Abstract
Iron removal from silicon powder waste by ultrasound-assisted leaching has been investigated and the leaching conditions optimized to an ultrasonic frequency of 80 kHz, ultrasonic power of 270 W, temperature of 60°C, and sulfuric acid concentration of 12%, achieving an iron removal fraction of 95.24%. The maximum iron removal fraction was obtained after 80 min of leaching without ultrasound, whereas ultrasound-assisted leaching could achieve the same removal fraction after 50 min under the same conditions. The dissolution of iron is a two-step process and follows a homogeneous control model with a second-order rate-controlling step. With the aid of ultrasound, the reaction rate constants khs increased from 0.0677–0.0995 to 0.0792–0.1914 and from 0.0285–0.1086 to 0.0399–0.1422 in the first and second leaching stage, respectively. This increase of the khs values further supports the enhancement induced by the application of ultrasound.
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Acknowledgements
This work was supported by the National Key Research and Development Program of China (Grant Nos. 2018YFC1901804 and 2018YFC1901805) and the National Natural Science Foundation of China (Grant Nos. 21978045 and U1902219).
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Kong, J., Xing, P., Wei, D. et al. Ultrasound-Assisted Leaching of Iron from Silicon Diamond-Wire Saw Cutting Waste. JOM 73, 791–800 (2021). https://doi.org/10.1007/s11837-020-04497-7
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DOI: https://doi.org/10.1007/s11837-020-04497-7