The deformation behavior, microstructure, phase composition, and mechanical and functional properties of Ti-50.9 at.%Ni shape memory alloy during uniaxial compression in the temperature range from 25°C to 1000°C have been analyzed and are discussed herein. It was found that the deformation temperature of 300°C marked a boundary for the transition from the low- to high-temperature type of flow curves; achievement of the steady-state deformation stage was observed across a wide range of deformation temperatures. Following comprehensive analysis of the obtained data, the temperature ranges of the dynamic processes of recovery, polygonization, and recrystallization of the Ti-50.9 at.%Ni alloy were determined. Deformation in the range of dynamic polygonization is accompanied by not only the formation of B2-austenite and R-phase, but also the precipitation of fine Ti3Ni4 particles during deformational aging. The highest shape recovery characteristics were obtained after deformation of the Ti-50.9 at.%Ni alloy in the temperature range from 300°C to 600°C.
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The reported study was funded by RFBR (Project No. 19-33-60090) and part of the TEM and X-ray analyses by the Ministry of Science and Higher Education of the Russian Federation within the framework of the State Task (Project Code 0718-2020-0030).
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Komarov, V., Khmelevskaya, I., Karelin, R. et al. Deformation Behavior, Structure, and Properties of an Aging Ti-Ni Shape Memory Alloy after Compression Deformation in a Wide Temperature Range. JOM 73, 620–629 (2021). https://doi.org/10.1007/s11837-020-04508-7