Abstract
The dipping of berries in a dilute solution of sodium hydroxide during a short time was evaluated as pretreatment undertaken prior to convective dehydration of wine grapes. The impact of the sodium hydroxide content and dipping time on weight loss (WL) at different dehydration times was thoroughly assessed using central composite design (CCD) and response surface methodology (RSM). Furthermore, the effects of these two variables were also investigated on the skin mechanical properties of dehydrated grapes. The effect of these two pretreatment factors on the dehydration kinetics and skin hardness was satisfactorily fitted to regression models. The berry pretreatment with low sodium hydroxide contents (from 10 to 20 g/L) facilitated the dehydration process during the first 5 days when dipping times longer than 300 s were used. From the seventh day of dehydration, at which time the average WL% was close to 50, the highest values of WL% were obtained using intermediate sodium hydroxide contents and dipping times (around 45 g/L and 185 s, respectively). Because skin hardness affects the dehydration kinetics during postharvest withering, the strongest decrease in skin hardness corresponded to these last berry pretreatment conditions, whereas the greatest increase required the highest sodium hydroxide contents and longest dipping times. The quality of berries dehydrated may be influenced by the pretreatment conditions used, and the present study contributes to increase the knowledge on this effect to a better management of the alkaline pretreatment and dehydration process.
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Angulo, O., Fidelibus, M. W., & Heymann, H. (2007). Grape cultivar and drying method affect sensory characteristics and consumer preference of raisins. Journal of the Science of Food and Agriculture, 87, 865–870.
Azzouz, S., Guizani, A., Jomaa, W., & Belghith, A. (2002). Moisture diffusivity and drying kinetic equation of convective drying of grapes. Journal of Food Engineering, 55, 323–330.
Bai, Y., Shafiur Rahman, M., Perera, C. O., Smith, B., & Melton, L. D. (2002). Structural changes in apple rings during convection air-drying with controlled temperature and humidity. Journal of Agricultural and Food Chemistry, 50, 3179–3185.
Barbanti, D., Mora, B., Ferrarini, R., Tornielli, G. B., & Cipriani, M. (2008). Effect of various thermo-hygrometric conditions on the withering kinetics of grapes used for the production of “Amarone” and “Recioto” wines. Journal of Food Engineering, 85, 350–358.
Barbosa de Lima, A. G., Delgado, J. M. P. Q., Neto, S. R. F., & Franco, C. M. R. (2015). Intermittent drying: fundamentals, modeling and applications. In J. M. P. Q. Delgado & A. G. Barbosa de Lima (Eds.), Drying and energy technologies (pp. 19–41). Switzerland: Springer Intern. Publ.
Bellincontro, A., De Santis, D., Botondi, R., Villa, I., & Mencarelli, F. (2004). Different postharvest dehydration rates affect quality characteristics and volatile compounds of Malvasia, Trebbiano and Sangiovese grapes for wine production. Journal of the Science of Food and Agriculture, 84, 1791–1800.
Bellincontro, A., Nicoletti, I., Valentini, M., Tomas, A., De Santis, D., Corradini, D., & Mencarelli, F. (2009). Integration of nondestructive techniques with destructive analyses to study postharvest water stress of winegrapes. American Journal of Enology and Viticulture, 60, 57–65.
Bingol, G., Roberts, J. S., Balaban, M. O., & Onur Devres, Y. (2012). Effect of dipping temperature and dipping time on drying rate and color change of grapes. Drying Technology, 30, 597–606.
Bolin, H. R., & Huxsoll, C. C. (1987). Scanning electron microscope/image analyzer determination of dimensional postharvest changes in fruit cells. Journal of Food Science, 6, 1649–1650.
Botondi, R., Lodola, L., & Mencarelli, F. (2011). Postharvest ethylene treatment affects berry dehydration, polyphenol and anthocyanin content by increasing the activity of cell wall enzymes in Aleatico wine grape. European Food Research and Technology, 232, 679–685.
Chong, C. H., Law, C. L., Cloke, M., Abdullah, L. C., & Daud, W. R. W. (2008). Drying kinetics, texture, color, and determination of effective diffusivities during sun drying of Chempedak. Drying Technology, 26, 1286–1293.
