-007-9019-y