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Preparation of γ-alumina nanoparticle modified polyacrylamide composite and study on its solid phase extraction of Sunset Yellow

  • Biotechnology
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Abstract

An organic-inorganic composite, γ-alumina nanoparticle modified polyacrylamide, was synthesized in this study. The composite was characterized by scanning electron microscope, nitrogen adsorption-desorption measurement, thermal gravimetric analyzer, differential scanning calorimetry, and Fourier-transformed infrared spectrometer. A novel solid-phase extraction method with the synthesized composite as the adsorbent was developed for the enrichment of Sunset Yellow coupled with ultraviolet-visible spectrophotometry. To obtain the optimum extraction efficiency, the experimental parameters in the processes of preparation of the adsorbent and solid-phase extraction were studied including synthesis temperature, synthesis time, the dosage of γ-alumina nanoparticles, sample flow rate, sample pH, eluant concentration, and eluant flow rate. Under the optimum conditions, the detection limit of the developed method was calculated to be 0.037 μg mL−1 with intra-day and inter-day relative standard deviation values of 2.57% and 3.89%, respectively. When the method was applied to the determination of Sunset Yellow in beverages, satisfactory recoveries were obtained in the range of 92.3–109.8%.

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References

  1. K. S. Minioti, C. F. Sakellariou and N. S. Thomaidis, Anal. Chim. Acta, 583, 103 (2007).

    Article  CAS  Google Scholar 

  2. K. Golka, S. Kopps and Z. W. Myslak, Toxicol. Lett., 151, 203 (2004).

    Article  CAS  Google Scholar 

  3. GB 2760-2011, Hygiene standards for use of food additives, Health Ministry of P. R. China, Beijing (2011).

    Google Scholar 

  4. W. J. Li, X. Zhou, S. S. Tong and Q. Jia, Talanta, 105, 386 (2013).

    Article  CAS  Google Scholar 

  5. H.-G. Gao, W.-J. Gong and Y.-G. Zhao, Anal. Sci., 31, 205 (2015).

    Article  CAS  Google Scholar 

  6. J. Zhang, M. Wang, S. Chao, W. Wang, Y. He and Z. Chen, J. Electroanal. Chem., 685, 47 (2012).

    Article  CAS  Google Scholar 

  7. E. C. Vidotti, J. C. Cancino, C. C. Oliveira and M. C. E. Rollemberg, Anal. Sci., 21, 149 (2005).

    Article  CAS  Google Scholar 

  8. N. Djafarzadeh, M. Safarpour and A. Khataee, Korean J. Chem. Eng., 31, 785 (2014).

    Article  CAS  Google Scholar 

  9. R. Qi, X. Zhou, X. Li, J. Ma, C. Lu, J. Mu, X. Zhang and Q. Jia, Analyst, 139, 6168 (2014).

    Article  CAS  Google Scholar 

  10. M. R. Fuh and K. J. Chia, Talanta, 56, 663 (2002).

    Article  CAS  Google Scholar 

  11. W. Liu, W. J. Zhao, J. B. Chen and M. M. Yang, Anal. Chim. Acta, 605, 41 (2007).

    Article  CAS  Google Scholar 

  12. Y. Wang, M. Mei, X. Huang and D. Yuan, Anal. Methods, 7, 551 (2015).

    Article  CAS  Google Scholar 

  13. X. Hu, Q. Cai, Y. Fan, T. Ye, Y. Cao and C. Guo, J. Chromatogr. A, 1219, 39 (2012).

    Article  CAS  Google Scholar 

  14. X. Yu, Y. Sun, C. Z. Jiang, Y. Gao, Y. P. Wang, H. Q. Zhang and D. Q. Song, J. Sep. Sci., 35, 3403 (2012).

    Article  CAS  Google Scholar 

  15. J. Xin, D. Zhao, L. Zhang, Z. Xu, J. Zhou and D. Qu, Chromatographia, 73, 235 (2011).

    Article  CAS  Google Scholar 

  16. R. Su, X. Zhao, Z. Li, Q. Jia, P. Liu and J. Jia, Anal. Chim. Acta, 676, 103 (2010).

    Article  CAS  Google Scholar 

  17. K. Naraghi, H. A. Panahi, A. H. Hassani and E. Moniri, Korean J. Chem. Eng., 31, 1818 (2014).

    Article  CAS  Google Scholar 

  18. J. Ye, S. Liu, M. Tian, W. Li, B. Hu, W. Zhou and Q. Jia, Talanta, 118, 231 (2014).

    Article  CAS  Google Scholar 

  19. Q. Geng and W. Cui, Ind. Eng. Chem. Res., 49, 11321 (2010).

    Article  CAS  Google Scholar 

  20. K. Mahmoudi, K. Hosni, N. Handi and E. Srasra, Korean J. Chem. Eng., 32, 274 (2015).

    Article  CAS  Google Scholar 

  21. Y. Wang and W. Chu, Ind. Eng. Chem. Res., 50, 8734 (2011).