Contreras, C., Martín-Esparza, M. E., Chiralt, A., & Martínez-Navarrete, N. (2008). Influence of microwave application on convective drying: effects on drying kinetics, and optical and mechanical properties of apple and strawberry. Journal of Food Engineering, 88, 55–64.
De Belie, N., Tu, K., Jancsok, P., & De Baerdemaeker, J. (1999). Preliminary study on the influence of turgor pressure on body reflectance of red laser light as a ripeness indicator for apples. Postharvest Biology and Technology, 16, 279–284.
Delgado, J. M. P. Q., & Barbosa de Lima, A. G. (2015). Drying and energy technologies. Switzerland: Springer Intern. Publ.
Di Matteo, M., Cinquanta, L., Galiero, G., & Crescitelli, S. (2000). Effect of a novel physical pretreatment process on the drying kinetics of seedless grapes. Journal of Food Engineering, 46, 83–89.
Doymaz, I., & Altıner, P. (2012). Effect of pretreatment solution on drying and color characteristics of seedless grapes. Food Science and Biotechnology, 21, 43–49.
Doymaz, I., & Pala, M. (2002). The effects of dipping pretreatments on air-drying rates of the seedless grapes. Journal of Food Engineering, 52, 413–417.
Femenia, A., Sánchez, E. S., Simal, S., & Rosselló, C. (1998). Effects of drying pretreatments on the cell wall composition of grape tissues. Journal of Agricultural and Food Chemistry, 46, 271–276.
Gabas, A. L., Menegalli, F. C., & Telis-Romero, J. (1999). Effect of chemical pretreatment on the physical properties of dehydrated grapes. Drying Technology, 17, 1215–1226.
Giacosa, S., Torchio, F., Río Segade, S., Caudana, A., Gerbi, V., & Rolle, L. (2012). Varietal relationship between skin break force and off-vine withering process for winegrapes. Drying Technology, 30, 726–732.
International Organization of Vine and Wine. (2008). Recueil International des Méthodes d’Analyse des Vins et des Moûts. Paris: OIV.
Lara, I., Belge, B., & Goulao, L. F. (2014). The fruit cuticle as a modulator of postharvest quality. Postharvest Biology and Technology, 87, 103–112.
Letaief, H., Rolle, L., Zeppa, G., & Gerbi, V. (2008). Assessment of grape skin hardness by a puncture test. Journal of the Science of Food and Agriculture, 88, 1567–1575.
López de Lerma, N., Moreno, J., & Peinado, R. A. (2014). Determination of the sun-drying time for Vitis vinifera L. cv. Tempranillo grapes by E-nose analysis and characterization of their volatile composition. Food and Bioprocess Technology, 7, 732–740.
Mencarelli, F., & Tonutti, P. (2013). Sweet, reinforced and fortified wines: Grape biochemistry, technology and vinification, Wiley-Blackwell, A John Wiley & Sons, Ltd., publication.
Mencarelli, F., Bellincontro, A., Nicoletti, I., Cirilli, M., Muleo, R., & Corradini, D. (2010). Chemical and biochemical change of healthy phenolic fractions in winegrape by means of postharvest dehydration. Journal of Agricultural and Food Chemistry, 58, 7557–7564.
Muganu, M., Bellincontro, A., Barnaba, F. E., Paolocci, M., Bignami, C., Gambellini, G., & Mencarelli, F. (2011). Influence of bunch position in the canopy on berry epicuticular wax during ripening and on weight loss during postharvest dehydration. American Journal of Enology and Viticulture, 62, 91–98.
Rahman, M. S. (2005). Dried food properties: challenges ahead. Drying Technology, 23, 695–715.
Ramming, D. W. (2009). Water loss from fresh berries of raisin cultivars under controlled drying conditions. American Journal of Enology and Viticulture, 60, 208–214.
Río Segade, S., Soto Vázquez, E., Orriols, I., Giacosa, S., & Rolle, L. (2011). Possible use of texture characteristics of winegrapes as markers for zoning and their relationship with anthocyanin extractability index. International Journal of Food Science and Technology, 46, 386–394.
