Skip to main content
Log in

A novel and simple approach for the synthesis of Fe3O4-graphene composite

  • Rapid Communication
  • Published:
Korean Journal of Chemical Engineering Aims and scope Submit manuscript

Abstract

High crystalline Fe3O4-graphene composite has been successfully synthesized via one-step thermolysis reaction. The results demonstrated that the attachment of iron-organic complex with graphene oxide sheets can facilely lead to magnetic graphene composites with a time-dependent calcination process. The composite was characterized by scanning electron microscopy, transmission electron microscopy, Raman spectroscopy, X-ray diffraction, and X-ray photoelectron spectroscopy. The high efficient removal of methylene blue determined that Fe3O4-graphene is a promising sorbent material for wastewater treatment.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. H. Jabeen, V. Chandra, S. H. Jung, J.W. Lee, K. S. Kim and S. B. Kim, Nanoscale., 3, 3583 (2011).

    Article  CAS  Google Scholar 

  2. K. Zhang, V. Dwivedi, C.Y. Chi and J. S. Wu, J. Hazard. Mater., 182, 162 (2010).

    Article  CAS  Google Scholar 

  3. J. F. Shen, Y. Z. Hu, M. Shi, N. Li, H.W. Ma and M.X. Ye, J. Phys. Chem. C., 114, 1498 (2010).

    Article  CAS  Google Scholar 

  4. H. P. Cong, J. J. He, Y. Lu and S. H. Yu, Small., 6, 169 (2010).

    Article  CAS  Google Scholar 

  5. X. P. Shen, J. L. Wu, S. Bai and H. Zhou, J. Alloys. Compd., 506, 136 (2010).

    Article  CAS  Google Scholar 

  6. X. Y. Zhang, X. Y. Yang, Y. F. Ma, Y. Huang and Y. S. Chen, J. Nanosci. Nanotechnol., 10, 2984 (2010).

    Article  CAS  Google Scholar 

  7. G.M. Zhou, D.W. Wang, F. Li, L. L. Zhang, N. Li, Z. S. Wu, L. Wen, G. Q. Lu and H. M. Cheng, Chem. Mater., 22, 5306 (2010).

    Article  CAS  Google Scholar 

  8. X.Y. Yang, X.Y. Zhang, Y. F. Ma, Y. Huang, Y. S. Wang and Y. S. Chen, J. Mater. Chem., 19, 2710 (2009).

    Article  CAS  Google Scholar 

  9. F. He, J.T. Fan, D. Ma, L. M. Zhang, C. Leung and H. L. Chan, Carbon., 48, 3139 (2010).

    Article  CAS  Google Scholar 

  10. V. Chandra, J. S. Park, Y. Chun, J.W. Lee, I. C. Hwang and K. S. Kim, ACS Nano., 4, 3979 (2010).

    Article  CAS  Google Scholar 

  11. V. Chandra and K. S. Kim, Chem. Commun., 47, 3942 (2011).

    Article  CAS  Google Scholar 

  12. X. J. Deng, L. L. Lv, H.W. Li and F. Luo, J. Hazard. Mater., 183, 923 (2010).

    Article  CAS  Google Scholar 

  13. H.M. Sun, L. Y. Cao and L. H. Lu, Nano. Res., 4, 550 (2011).

    Article  CAS  Google Scholar 

  14. W. S. Hummers and R. E. Offeman, J. Am. Chem. Soc., 80, 1339 (1958).

    Article  CAS  Google Scholar 

  15. S. H. Lee, H.W. Kim, J. O. Hwang, W. J. Lee, J. Kwon, C.W. Bielawski, R. S. Ruoff and S. O. Kim, Angew. Chem. Int. Ed., 49, 10084 (2010).

    Article  CAS  Google Scholar 

  16. H.M. Ju, S. H. Choi and S. H. Huh, J. Kor. Phys. Soc., 57, 1649 (2010).

    Article  CAS  Google Scholar 

  17. F. Tuinstra and J. L. Koenig, J. Chem. Phys., 53, 1126 (1970).

    Article  CAS  Google Scholar 

  18. A. C. Ferrari and J. Robertson, Phys. Rev. B., 61, 14095 (2000).

    Article  CAS  Google Scholar 

  19. J. Lu, X. Jiao, D. Chen and W. Li, J. Phys. Chem. C., 113, 4012 (2009).

    Article  CAS  Google Scholar 

  20. D. Zhang, Z. Liu, S. Han, C. Li, B. Lei, M. P. Stewart, J.M. Tour and C. Zhou, Nano. Lett., 4, 2151 (2004).

    Article  CAS  Google Scholar 

  21. J. E. Kim, T. H. Han, S. H. Lee, J.Y. Kim, C.W. Ahn, J.M. Yun and S. O. Kim, Angew. Chem. Int. Ed., 50, 3043 (2011).

    Article  CAS  Google Scholar 

  22. J. F. Shen, M. Shi, H.W. Ma, B. Yan, N. Li and M.X. Ye, Mater. Res. Bull., 46, 2077 (2011).

    Article  CAS  Google Scholar 

  23. X.Y. Li, X. L. Huang, D. P. Liu, X. Wang, S.Y. Song, L. Zhou, H. J. Zhang, J. Phys. Chem. C., 115, 21567 (2011).

    Article  CAS  Google Scholar 

  24. Y. Zhang, B. Chen, L.M. Zhang, J. Huang, F. H. Chen, Z. P. Yang, J. L. Yao and Z. J. Zhang, Nanoscale., 3, 1446 (2011).

    Article  CAS  Google Scholar 

  25. G. Williams, B. Seger and P.V. Kamat, ACS Nano., 2, 1487 (2008).

    Article  CAS  Google Scholar 

  26. D.X. Yang, A. Velamakanni, G. Bozoklu, S. J. Park, M. Stoller, R.D. Piner, S. Stankovich, I. H. Jung, D. A. Field, C. A. Ventrice Jr. and R. S. Ruoff, Carbon., 47, 145 (2009).

    Article  CAS  Google Scholar 

  27. C.M. Cowey, K. D. Bartle, M. D. Burford, A. A. Clifford and S. Zhu, J. Chem. Eng. Data., 406, 1217 (1995).

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding authors

Correspondence to Feng-Jun Zhang or Won-Chun Oh.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Zhang, FJ., Liu, J., Zhang, K. et al. A novel and simple approach for the synthesis of Fe3O4-graphene composite. Korean J. Chem. Eng. 29, 989–993 (2012). https://doi.org/10.1007/s11814-012-0031-2

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11814-012-0031-2

Key words

Navigation