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Microstructural Evolution and Bio-Corrosion Behavior of a CP-Ti Processed by Multi-Pass of Severe Plastic Deformation

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Abstract

The microstructure evaluation and phase transformation of multi-pass friction stir-processed (FSP) commercially pure titanium were investigated using optical microscopy, scanning electron microscopy equipped with a backscatter detector, and electron backscatter diffractometer. The microstructure characterization shows that the grain refinement mechanism changed with the increasing number of passes. The equiaxed α grains in the untreated sample changed to lath-shaped grains surrounded by serrated grain boundaries, and produced Widmanstätten morphology during the cooling cycle of FSP. The higher micro-hardness values and bio-corrosion resistances of the FSP-treated samples are due to their lower grain size compared to the untreated samples. Furthermore, the presence of lath-shaped Widmanstätten morphology shows a higher micro-hardness value and lower bio-corrosion resistance.

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Authors and Affiliations

  1. Department of Materials Engineering, Faculty of Engineering, University of Gonabad, Gonabad, Iran

    Mojtaba Vakili-Azghandi & S. M. Moosavi Nezhad

  2. Department of Materials Science and Engineering, Sharif University of Technology, Tehran, Iran

    Mohammad Famil Hatami

  3. Department of Mechanical Engineering, Faculty of Engineering, University of Gonabad, Gonabad, Iran

    Seyed Amir Hoseini Sabzevari

  4. Department of Chemistry, Faculty of Science, University of Gonabad, Gonabad, Iran

    Valiollah Mandanipour

  5. Department of Mechanical Engineering, University of Saskatchewan, Saskatoon, SK, S7 N 5A9, Canada

    Jerzy A. Szpunar

Authors
  1. Mojtaba Vakili-Azghandi
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  2. Mohammad Famil Hatami
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  3. Seyed Amir Hoseini Sabzevari
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  4. S. M. Moosavi Nezhad
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  6. Jerzy A. Szpunar
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Correspondence to Mojtaba Vakili-Azghandi.

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Vakili-Azghandi, M., Famil Hatami, M., Hoseini Sabzevari, S.A. et al. Microstructural Evolution and Bio-Corrosion Behavior of a CP-Ti Processed by Multi-Pass of Severe Plastic Deformation. JOM 74, 4621–4631 (2022). https://doi.org/10.1007/s11837-022-05415-9

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  • DOI: https://doi.org/10.1007/s11837-022-05415-9

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