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Facile synthesis of imprinted submicroparticles blend polyvinylidene fluoride membranes at ambient temperature for selective adsorption of methyl p-hydroxybenzoate

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Abstract

We developed a simple phase inversion technique to prepare molecularly imprinted membrane (MIM) at room temperature for membrane selective adsorption and separation of methyl p-hydroxybenzoate (M4HB). The prepared SMIP-MIM was characterized by SEM, FT-IR, TGA. Compared with non-imprinted membrane (NIM1-5) adsorbent, SMIP-MIM1-5 adsorbent with high specific surface area and showed higher binding capacity, faster kinetic and better selectively adsorption capacity for M4HB. The maximum isotherm adsorption capacity for M4HB of SMIP-MIM4 was 3.519mg·g−1, and the experimental data was well fitted to the slips model by multiple analysis. The maximum kinetic adsorption capacity and equilibrium adsorption time for SMIP-MIM4 were 1.335mg·g−1 and 160 min, respectively. The mechanism for dynamic adsorption of M4HB onto SMIP-MIM4 was found to follow pseudo-first-order model and pseudo-second-order model. Additionally, the permeability separation factor of SMIP-MIM4 for M4HB compared to a structural analogues methyl 2-hydroxybenzoate (M2HB) could reach 2.847. The adsorption capacity of SMIP-MIM4 for M4HB and M2HB was 0.549mg·cm−2 and 1.563mg·cm−2, respectively. The adsorption behavior of M4HB through SMIP-MIM4 followed the retarded permeation mechanism.

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Authors and Affiliations

  1. School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang, 212013, China

    Yanhua Cui, Minjia Meng, Dongshu Sun, Yan Liu, Jianming Pan, Xiaohui Dai & Yongsheng Yan

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  1. Yanhua Cui
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  2. Minjia Meng
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  3. Dongshu Sun
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  4. Yan Liu
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  5. Jianming Pan
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  6. Xiaohui Dai
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  7. Yongsheng Yan
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Correspondence to Yongsheng Yan.

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Cui, Y., Meng, M., Sun, D. et al. Facile synthesis of imprinted submicroparticles blend polyvinylidene fluoride membranes at ambient temperature for selective adsorption of methyl p-hydroxybenzoate. Korean J. Chem. Eng. 34, 600–608 (2017). https://doi.org/10.1007/s11814-016-0365-2

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  • DOI: https://doi.org/10.1007/s11814-016-0365-2

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