Abstract
With supercritical CO2 fluid extraction(SCFE), essential oil was extracted from three cultivars of Xianning osmanthus. The fresh osmanthus flower was processed with a petroleum ether digestion method to produce the extractum. The yields of essential oil and extractum were 0.19 % and 0.13 % (m/m) respectively. The essential oil and fragrance composition and content extracted were analyzed with gas chromatography-mass spectrometer (GC-MS). The result showed that essential oil contained 36.99%(area/total area) of ionone, ionol and 13.11% of linalool; ionone and ionol contained in extractum were as high as up to 33.33%, while linalool up to 21.92%. Whether essential oil or extractum contains only about 40% fat acid and other ester matters. None of environmental estrogen (phthalic ester) was found in fragrance ingredients. The result also showed that the quality of O. fragrans Albus group fragrance in Xianning is better than that produced in Hangzhou and Anhui districts.
Similar content being viewed by others
References
Susanne B, Masaya K, Miwako K, et al. Functional characterization of a carotenoid cleavage dioxygenase 1 and its relation to the carotenoid accumulation and volatile emission during the floral development of Osmanthus fragrans Lour [J]. Journal of Experimental Botany, 2010, 61(11): 2967–2977.
Zang Dekui, Xiang Qibai. Studies on the cultivar classification of chinese sweet Osmanthus [J]. Chinese Garden, 2004, 11: 40–49(Ch).
Chen Hongguo, Wang Hua. The study and the application of Osmanthus resource and its development in Xianning [J]. Journal of Xianning College, 2004, 24(3): 116–118(Ch).
Maddocks-Jennings W, Wilkinson J. Aromatherapy practice in nursing: Literature review [J]. J Adv Nurs, 2004, 48(1): 93–103.
Keegan L. Therapies to reduce stress and anxiety [J]. Crit Care Nurs Clin North Am, 2003, 15(3): 321–327.
Margo A H. Essential oils for management of symptoms in critically ill patients [J]. American Journal of Critical Care, 2008, 17: 160–163.
Wang Lan. Exploitation and use of natural essential oil from plant [J]. China Oils and Fats, 2003, 28(12): 86–89(Ch).
Wang Guangyao, Zhou Hu, Zeng Xiaofeng. Advances in the research and the development of plant essential oils [J]. Food Science and Technology, 2006, 5: 12–14(Ch).
Wang Chengzhong, Su Yue, Guo Yinlon. Analysis of the volatile components from flowers and leaves of Osmanthus fragrans Lour. by Headspace-GC-MS [J]. Chinese Journal of Organic Chemistry, 2009, 29(6): 948–955(Ch).
Feng Jianyue, Zhao Jing, Huang Qiaoqiao, et al. Study on aroma components of Osmanthus by absorption wire gas chromatography-mass spectrometry [J]. Journal of Zhejiang University(Science Edition), 2001, 28(6): 672–675(Ch).
Hu Chundi, Liang Yizeng, Zeng Maomao. Analysis on different volatile oil composition of different Osmanthus species [J]. Chemical Reagent, 2010, 32(3): 231–234(Ch).
Sun Peng, Liu Wenwen. Study progress on extraction and application of essential oil from plants [J]. Gansu Science and Technology, 2007, 23(5): 139–141(Ch).
Qu Xinhua. Extraction and separation technique of essential oil from plants [J]. Journal of Anhui Agricultural Sciences, 2007, 35(32): 10194–10195(Ch).
Machida K, Sakamoto S, Kikuchi M. Structure elucidatio and NMR spectral assignments of four neolignan glycosides with enantiometric aglycones from Osmanthus ilicifolius [J]. Magn Reson Chem, 2008, 46: 990–994.
Zhang Hui, Kong Fanxiang, Wang Shihe, et al. Analysis and prediction of combination efects of estrogenic environmental pollutants [J]. Journal of Southeast University (Nnatural Sscience Edition), 2008, 38(3): 488–492(Ch).
Jani D, Künzler J. Supercritical fuild extraction based purification of silicone oil for vitreoretinal tamponade use [J]. Invest Ophthalmol Vis Sci, 2008, 49: 5990.
Chao Wenjun, Wu Dingxin, Mao Guofang. Supercritical fuild extraction of vegetable essential oil [J]. Journal of Beijing Forestry University, 1998, 20(1): 67–74(Ch).
Xu Pengxiang, Jia Weimin, Bi Liangwu, et al. Gas chromatographic technologies for the analysis of essential oil of aromatic plants [J]. Journal of Analytical Science, 2004, 20(3): 312–316(Ch).
Yang Zai, Chen Jiaming, Huang Xiaolan. New technology of extracting effective components of natural plant-supercritical fuild extraction tecchnology [J]. Feed Review, 2005, 6: 30–33(Ch).
Tao Qing, Xu Dexu, Lü Jianquan. Study on the Supercritical CO2 fuild extraction of Osmanthus fragrans [J]. Food Research and Development, 2007, 28(7): 57–60(Ch).
Tian Guanghui, Liu Cunfang, Gu Tianqi, et al. Analysis of aroma components from the senescence flower of Osmanthus fragrans by GC-MS [J]. Journal of Anhui Agri Sci, 2008, 36(17): 7214–7216(Ch).
Li Zuguang, Cao Hui, Zhu Guohua, et al. Study on chemical constituents of fragrance released from fresh flowers of three different Osmanthus franrans Lour. during different florescence [J]. Chemistry and Industry of Forest Products, 2008, 28(3): 75–80(Ch).
Mai Qiujun. Analysis of chemical constituents of Osmanthus absolute oil [J]. Journal of Guangdong University of Technology, 2000, 17(1): 73–75(Ch).
Xu Jiming, Li Jinshun. Chemical research of Osmanthus essential oil [J]. Chinese Journal of Analysis Laboratory, 2007, 26(1): 39–41(Ch).
Wu Huamei, Chen Xun, He Xiangyin, et al. The chemical constituents of the absolute oils from Osmanthus fragrans flowers [J]. Acta Botanica Ynnnanica, 1997, 19(2): 213–216 (Ch).
Zang Jian. The Research on the Osmanthus Oil Extraction and Composition Analysis [D]. Hangzhou: Zhejiang Industrial University, 2006: 213–216(Ch).
Ding Lixin, Zhang Yu, Yu Decheng. Antioxidant and anti-inflammatory activities in vivo from Osmanthus fragrans Lour [J]. Heilongjiang Medicine and Pharmacy, 2009, 32(4): 7(Ch).
Ding Lixin, Zhang Lanlan, Zhang Yujie, et al. Extraction and purification of flavonoids from Osmanthus fragrans Lour [J]. Heilongjiang Medicine and Pharmacy, 2008, 31(5): 23–24(Ch).
Author information
Authors and Affiliations
Corresponding author
Additional information
Foundation item: Supported by the Manufacture-Learning-Research Cooperation Funded Projects of the Education Department in Hubei Province( C2010064)
Biography: LI Fafang, female, Ph. D., research direction: evaluation and processing of the osmanthus fragrans resources.
Rights and permissions
About this article
Cite this article
Li, F., Huang, Q. Analysis of fragrance composition in three cultivars of Osmanthus fragrans Albus group flower by gas chromatography-mass spectrometry. Wuhan Univ. J. Nat. Sci. 16, 342–348 (2011). https://doi.org/10.1007/s11859-011-0761-8
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11859-011-0761-8
Key words
- Xianning
- Osmanthus fragrans
- supercrifieal CO2 fluid extration(SCFE)
- extractum
- gas chromatography-mass spectrometer(GC-MS)