    Article  CAS  Google Scholar 

  22. J. Roh, H. N. Umh, C. M. Yoo, S. Rengaraj, B. Lee and Y. Kim, Korean J. Chem. Eng., 29, 903 (2012).

    Article  CAS  Google Scholar 

  23. Y. S. Al-Degs, A. H. El-Sheikh, M. A. Al-Ghouti, B. Hemmateenejad and G. M. Walker, Talanta, 75, 904 (2008).

    Article  CAS  Google Scholar 

  24. Z. Xu, Q. Zhang and H. H. P. Fang, Crit. Rev. Environ. Sci. Technol., 33, 363 (2003).

    Article  CAS  Google Scholar 

  25. Y. Guan, Y. Mao, D. Wei, X. Wang and P. Zhu, Korean J. Chem. Eng., 30, 1810 (2013).

    Article  CAS  Google Scholar 

  26. J. J. Ye, W. Feng, M. M. Tian, J. L. Zhang, W. H. Zhou and Q. Jia, Anal. Methods, 5, 1046 (2013).

    Article  CAS  Google Scholar 

  27. B. F. Senkal and E. Yavuz, Polym. Adv. Technol., 17, 928 (2006).

    Article  CAS  Google Scholar 

  28. A. Hashem, E. S. Abdel-Halim and H. H. Socker, Polym. Plast. Tech. Eng., 46, 71 (2007).

    Article  CAS  Google Scholar 

  29. G. F. Fanta, R. C. Burr, C. R. Russell and C. E. Rist, J. Appl. Polym. Sci., 10, 929 (1966).

    Article  CAS  Google Scholar 

  30. M. Wu, R. Wu, Z. Zhang and H. Zou, Electrophoresis, 32, 105 (2011).

    Article  Google Scholar 

  31. R. Ahmad and R. Kumar, Clean: Soil, Air, Water, 39, 74 (2011).

    CAS  Google Scholar 

  32. J. Krenkova and F. Foret, J. Sep. Sci., 34, 2106 (2011).

    CAS  Google Scholar 

  33. S. Tong, Q. Liu, Y. Li, W. Zhou, Q. Jia and T. Duan, J. Chromatogr. A, 1253, 22 (2012).

    Article  CAS  Google Scholar 

  34. J. Kujawa, W. Kujawski, S. Koter, A. Rozicka, S. Cerneaux, M. Persin and A. Larbot, Colloids Surf., A, 420, 64 (2013).

    Article  CAS  Google Scholar 

  35. F. Meder, T. Daberkow, L. Treccani, M. Wilhelm, M. Schowalter, A. Rosenauer, L. Mäler and K. Rezwan, Acta Biomater., 8, 1221 (2012).

    Article  CAS  Google Scholar 

  36. M. Tian, W. Feng, J. Ye and Q. Jia, Anal. Methods, 5, 3984 (2013).

    Article  CAS  Google Scholar 

  37. Y. J. Chen, R. Z. Jing, S. C. Cheng, Y. H. Wang, Q. J. Wan, L. Y. Xiong and Z. F. He, J. GuiZhou Agric. Coll., 15, 66 (1996).

    Google Scholar 

  38. S. Xie, F. Svec and J. M. J. Frechet, J. Polym. Sci. Pol. Chem., 35, 1013 (1997).

    Article  CAS  Google Scholar 

  39. F. Svec and J. M. J. Frechet, Chem. Mater., 7, 707 (1995).

    Article  CAS  Google Scholar 

  40. C. H. Shek, J. K. L. Lai, T. S. Gu and G. M. Lin, Nanostruct. Mater., 8, 605 (1997).

    Article  CAS  Google Scholar 

  41. N. Yoshioka and K. Ichihashi, Talanta, 74, 1408 (2008).

    Article  CAS  Google Scholar 

  42. S. P. Alves, D. M. Brum, É. C. Branco de Andrade and A. D. Pereira Netto, Food Chem., 107, 489 (2008).

    Article  CAS  Google Scholar 

  43. M. Ma, X. B. Luo, B. Chen, S. P. Sub and S. Z. Yao, J. Chromatogr. A, 1103, 170 (2006).

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Department of Chemistry and Chemical Engineering, Taiyuan Institute of Technology, Taiyuan, 030008, P. R. China

    Wanjun Li

  2. College of Chemistry, Jilin University, Changchun, 130012, P. R. China

    Qiong Jia & Yuanpeng Wang

  3. State Key Laboratory of Supramolecular Structure and Materials, College of Chemistry, Jilin University, Changchun, 130012, P. R. China

    Zhenyu Zhang

Authors
  1. Wanjun Li
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  2. Qiong Jia
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  3. Zhenyu Zhang
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  4. Yuanpeng Wang
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Correspondence to Wanjun Li.

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Li, W., Jia, Q., Zhang, Z. et al. Preparation of γ-alumina nanoparticle modified polyacrylamide composite and study on its solid phase extraction of Sunset Yellow. Korean J. Chem. Eng. 33, 1337–1344 (2016). https://doi.org/10.1007/s11814-015-0279-4

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  • DOI: https://doi.org/10.1007/s11814-015-0279-4

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