Abstract
High crystalline Fe3O4-graphene composite has been successfully synthesized via one-step thermolysis reaction. The results demonstrated that the attachment of iron-organic complex with graphene oxide sheets can facilely lead to magnetic graphene composites with a time-dependent calcination process. The composite was characterized by scanning electron microscopy, transmission electron microscopy, Raman spectroscopy, X-ray diffraction, and X-ray photoelectron spectroscopy. The high efficient removal of methylene blue determined that Fe3O4-graphene is a promising sorbent material for wastewater treatment.
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H. Jabeen, V. Chandra, S. H. Jung, J.W. Lee, K. S. Kim and S. B. Kim, Nanoscale., 3, 3583 (2011).
K. Zhang, V. Dwivedi, C.Y. Chi and J. S. Wu, J. Hazard. Mater., 182, 162 (2010).
J. F. Shen, Y. Z. Hu, M. Shi, N. Li, H.W. Ma and M.X. Ye, J. Phys. Chem. C., 114, 1498 (2010).
H. P. Cong, J. J. He, Y. Lu and S. H. Yu, Small., 6, 169 (2010).
X. P. Shen, J. L. Wu, S. Bai and H. Zhou, J. Alloys. Compd., 506, 136 (2010).
X. Y. Zhang, X. Y. Yang, Y. F. Ma, Y. Huang and Y. S. Chen, J. Nanosci. Nanotechnol., 10, 2984 (2010).
G.M. Zhou, D.W. Wang, F. Li, L. L. Zhang, N. Li, Z. S. Wu, L. Wen, G. Q. Lu and H. M. Cheng, Chem. Mater., 22, 5306 (2010).
X.Y. Yang, X.Y. Zhang, Y. F. Ma, Y. Huang, Y. S. Wang and Y. S. Chen, J. Mater. Chem., 19, 2710 (2009).
F. He, J.T. Fan, D. Ma, L. M. Zhang, C. Leung and H. L. Chan, Carbon., 48, 3139 (2010).
V. Chandra, J. S. Park, Y. Chun, J.W. Lee, I. C. Hwang and K. S. Kim, ACS Nano., 4, 3979 (2010).
V. Chandra and K. S. Kim, Chem. Commun., 47, 3942 (2011).
X. J. Deng, L. L. Lv, H.W. Li and F. Luo, J. Hazard. Mater., 183, 923 (2010).
H.M. Sun, L. Y. Cao and L. H. Lu, Nano. Res., 4, 550 (2011).
W. S. Hummers and R. E. Offeman, J. Am. Chem. Soc., 80, 1339 (1958).
S. H. Lee, H.W. Kim, J. O. Hwang, W. J. Lee, J. Kwon, C.W. Bielawski, R. S. Ruoff and S. O. Kim, Angew. Chem. Int. Ed., 49, 10084 (2010).
H.M. Ju, S. H. Choi and S. H. Huh, J. Kor. Phys. Soc., 57, 1649 (2010).
F. Tuinstra and J. L. Koenig, J. Chem. Phys., 53, 1126 (1970).
A. C. Ferrari and J. Robertson, Phys. Rev. B., 61, 14095 (2000).
J. Lu, X. Jiao, D. Chen and W. Li, J. Phys. Chem. C., 113, 4012 (2009).
D. Zhang, Z. Liu, S. Han, C. Li, B. Lei, M. P. Stewart, J.M. Tour and C. Zhou, Nano. Lett., 4, 2151 (2004).
J. E. Kim, T. H. Han, S. H. Lee, J.Y. Kim, C.W. Ahn, J.M. Yun and S. O. Kim, Angew. Chem. Int. Ed., 50, 3043 (2011).
J. F. Shen, M. Shi, H.W. Ma, B. Yan, N. Li and M.X. Ye, Mater. Res. Bull., 46, 2077 (2011).
X.Y. Li, X. L. Huang, D. P. Liu, X. Wang, S.Y. Song, L. Zhou, H. J. Zhang, J. Phys. Chem. C., 115, 21567 (2011).
Y. Zhang, B. Chen, L.M. Zhang, J. Huang, F. H. Chen, Z. P. Yang, J. L. Yao and Z. J. Zhang, Nanoscale., 3, 1446 (2011).
G. Williams, B. Seger and P.V. Kamat, ACS Nano., 2, 1487 (2008).
D.X. Yang, A. Velamakanni, G. Bozoklu, S. J. Park, M. Stoller, R.D. Piner, S. Stankovich, I. H. Jung, D. A. Field, C. A. Ventrice Jr. and R. S. Ruoff, Carbon., 47, 145 (2009).
C.M. Cowey, K. D. Bartle, M. D. Burford, A. A. Clifford and S. Zhu, J. Chem. Eng. Data., 406, 1217 (1995).
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Zhang, FJ., Liu, J., Zhang, K. et al. A novel and simple approach for the synthesis of Fe3O4-graphene composite. Korean J. Chem. Eng. 29, 989–993 (2012). https://doi.org/10.1007/s11814-012-0031-2
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DOI: https://doi.org/10.1007/s11814-012-0031-2