Rolle, L., Caudana, A., Giacosa, S., Gerbi, V., & Río Segade, S. (2011a). Influence of skin hardness on dehydration kinetics of wine grapes. Journal of the Science of Food and Agriculture, 91, 505–511.
Rolle, L., Gerbi, V., Schneider, A., Spanna, F., & Río Segade, S. (2011b). Varietal relationship between instrumental skin hardness and climate for grapevines (Vitis vinifera L.). Journal of Agricultural and Food Chemistry, 59, 10624–10634.
Rolle, L., Torchio, F., Giacosa, S., Río Segade, S., Cagnasso, E., & Gerbi, V. (2012). Assessment of physicochemical differences in Nebbiolo grape berries from different production areas and sorted by flotation. American Journal of Enology and Viticulture, 63, 195–204.
Rolle, L., Giacosa, S., Río Segade, S., Ferrarini, R., Torchio, F., & Gerbi, V. (2013). Influence of different thermohygrometric conditions on changes in instrumental texture properties and phenolic composition during postharvest withering of ‘Corvina’ winegrapes (Vitis vinifera L.). Drying Technology, 31, 549–564.
Rutledge, D. N., & Barros, A. S. (2002). Durbin–Watson statistic as a morphological estimator of information content. Analytica Chimica Acta, 454, 277–295.
Sato, A., Yamada, M., Hiroshi, I., & Hirakawa, N. (2000). Optimal spatial and temporal measurement repetition for reducing environmental variation of berry traits in grape breeding. Scientia Horticulturae, 85, 75–83.
Serratosa, M. P., Lopez-Toledano, A., Merida, J., & Medina, M. (2008). Changes in color and phenolic compounds during the raisining of grape cv. Pedro Ximenez. Journal of Agricultural and Food Chemistry, 56, 2810–2816.
Serratosa, M. P., Márquez, A., Lopez-Toledano, A., & Merida, J. (2012). Sensory analysis of sweet musts in Pedro Ximenez cv. grapes dried using different methods. South African Journal of Enology and Viticulture, 33, 14–20.
Serratosa, M. P., Márquez, A., Moyano, L., Zea, L., & Merida, J. (2014). Chemical and morphological characterization of Chardonnay and Gewürztraminer grapes and changes during chamber-drying under controlled conditions. Food Chemistry, 159, 128–136.
Torchio, F., Cagnasso, E., Gerbi, V., & Rolle, L. (2010). Mechanical properties, phenolic composition and extractability indices of Barbera grapes of different soluble solids contents from several growing areas. Analytica Chimica Acta, 660, 183–189.
Torchio, F., Río Segade, S., Gerbi, V., Cagnasso, E., & Rolle, L. (2011). Changes in chromatic characteristics and phenolic composition during winemaking and shelf-life of two types of red sweet sparkling wines. Food Research International, 44, 729–738.
Vázquez, G., Chenlo, F., Moreira, R., & Costoyas, A. (2000). Effects of various treatments on the drying kinetics of Muscatel grapes. Drying Technology, 18, 2131–2144.
Veraverbeke, E. A., Verboven, P., Scheerlinck, N., Hoang, M. L., & Nicolaï, B. M. (2003). Determination of the diffusion coefficient of tissue, cuticle, cutin and wax of apple. Journal of Food Engineering, 58, 285–294.
Xiao, H.-W., Pang, C.-L., Wang, L.-H., Bai, J.-W., Yang, W.-X., & Gao, Z.-J. (2010). Drying kinetics and quality of Monukka seedless grapes dried in an air-impingement jet dryer. Biosystems Engineering, 105, 233–240.
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Onofrio Corona and Fabrizio Torchio contributed equally to this work.
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Corona, O., Torchio, F., Giacosa, S. et al. Assessment of Postharvest Dehydration Kinetics and Skin Mechanical Properties of “Muscat of Alexandria” Grapes by Response Surface Methodology. Food Bioprocess Technol 9, 1060–1069 (2016). https://doi.org/10.1007/s11947-016-1697-y
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DOI: https://doi.org/10.1007/s11947-016-1697-y