Abstract
Lowering the cost of feedstock powder has been a major issue for wider applications of additive manufacturing (AM) of titanium (Ti) and its alloys. A novel and inexpensive Ti sponge material was selected as a precursor and processed using a CSIRO proprietary powder manipulation technology (PMT). The manipulated powder was characterized in terms of the particle size distribution (PSD), roundness, flowability in the Hall Funnel flowmeter, static angle of repose (AOR), apparent density and tap density. In addition, a universal powder bed (UPB) system was used to characterize the manipulated powder behavior after raking. Two benchmark powders, virgin Arcam Ti-6Al-4V powder and used Arcam Ti-6Al-4V powder, were assessed for a comparison. PMT processing of the Ti powder precursor produced near spherically shaped Ti powder in the size range of 75–106 µm, which performed very similarly to the used Arcam powder in the UPB system. The CSIRO PMT offers a cost-effective manipulation process to produce Ti powder promising for AM applications, while the UPB system allows a quick assessment of the powder spreading behavior in AM processes.
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References
M.J. Donachie, Titanium: A Technical Guide (Materials Park, OH: ASM International, 2000), p. 47.
L. Thijs, F. Verhaeghe, T. Craeghs, J.V. Humbeeck, and J.P. Kruth, Acta Mater. 58, 3303 (2010).
L.E. Murr, S.M. Gaytan, D.A. Ramirez, E. Martinez, J. Hermandez, K.N. Amato, P.W. Shindo, F.R. Medina, and R.B. Wicker, J. Mater. Sci. Tech. 28, 1 (2012).
L.E. Murr, S.M. Gaytan, F. Medina, M.I. Lopez, E. Martinez, and R.B. Wicker, (Paper presented at the 25th Southern Biomedical Engineering Conference 2009, Miami, FL, 2009).
L.E. Murr, S.A. Quinones, S.M. Gaytan, M.I. Lopez, A. Rodela, E.Y. Martinez, D.H. Hernandez, E. Martinez, F. Medina, and R.B. Wicker, J. Mech. Behav. Biomed. Mater. 2, 20 (2009).
K.P. Cooper, JOM 53, 29 (2001).
W. Xu, M. Brandt, S. Sun, J. Elambasseril, Q. Liu, K. Latham, K. Xia, and M. Qian, Acta Mater. 85, 74 (2015).
W. Xu, S. Sun, J. Elambasseril, Q. Liu, M. Brandt, and M, Qian, JOM 67 (2015). doi:10.1007/s11837-015-1297-8.
L.E. Murr, E.V. Esquivel, S.A. Quinones, S.M. Gaytan, M.I. Lopez, E.Y. Martinez, F. Medina, D.H. Hernandez, E. Martinez, J.L. Martinez, S.W. Stafford, D.K. Brown, T. Hoppe, W. Meyers, U. Lindhe, and R.B. Wicker, Mater. Charact. 60, 96 (2009).
H.P. Tang, M. Qian, N. Liu, X.Z. Zhang, G.Y. Yang, JOM 67 (2015). doi:10.1007/s11837-015-1300-4.
S.M. Gaytan, L.E. Murr, D.H. Hernandez, E. Martinez, S.A. Quinones, F. Medina, and R.B. Wicker, Supplemental Proceedings: Vol. 1: Fabrication, Materials, Processing and Properties (Warrendale, PA: TMS, 2009), pp. 363–369.
P.A. Kobryn, E.H. Moore, and S.L. Semiatin, Scripta Mater. 43, 299 (2000).
P.A. Kobryn and S.L. Semiatin, J. Mater. Proc. Tech. 135, 330 (2003).
S. Bontha, N.W. Klingbeil, P.A. Kobryn, and H.L. Fraser, Mater. Sci. Eng. A 513–514, 311 (2009).
H. Fukuda, H. Takahashi, K. Kuramoto, and T. Nakano, Mater. Sci. Forum 706, 488 (2012).
M.J. O’Hara and I.B. Cutler, Proceedings of the British Ceramic Society, vol. 12 (Covina, CA: SAMPE, 1969), pp. 145–154.
N.A. Pohlman, J.A. Roberts, and M.J. Gonser, Powder Technol. 228, 141 (2012).
A. Bauereiß, T. Scharowsky, and C. Körner, J. Mater. Proc. Tech. 214, 2522 (2014).
AMETEK Inc., Metal-Powders, http://www.readingalloys.com/Products/Metal-Powders.aspx.
J. Withers, J. Laughlin, and R. Loutfy (Paper presented at PM2014 World Congress, Orlando, FL, 2014).
X. Lu, C.C. Liu, L.P. Zhu, and X.H. Qu, Powder Technol. 254, 235 (2014).
ASTM F1877-05, Standard Practice for Characterization of Particles (West Conshohocken, PA: ASTM, 2010).
ASTM B855-06, Standard Test Method for Volumetric Flow Rate of Metal Powders Using Arnold Meter and Hall Funnel (West Conshohocken, PA: ASTM, 2006).
ASTM B703-05, Standard Test Method for Apparent Density of Powders Using Arnold Meter (West Conshohocken, PA: ASTM, 2005).
ASTM B527-06, Standard Test Method for Determination of Tap Density of Metallic Powders and Compounds (West Conshohocken, PA: ASTM, 2006).
J. Karlsson, A. Snis, H. Engqvist, and J. Lausmaa, J. Mater. Proc. Tech. 213, 2109 (2013).
Arcam AB Inc., New! 50 µm Process for High Resolution and Surface Finish (Mölndal, Sweden: Arcam, 2012), http://www.arcam.com/new-50-um-process-for-high-resolution-and-surface-finish.
C. Mangano, A. Piattelli, S. d’Avila, G. Iezzi, F. Mangano, T. Onuma, and J.A. Shibli, J. Oral. Implantol. 36, 91 (2010).
C.Y. Lin, T. Wirtz, F. LaMarca, and S.J. Hollister, J. Biol. Mater. Res. A 83, 272 (2007).
T. Traini, C. Mangano, R.L. Sammons, F. Mangano, A. Macchi, and A. Piattelli, Dental Mater. 24, 1525 (2008).
A. Santomaso, P. Lazzaro, and P. Canu, Chem. Eng. Sci. 58, 2857 (2003).
Acknowledgements
Y.Y. Sun acknowledges a scholarship received from the China Scholarship Council and a fee waiver scholarship offered by the RMIT University. M. Qian acknowledges the the support from the Australian Research Council (ARC) through the Linkage Projects program under ARC LP140100608.
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Sun, Y.Y., Gulizia, S., Oh, C.H. et al. Manipulation and Characterization of a Novel Titanium Powder Precursor for Additive Manufacturing Applications. JOM 67, 564–572 (2015). https://doi.org/10.1007/s11837-015-1301-3
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DOI: https://doi.org/10.1007/s11837-015-1301-3